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An aminobenzene sulfonate-formaldehyde based polymer dispersant with good grinding efficiency was synthesized under alkaline condition using aminobenzene sulfonate, phenol and formaldehyde as main raw materials.

以对氨基苯磺酸、苯酚、甲醛为主要原料,采用碱性合成线路制备了具有助磨效果的氨基磺酸系高效减水剂,系统地研究了单体比例、单体浓度、交联剂用量、反应体系初始pH值、反应时间和反应温度等因素对助剂助磨效果的影响。

To study the contents of amino acids of the samples of mulberry leaves from five varieties,the amino acids of mulberry leaves were derived with o-phthaldialdehyde and 9-fluorenylmetloyl chloroformate in pre-column,and DAD variable-wavelength as measure function,and separated by RP-HPLC.

以邻苯二甲醛与9-芴基羰酰氯作衍生剂,正缬氨酸为内标利用二极管阵列可变波长检测程序,采用柱前衍生反相高效液相色谱法测定5个桑叶品种的氨基酸含量。

After acid hydrolysis of urine, primary amino acids were derivatized with ortho-phthaldialdehyde and removed from the sample by use of silica gel, followed by devivatized of hydroxyproline with 9-fluorenylmethyl chloroformate, and then injected into a C8 reversed-phase column.

采用邻苯二甲醛和芴甲基氯甲酸酯两个衍生剂,先后处理尿标本,以国产C8柱为固定相,在醋酸钠缓冲液中加入23%的乙腈作为洗脱液,3,4-脱氢脯氨酸作为内标。

A novel planar chiral diferrocenylimine-diols 6 was synthesized by the condensation of R, S(subscript p-1-(2-diphenyl hydroxyl methyl) ferrocenylethylamine [R, S(subscript p-4] with phthaldehyde in anhydrous ethanol, and was crystallographically characterized.

通过R,S(下标 p-1-(2-二苯基羟甲基)二茂铁乙胺[R,S(下标 p-4]和对苯二甲醛在无水乙醇中的缩合反应合成了一种新型平面手性双二茂铁亚胺二醇化合物6,并经X-射线衍射分析它的晶体结构。

Methods 151 cars used for different periods of time were selected and the concentrations of formaldehyde,benzene,toluene,dimethylbenzene and TVOC were detected.

方法选择使用不同年限的151辆小汽车,分别测定车厢空气中甲醛、苯、甲苯、二甲苯、TVOC的浓度,同时对驾驶人员的不良反应进行调查。

Methods To detect benzene,methylbenzene, dimethylbenzene ,and formaldehyde levels in indoor air of 48 rooms decorated in different seasons.

方法在春夏季(4~9月)和秋冬季(1~3月,10~12月)选择装修完毕3个月左右尚未入住的居室48户,检测室内空气中的苯、甲苯、二甲苯和甲醛浓度,并进行比较。

Results The exceed standard rates of benzene, methylbenzene, dimethylbenzene, formaldehyde in indoor air were 11.39%, 14.58%, 7.64% and 38.17% respectively.

结果 室内空气中苯、甲苯、二甲苯和甲醛的超标率分别为11.39%、14.58%、7.64%和38.17%。

Methods The levels of formaldehyde, benzene, toluene and dimethylbenzene indoors at different time after decoration were determined with methods described in GB11737 and the dwellers' adverse reaction with a given questionnaire was surveyed????

选择装饰竣工后不同时期的居室,分别测定室内空气中甲醛、苯、甲苯、二甲苯的浓度,同时对居留者的不良反应进行调查。

The extracted components were qualitatively and quantitatively analyzed by gas chromatography mass spectrometry.The results showed that 30,26 compounds were identified from the volatile components extracted by DSE,SDE methods resp.36 kinds of components were extracted by 2 methods in total,among them the content of hexadecanoic aci...

结果表明,从DSE、SDE法提取的挥发性成分中分别鉴定出30(总含量58.24μg/g)、26种化合物总含量(86.66μg/g,2种方法共提取出36种化合物,其中十六酸含量最高,其次为亚油酸、油酸、邻苯二甲酸二异丁酯、间甲苯甲醛、龙脑。

By analyzing and researching the corrosion resistant mechanism of adsorption typal acidification corrosion inhibitor, taking single equational experimental method, making use of mannich reaction and using the hydrochloric acid as catalyst and the ethyl alcohol absolute as solvent, the new acidification corrosion inhibitor HZ-1 is synthesed by formaldehyde、hypnone、aromatic amines in the present research of this thesis.

本文通过对吸附型酸液缓蚀剂缓蚀机理的分析和研究,利用单因素实验方法,采用曼尼希反应,以盐酸为催化剂,无水乙醇为溶剂,用甲醛、苯乙酮、芳香多胺合成了新型酸化缓蚀剂HZ-1。

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