苯甲醛

The effects of temperature and reaction time on the conversion of phenylaldehyde and yield of cinnamaldehyde were determined from 220℃ to 300℃.

在温度220~300℃范围内，测定了温度和反应时间对苯甲醛转化率和肉桂醛收率的影响。

The results showed that cinnamaldehyde could be synthesized successfully through the reaction of phenylaldehyde with acetaldehyde in near-critical water without adding any catalyst.

在近临界水中，以苯甲醛和乙醛为原料，在无外加任何催化剂的条件下，合成肉桂醛。

Application of organic acid catalysis to the polymerization of pyrroles and pentafluorobenzaldehydes, with the xylene as reaction medium instead of expensive collidine used in the conventional methodology, resulted in a relatively high yield of TPFPPH〓.

本研究利用有机酸如氯乙酸催化吡咯和五氟化苯甲醛聚合，并以二甲苯替代传统方法所用的昂贵溶剂2，4，6-三甲基吡啶，获得了产率较高的TPFPPH〓。

Potassium zinc phosphate was used as the catalyst for Knoevenagel condensation of benzaldehyde with ethyl cyanoacetate.

以磷酸锌钾为催化剂，催化苯甲醛与氰乙酸乙酯进行Knoevenagel缩合反应。

Catalyzed by KF-Al2O3, Knoevenagel condensation of benzaldehyde with ethyl cyanoacetate under microwave irradiation without solvent has been found to proceed with high yield.

采用KF-Al2O3为催化剂，在无溶剂微波辐射下苯甲醛与氰基乙酸乙酯发生 Knoevenagel 缩合反应，得到了较高的产率，并考察了反应条件对产率的影响。

In a similar way, using N,N\'-dibenzyl tartamide as auxiliary,-(2-methyl)allyl-2-chloro-phenyl-methyl azide, a vital intermediate of Repaglinide, can be prepared via asymmetric allylation of o-chlorobenzaldehyde in

产物经氧化和碘加成内酯化反应得到阿伐他汀中间体(3R，5S)-3-羟基-5-碘甲基戊内酯(10)；将N-苄基酒石酸二酰胺用于邻氯苯甲醛的不对称烯丙基化反应以较高光学收率得-甲基烯丙基-2-氯苯基-甲基醇

The first asymmetric total synthesis of coumarinolignoids Daphneticin and it's enantiomer was accomplished starting from 7-hydroxycoumarin and 3, 4, 5-trimethoxybenzaldehyde, in which Sharpless asymmetric dihydroxy reaction was used to construct chiral center, and Mitsunobu reaction was used to obtain desired configuration.

并以7-羟基香豆素和3，4，5-三甲氧基苯甲醛为起始原料，用Sharpless不对称双羟化反应构筑手性中心，用Mitsunobu偶联反应作为关键步骤，合成了手性的香豆素木脂素Daphneticin及其异构体。

Leuco crystal violet lactone was prepared by heating the mixture of dimethylaniline, p- dimethylaminobenzaldehyde and m- dimethylaminobenzoic acid at 60 ℃ for 5 hours in presence of hydrochioric acid and unea and in the nitrogen atmosphere with 72% yield of LCVL.

等摩尔比的N，N-二甲基苯胺和对二甲氨基苯甲醛在盐酸和脲的存在及氮气保护下，80℃反应0.5h，加入间二甲氨基苯甲酸于90℃反应5h。将反应混合物中和，抽滤，得到无色结晶紫内酯，产率为72%。

Leuco crystal violet lactone was prepared by heating the mixture of dimethylaniline, p-dimethylaminobenzaldehyde and m-dimethylaminobenzoic acid at 60℃ for 5 hours in presence of hydrochloric acid and urea and in the nitrogen atmosphere with 72%yield of LCVL.

等摩尔比的N，N-二甲基苯胺和对二甲氨基苯甲醛在盐酸和脲的存在及氮气保护下，80℃反应0.5h，加入间二甲氨基苯甲酸于90℃反应5h。将反应混合物中和，抽滤，得到无色结晶紫内酯，产率为72%。

In the third part of this dissertation, based on the leading compound ACPD, we design and asymmetric syhthesized two analogues: 56 and 57 by using Seebach's self- regeneration strategy to synthesize α,α-disubstituted amino acid as the key step.

论文的第二部分，我们利用我们所开发的合成α，α双取代氨基酸的方法，以对甲基苯甲醛为原料，经过分子内付克烷基化、氧化银氧化和氢化等16步反应，完成了代谢型谷氨酸受体拮抗剂-AIDA的不对称合成。

However, as the name（read－only memory）implies, CD disks cannot be written onorchanged in any way.

然而，正如其名字所指出的那样，CD盘不能写，也不能用任何方式改变其内容。

Galvanizes steel pallet is mainly export which suits standard packing of European Union, the North America. galvanizes steel pallet is suitable to heavy rack. Pallet surface can design plate type, corrugated and the gap form, satisfies the different requirements.

镀锌钢托盘多用于出口，替代木托盘，免薰蒸，符合欧盟、北美各国对出口货物包装材料的法令要求；喷涂钢托盘适用于重载上货架之用，托盘表面根据需要制作成平板状、波纹状及间隔形式，满足不同的使用要求。