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苯甲醛

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A new method for simultaneous determination of multicomponent with spectrum transform single wavelength spectropotometry is presented.

提出了一种新的单波长法同时测定多组分的光谱变换分光光度法,并以苯甲酸和苯甲醛混合组分为例论证了该方法的可行性。

The results show that myristic acid radical anion of precursor Zn0.78 Al0.2220.22c13h27COO0.81H2O can be almost completely replaced by complex anion [La(TiW11 O39)2]^3- under special controlled reaction conditions.

结果表明,该产物中[La(TiW11O39)2](上标 13-)配阴离子沿其长轴垂直于层板的方向分布于水滑石层板间,产物有规整的层状结构、大的层间距(d003=3.29nm)、良好的结晶度和热稳定性,产物对二甘醇与苯甲酸的酯化反应、二甘醇的脱水环化反应和苯甲醛的氧化反应具有良好的催化性能。

In this paper,ortho nitrobenzaldehyde is prepared with indirect oxo-process for o nitrotoluene .

以邻硝基甲苯为原料,采用间接氧化法制备邻硝基苯甲醛

The intermediate which obtained from oximation of 7a-e reacted withmethyl N-(2-bromomethylphenyl)-N-methoxycarbamate to synthesize oxime ether methyl carbamate 3a-e.

以邻位卤代苯甲醛和3-丁烯-2-醇为原料通过钯催化&一锅法&反应合成了2-乙酰基茚7a-e,7a-e 肟化之后和N-(2-溴甲基苯基)-N-甲氧基氨基甲酸甲酯反应合成了肟醚类氨基甲酸甲酯3a-e,进一步胺解之后得到了肟醚类氨基甲酰甲胺3f-j。

Copper and cobalt oxides catalyst supported on activecarbon showed specific selectivity for salicylaldehyde and realized74% conversion of o-cresol and 57% selectivity for salicylaldehyde.

论文在液相条件下采用多相催化剂和分子氧,首次实现了催化选择氧化邻甲酚和对甲酚合成相应的羟基苯甲醛

A new fullerene derivative containing energy-producing groups was prepared, and the reaction conditions affecting the yield were studied by the kroenecker method. The optimal reaction conditions with a 53.5% yield (based on consumed C60) are: 1:3:6 of molar ratio of C60 , o–nitrobenzaldehyde and sarcosine , 55℃ of reaction temperature, 12 h of reaction time, 40mL of toluene solvent.

利用N-甲基甘氨酸、邻-硝基苯甲醛和C60反应,合成分离出了含有硝基的新型富勒烯吡咯烷衍生物,通过正交试验对其工艺条件进行了研究,探讨了反应物剂量比、温度、时间和溶剂体积对产物产率的影响,得到了合成产物的最佳工艺条件:反应物剂量比为1:3:6、温度为55℃、反应时间为12h、溶剂甲苯体积为40mL,此时产物产率可达到53.5%(以消耗的C60计)。

Results Six compounds were isolated and identified as:5α,8α-epidioxy-(22E,24R)-ergosta-6,22-dien-3β-ol,scopoletin,isofraxidin,p-hydroxy benzaldehyde,3,4,5-trimethoxy benzoic acid,protocatechuic acid ethyl ester...

结果得到6个化合物,分别鉴定为:5α,8α表二氧(22E,24R)麦角甾6,22二烯3β醇、东莨菪素、异秦皮啶、对羟基苯甲醛、3,4,5三甲氧基苯甲酸、原儿茶酸乙酯。结论化合物Ⅰ~Ⅵ均为首次从该属植物中分离得到。

Thiobarbituric acid was synthesized by sulfourea and diethyl malonate in sodium alcohol and 5-Arylidene thiobarbituric acid was prepared by the Knoevenagel condensation reaction from benzaldehyde and thiobarbituric acid.

采用丙二酸二乙酯和硫脲在乙醇钠存在下合成了硫代巴比妥酸,再分别采用固相反应和水相反应,由硫代巴比妥酸和苯甲醛经Knoevenagel缩合反应,制备了5-亚苄基硫代巴比妥酸。

Batch and semi-continuous oxidation of p-xylene to terephthalic acid in oxygen-enriched atmosphere with volume fraction of oxygen from 21% to 80% were investigated.

在体积分数为21%~80%的富氧空气中进行对二甲苯的间歇和半连续氧化反应,获得了富氧条件下对二甲苯氧化反应的固相中间产物(对羧基苯甲醛、对甲基苯甲酸)含量的变化规律。

The target compound was cut off from the middle of the two benzene ring of Biphenyl Tetrazole and the key step was accomplished through Suzuki Coupling reaction.

第二部分:抗高血压药物——缬沙坦的新合成路线研究我们分别以对溴甲苯,对溴苄溴和对溴苯甲醛为起始原料分三条路线完成了缬沙坦的全合成。

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