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苯甲醛

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METHODS Acetylacetone, 4-Dimethylaminobenzaldehyd and alcohol without aldehyde were used as color reagents. The determination method was colorimetry.

以乙酰丙酮、无醛乙醇和对二甲氨基苯甲醛溶液为显色剂,用比色法测定。

Benzoic acid is both safe to people and acquirable.

苯甲醛是甲苯氧化的中间产物,容易被过氧化成苯甲酸。

Research direction in the future are pointed out, such as further perfection of the electrode material selection and electrolysis without membrane in commercial practice, more attention paid to study and popularization of indirect electro-oxidation, especially of the alkoxy benzaldehydes, and study on the basic theory also should be enhanced.

指出今后应进一步完善电极材料和无隔膜电解等的工业实践,加强间接电氧化特别是烷氧基基苯甲醛的电氧化合成的研究与推广,同时加强基础理论研究。

The condensation of 3 carbethoxy isoquinol 4 one with carbamidine, amidine, carbamide and sulfocarbamide gave isoquinolo pyrimidine derivatives, respectively and isoquinolo quinoline derivatives were synthesized by the reaction of o aminobenzaldehyde or o aminopiperonal with isoquinol 4 one.

报道了利用 3 乙氧甲酰基异喹啉 4 酮分别与胍、脒、脲及硫脲类化合物缩合反应合成异喹啉并嘧啶衍生物,邻氨基苯甲醛、邻氨基胡椒醛分别与异喹啉 4 酮反应合成异喹啉并喹啉化合物。6个新化合物的结构通过元素分析、红外光谱、核磁共振氢谱和质谱予以证

Methods starting from dimethyl succinate and benzaldehyde, mitiglinide calcium was obtained via 7 chain steps including stobble condensation, hydrolization, anhydration, condensation with cis-hexahydroisoindoline, reduction, separation, salt formation.

方法以丁二酸二甲酯和苯甲醛为原料,经stobble缩合、水解、脱水,与顺-全氢异吲哚缩合后经还原、拆分、成盐等7步反应制得糖尿病治疗药物米格列奈钙。

A compound 2-(3-hydroxyphenyl)[60] fullerene pyrrolidine was synthesized by the 1,3-dipolar cycloaddition reaction of the fullerene(C60) and azomethine ylide (prepared from glycine and 3-hydroxybenzaldehyde). The product was characterized by UV-Vis,1H-NMR ,FT-IR and MS. The reaction conditions affecting the yields of product were investigated and the optimum reaction conditions with product yield 75%(based on consumed C60) were:molar ratio of C60∶3-hydroxybenzaldehyde:glycine 1∶3∶6,reaction temperature 95℃,reaction time 18h.

利用甘氨酸和3-羟基苯甲醛与C60发生1, 3-偶极环加成反应,合成分离得到了2-(3-羟基苯基)[60]富勒烯吡咯烷,用UV-Vis、1H-NMR、FT-IR、MS等测试手段表征了产物的结构,并通过单因素方法,探讨了反应条件对产物产率的影响,得到最佳工艺条件:反应物摩尔比1∶3∶6,温度95 ℃,反应时间18 h,产物的产率可达75%(以消耗的C60计)。

We had to give uP it. We began to synthesize another i ntermedi at6,benzal dehyde.

因此,我们采用了合成另一中间体苯甲醛来替代乙酰丙酮的合成。

The kinetic of hydrolysis of benzal chloride was studied by using a new kind of phase transfer catalyst in this paper.

1前言苯甲醛是一种重要的化工中间体,在医药、香料、农药、染料、树脂等工业中用途甚广。

Using benzyl chloride and chlorine as starting materials, benzal chloride is prepared through photo-chlorination in loop reactor.

采用环流反应器、以氯化苄和氯气为原料进行光氯化反应,制备苄叉二氯;将制得的苄叉二氯粗品进行真空精馏得到高纯度的精品;然后用一种新型醇胺类相转移催化剂,分别以盐酸和水作为介质,在 90~ 110℃水解后得到了高纯度的苯甲醛

The procedure of benzal chloride and benzylchloride was obtained by chlorination toluene, then through catalytic acidic hydrolysis and oxidation, produced benzaldehyde.

本文研究了甲苯氯化得到苄叉二氯和氯化苄混合物,然后经催化酸解氧化制备苯甲醛,并探讨了氯化催化酸解及氧化的反应条件。

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