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苯甲醛

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The synthetic condition s of benzaldehyde and glycol acetals by 732#strong acidic ion exchange resin are studied.

研究了苯甲醛与乙二醇在732#强酸性阳离子交换树脂催化下的合成条件,得到了缩醛化反应的最佳合成条件:醛/醇摩尔比为1∶1。

Many kinds of catalysts have been studied respectively in this dissertation.

对苯甲酸加氢还原制备苯甲醛的研究,主要是对其催化剂的研究。

Third, the phenyl aldehyde precipitation method and ion-exchange method were utilized to refine the eluent.

次之,分别采用苯甲醛沉淀法和离子交换法对L-精氨酸粗提液进行纯化精制。

Its reaction with ketenes generated in situ from acid chlorides afforded-4--azetidin-2-one, thus provided a 14-member library of-4--azetidin-2-one with yields 76~91% and an excellent stereoselectivity.

我们从PEG支载的苯甲醛出发,经腙的制备及其氯代之后,在三辛胺作用下,由氯代腙原位生成的腈亚胺与亚胺发生[3+2]偶极环加成反应,得到PEG支载四芳基-4,5-二氢-1,2,4-三氮唑衍生物。

Using PbO2/Ti as anode,pure lead as cathode,H2SO4 as medium,MnSO4 was electrolyzed into Mnin a undivided cell,then,using Mnas oxidant, p-chloro-toluene was oxidized into p-chloro-phenylaldehyde.

采用无隔膜电解槽,以PbO2/Ti为阳极,纯Pb为阴极,MnSO4在H2SO4介质中电解为Mn,于电解槽外氧化对氯甲苯生成对氯苯甲醛

A new Schiff baseH_(2Lhas been synthesized from sulfamethoxazole and complexes of this ligand have been prepared with it and characterized by elemental analysis,infrared spectrum,nuclear magnetic resonance,thermal analysis,molar electric conductance and solubility.

以磺胺甲基异口恶唑与对羟基苯甲醛合成一种新西佛碱(H2L),并用此配体制备8个稀土配合物,通过元素分析、红外光谱、核磁共振、热分析、摩尔电导和溶解性试验对配合物进行了表征。

The new technology, which contained three parts: treating the electrolyte by the activated carbon, stoving solid MnSO〓 and adjusting the acidity in many recycles, was firstly proposed to solve the current efficiency losses, so that possibility of the recycle of the mediator was guaranteed.

首次提出了采用活性炭处理循环电解媒质并包括固体MnSO〓烘干、多次循环酸度进行调整的电合成苯甲醛新工艺,有效地解决了循环电流效率显著下降的问题。

Chapter 3: The microscopic and macroscopic NLO properties of these condensations of aromatic amine with benzaldehyde derivatives were studied.

第三章:从微观和宏观两个方面研究了四类苯甲醛缩芳胺希夫碱衍生物系列二阶非线性光学材料的性质。

High yields of indazoles (70-85%) were obtained in the condensations of aldehydes with various substitution patterns with the exception of those possessing electron-donating groups in the 5-position and the unsubtituted o -fluorobenzaldehyde.

高产量吲唑(1970年至1985年%)获得了各种替代方式醛缩合的例外拥有电子基团的5位和unsubtituted 邻氟苯甲醛

Chapter 2: Four kinds of condensations of aromatic amine with benzaldehyde derivatives were obtained by solid phase synthesis. Their structures were identified by element analysis and 1H NMR spectroscopy. Their SHG properties, fluorescent and thermochromic properties were also tested.

第二章:通过室温固相反应合成了四类苯甲醛缩芳胺希夫碱衍生物,用元素分析和核磁共振对其结构进行了确定,并测试了它们的非线性性质、荧光性质以及热致变色性质。

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然而,正如其名字所指出的那样,CD盘不能写,也不能用任何方式改变其内容。

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