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苯甲醇

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The optimum technical parameters were obtained as follows:bromating temperature is 15℃,solvent is methyl arcohol, bromating agent is BrCl,the molar ratio of 4-hydroxy-benzaldehyde to BrCl is 1:1.15,reaction time is 2.5 hours.

其工艺参数优化如下:溴化时反应温度选择15℃,溶剂选择甲醇+乙酸甲酯,溴化剂选择氯化溴,对羟基苯甲醛与氯化溴之比为1∶1.15,反应时间选择2.5个小时,滴溴时间约半个小时。

Antibacterial deodorizes : The bamboo coal's charcoal structure is compact, the proportion is big, the holes are many, the mineral substance content is rich, therefore has the very strong adsorption resolution capability, to the air sulfide, the nitride, the methyl alcohol, the benzene, the phenol, the chloroform and so on organic pollutant or the harmful chemical substance, can display the outstanding absorption and disappear the smelly function.

六:抗菌除臭:竹炭的炭质结构非常致密、比重大、孔隙多、矿物质含量丰富,因此具有很强的吸附分解能力,对空气中的硫化物、氮化物、甲醇、苯、酚、三氯甲烷等有机污染物或有害化学物质,均能发挥优异的吸收和消臭功能。

Variety is the main business: toluene and xylene, Chunben, solvent oil, methanol, acetone, alcohol and alcohol iso.

主要经营品种有:甲苯、二甲苯、纯苯、溶剂油、甲醇、丙酮、异丁醇和正丁醇。

DPPH method, pyrogallol method and Fenton reaction were used to study the scavenging ability of extracts with 95% ethanol, ethyl acetate, acetone, acetic acid, chloroform, methanol to free radical activity.

方法]应用DPPH法、邻苯三酚自氧化法和Fenton反应分别研究了浓度95%乙醇、乙酸乙酯、丙酮、乙酸、氯仿、甲醇提取物清除自由基活性的能力。

They are insoluble in water, ethanol, methanol, acetone, chloroform and benzene, but soluble in DMA, DMF and DMSO.

它们溶于N,N-二甲基甲酰胺、N,N-二甲基乙酰胺和二甲基亚矾等溶剂,但不溶于水、乙醇、甲醇、丙酮、氯仿和苯。

The results showed that Kaidimycin was chemically neutral, macrocylic polylactones, stable and liable to dissolve into water and pyridine, slight to dissolve into methanol, ethanol and N-butanol, difficult to dissolve into ethyl acetate, acetone, benzene and chloroform. Chemical reaction of functional group of Kaidimycin showed that it had glycoside, amino acid and aldehyde, no reducing sugar, polypeptide and phenol.

凯地菌素属中等极性的、中性抗生素,极性纸层析结果与多烯类抗生素的纸层析结果相似:易溶于水、吡啶,微溶于甲醇、乙醇、正丁醇,不溶于乙酸乙酯、丙酮、苯、三氯化碳;对高温、光照和紫外处理有很好的稳定性;官能团反应试验结果发现,凯地菌素可能含有糖苷键、氨基酸伯氨基和醛基,不含有还原糖、多肽和酚基,高锰酸钾、浓硫酸反应与多烯大环内酯类抗生素的特性相似;并且依据纯品,采用生物法和分光光度法对摇床发酵液进行了效价的测定。

Lu Po new energy group premium coal, a metallurgical coke, raw benzene, tar quality chemical products anthracene oil, naphtha, wash oil, industrial naphthalene, in the warm asphalt, etc.

潞宝新能源集团的特级精煤、一级冶金焦、粗苯、优质焦油化工产品(蒽油、轻油、洗油、工业萘、中温沥青等)、优质甲醇等十几种产品畅销全国;冶金焦成功进入美国市场,中温沥青出口印度。

IV . Content and Capacity: 2,400,000t/a stamping coke, 30,0000 t/a coal tar, 10,0000 t/a methanol, 10,0000 t/a phenol anhydride, 5,0000 t/a Needle coke, 10,0000 t/a Hydrogenation of anthracene oil, 10,0000 t/a Hydrogenation of Crude benzene, 2,0000t/a β-naphthol, 1,0000t/a 2-hydroxy-3-naphthaoic acid , 2,0000t/a UHP ultra-high power electrode.

四、项目建设内容及规模:240万吨/年捣固焦炉及化产回收、30万吨/年焦油、10万吨/年甲醇、10万吨/年苯酐、5万吨/年针状焦、10万吨/年蒽油加氢、10万吨/年粗笨加氢、2万吨/年二萘酚、1万吨/年2.3酸、2万吨/年 UHP 超高功率电极。

The biogenic amines in test samples were extracted by 10% trichloroacetic acid and then derived with benzoyl chloride. The HPLC analysis for the samples were conducted as the following condition: mobile phase was a gradient elution program of methanol and water, the flow rate was 0.8 mL/min.

用10%的三氯乙酸提取样品中的生物胺,采用苯甲酰氯衍生处理后,以甲醇/水为流动相,进行梯度洗脱,流速0.8 mL/min,紫外检测器波长为254 nm。

Seven biogenic amines were extracted from a sample with 6% perchloric acid, then derivatized with benzoyl chloride. 0.02 mol/L borate buffer (pH 9.2) containing 0.06 mol/L sodium deoxycholate-methanol (95∶5, v/v)was used as a running buffer. The detection wavelength was set at 214 nm. The separation was achieved within 12 min. Good linearities were observed from the calibration plots in the concentration ranges.

样品经6%过氯酸萃取后,由苯甲酰氯衍生化,以含0.06 mol/L脱氧胆酸钠的0.02 mol/L硼酸(pH 9.2)-甲醇(体积比为95∶5)混合液为电泳介质,电泳电压25 kV,温度25 ℃,检测波长214 nm,在12 min内实现了7种生物胺的完全分离。7种生物胺的浓度与其峰面积在一定的范围呈良好的线性关系,检出限除组胺为15 μg/g外,其余均为5 μg/g。

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