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The dye intermediate 2,6-dichloro-4-nitroaniline was prepared by direct chloridization of nitroaniline in the solution of hydrochloric acid.

在盐酸溶液中,以对硝基苯胺为原料,采用直接氯化法制取了染料中间体2,6-二氯-4 -硝基苯胺

A monoclonal antibody against nitroaniline was prepared for measuring nitroaniline residuals and for an enzyme linked immuno-sorbent assay reagent kit.

为了测定水中硝基苯胺类化合物,进而开发酶联免疫分析法快速检测方法,制备了抗硝基苯胺单克隆抗体。

This thiosemicarbazide was treated under the catalysis of glacier acetic acid,mercuric acetate giving 2 benzyl 5 phenylamino 1,3,4 thiodiazole and 2 benzyl 5 phenylamino 1,3,4 oxadiazole respectively.

然后分别将其在冰醋酸、醋酸汞存在下关环,制得 2 苯甲基 5 苯胺基 1,3 ,4 噻二唑与 2 苯甲基 5 苯胺基 1,3 ,4 口恶二唑

METHOD Dofetilide was synthesized by steps of reaction (substitution ,reduction, methylsulfonylation and methylammoniation, etc) from p-nitrophenol and p-amino phenethyl alcohol.

以对硝基苯酚为起始原料,经取代、还原、甲磺酰化等反应制得 4甲磺酰苯胺(5 );以对氨基苯乙醇为起始原料,经甲磺酰化、甲氨化等反应制得 4 甲磺酰苯胺(8),再与5经取代反应制得多非利特。

Using phenylamine and acetic acid as raw materials,cyclohexane and toluene-p-sulfonic acid as dehydration and catalyst respectively.

苯胺和冰醋酸为原料,环己烷为脱水剂,对甲苯磺酸为催化剂,采用正交实验法,探讨了乙酰苯胺合成的适宜工艺条件。

Paraacetaminophenyl-β-hydroxyethylsulfone can be used as raw material to produce the target product 2-sulfonic-4-(β-sulphatoethyl-sulphone) phenylamine through sulfonationating and hydrolytic reactions.

本文研究了以对乙酰氨基苯基-β-羟乙基砜为原料,经磺化和水解反应,制得产品2-磺酸-4-苯胺的合成工艺,以及2-磺酸-4-乙基砜基硫酸酯苯胺钠盐后处理的最佳操作工艺。

Sulfonic-4-(β-sulphatoethyl-sulphone) phenylamine is often applied to producing bifunctional-soluble reactive dyes and is an important dye intermediate. It plays an important role in the synthesis of KN style reactive dye M style double reactive dye and modified dissimilar double reactive dye. Used 2-sulfonic-4-(β-sulphatoethyl-sulphone) phenylamine as raw material can improve the uniformly dying performance and scourablility of dyestuff molecules and can improve the firm degree of colour staining.

2-磺酸-4-苯胺是制备水溶性双活性染料的重要中间体,在KN型活性染料、M型双活性染料以及改性异种双活性染料的合成中起着重要的作用,用2-磺酸-4-苯胺作原料合成活性染料可增加染料分子的匀染性和易洗涤性,提高染料的粘色牢度。

Several aminated Fullerene derivatives were synthesized by the reaction of C〓 with phenylamine, diphenylamine and triethylamine etc., the phenomena of fragmentation and aggregation of the aminated Fullerene derivatives in UV laser desorption ionization mass spectrometer was observed, a few nitrogenous poly-Fullerene ions, such as C〓NH, C〓N〓H〓, C〓N〓H〓, C〓N〓H〓, C〓N〓H〓 etc.

对C〓富勒烯与苯胺、二苯胺、三乙胺等形成的加合物在紫外激光解吸电离作用下可以发生不同寻常的裂解和聚合现象进行了研究,认为其形成机理为:上述加合物在紫外激光解吸电离作用下,发生裂解产生C〓NH、C〓N及C〓等离子,然后它们之间发生聚合,形成如:C〓NH、C〓N〓H〓、C〓N〓H〓、C〓N〓H〓、C〓N〓H〓等含氮原子的聚富勒烯离子。

New hyperbranched polymers containing triphenylamine were synthesized by polycyclotrimerization of bis(4-ethynylphenyl)phenylamine and 1-octyne with dicarbonyl- cyclopentadienyl-cobalt CpCo(CO2 as catalyst under ultraviolet irradiation.

在以CpCo2为催化剂和紫外光照射的条件下,以二-(4-乙炔苯基)-苯胺和1-辛炔为单体合成了新型的含三苯胺超支化聚合物。

Keywords hyperbranched polymer;triphenylamine;bis(4-ethynylphenyl)phenylamine;1-octyne;[2+2+2] cyclotrimerization;dicarbonyl-cyclopentadienyl-cobalt catalyst;fluorescence quantum yields

超支化聚合物;三苯胺;二-(4-乙炔苯基)-苯胺; 1-辛炔; [2+2+2]环三聚;二羰基茂钴催化剂;荧光量子效率

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