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In this paper, the influences of acetanilide content on the microstructure and macro properties of polyvinyl chloride were studied by means of differential scanning calorimetry, wide angle X-ray diffraction and scanning electron microscope.

利用差示扫瞄量热法、广角X-射线衍射和扫瞄电镜方法研究了乙酰苯胺质量分数对聚氯乙烯的结晶度、微观形态和宏观机械性能的影响。

The catalysis of single and mixed micelles and functional molecules for alkaline hydrosis of acetanilide has been studied at 40℃ in aqueous acetonitrile solution with UV spectrophotometry.

在40℃下乙腈水溶液中,用紫外分光光度法研究了单一和混合胶束及功能分子对乙酰苯胺碱性水解反应的催化作用。

Alkaline hydrolysis of acetanilide ; single and mixed micelles ; functional molecule ; consecutive first order reaction ; self function regression method

乙酰苯胺碱性水解;单一和混合胶束;功能分子;连续一级反应;自函数回归法

In this paper, acetanilide used as start material was chlorosulfonated, then reacted with alkylamines with different length of carbon chain to prepare 4 p-acetylaminophenylsulfonylalkylamine.

本文以乙酰苯胺为起始原料,经氯磺化后分别和不同碳链的正烷基胺反应制得4种不同碳链长度的对乙酰氨基苯磺酰烷基胺,将其水解后制得了对氨基苯磺酰正丁胺、对氨基苯磺酰正辛胺、对氨基苯磺酰正十二胺和对氨基苯磺酰正十八胺。

Methods Protein in blood and urine was precipitated directly by acetonitrile with acetanilide was used as the internal standard using Agilent Zorbax SB-Aq column (250 mm×4.6 mm, 5 μm). The mixed solvents of water (triethylamine 0.12%, acetic acid 0.12%) and acetonitrile were used as the mobile phase to separate cephalosporins using gradient elution method at 1 mL/min and 254 nm.

以乙酰苯胺为内标,血液和尿液用乙腈直接沉淀蛋白,采用Agilent Zorbax SB-Aq(250 mm×4.6 mm, 5 μm)色谱柱,流动相选用水(含0.12%三乙胺和0.12%乙酸)和乙腈的混合溶剂梯度洗脱,流速1 mL/min,检测波长254 nm。

Acetanilide,hexane diacid and potassium hydrogen phthalate were used as additives to improve polyvinyl chloride crystallinity.

通过傅里叶转换红外光谱、差示扫描量热法及广角X射线衍射法研究了乙酰苯胺、己二酸和邻苯二甲酸氢钾与聚氯乙烯的相容性及对聚氯乙烯结晶度的影响。

The results of clinical assessment showed that levosimendan was safe and effective which could improve the prognosis of the patients and kept normal blood kinetics. By improving the reported synthetic route, levosimendan was synthesized from acetanilide via eight steps of reaction.

本论文探索了左西孟旦的合成路线,对文献报道的合成工艺进行了合理有效的改进,以乙酰苯胺为原料,最终经Friedel-Crafts反应,羰基α-位溴代,丙二酸二乙酯缩合,水解,脱羧,环合,拆分及重氮化加成等八步反应合成了左西孟旦。

In this paper,acetanilide,adipic acid and potassium hydrogen phthalate were chosen as additives to advance polyvinyl chloride to crystallize. The effects of compress mold,annealing temperature and time,additive property and loading on the crystallization,microscopicmorphology and mechanical properties of PVC were studied by means of wide angle X-ray diffraction,differential scanning calorimetry,fourier transform infrared spectrophotometer,scanning electron microscopeand tensile test.

本文利用乙酰苯胺、己二酸和邻苯二甲酸氢钾作为聚氯乙烯结晶改性的添加剂,通过广角X-射线衍射法、差示扫描量热法、傅立叶转换红外光谱、扫瞄电镜和万能电子实验机研究了热压、热处理温度和时间、添加剂结构和质量分数对PVC结晶、微观形态和宏观机械性能的影响。

Anilido-imino nickel complex 1 {(C6H3Me2-2,6)N=CH-5-NO2-C6H3N (C6H3Me2-2,6)}NiBr was first synthesized, and its catalytic behavior toward polymerizations of norbornene and ethylene in the presense of methylaluminoxane were investigated in detail. The complex activated with methylaluminoxane exhibited high activities for norbornene polymerization.

首次合成了苯胺基亚胺镍配合物1{(C6H3Me2-2,6)N=CH-5-NO2-C6H3N(C6H3Me2-2,6)}NiBr,研究了其在助催化剂甲基铝氧烷的作用下对降冰片烯、乙烯的均聚以及对降冰片烯和乙烯的共聚的催化性能。

N -alkylation of aniline by diethyl ether on Al 2O 3 was studied.

研究了在氧化铝催化剂上,苯胺与乙醚气相N -乙基化反应的动力学,得到了幂函数型动力学模型。

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