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苯甲醇

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A sample-pretreated method of ether-extraction-precolumn-derivation was established, and the chromatographic conditions, which was used for determinating the derivant of extracted UDCA, were decided to be Hypersil C_(18) column(250×4.6mm, 10μm), acetonitrile-methol-0.005mol·L~(-1) phosphoric buffer-triethylamine(50:27:42:0.25, adjusted to pH3.0±0.1 by phosphoric acid) as mobile phase with detective UV wavelength at 247nm and column temperature at 35℃.

建立了乙醚提取-柱前衍生化血浆样品预处理方法,采用Hypersil C_(18)柱(250×4.6mm,10μm),乙腈-甲醇-0.005mol·L~(-1)NaH_2PO_4缓冲液-三乙胺(50:27:42:0.25,磷酸调节pH3.0±0.1)为流动相的HPLC法,以溴苯乙酮为衍生化试剂,在247nm处测定家兔血浆中熊去氧胆酸衍生化产物。

When 45% methanol solution containing 0.5 mmol/L hexamethylene tetraamine was used as the pump carrier, the pump flow rate and output pressure achieved 0.58 mL/min and 0.79 MPa at 4950 V, respectively. By using the pump carrier as the mobile phase, benzene and naphthanlene were separated on baseline by the EFA system.

在4950 V的外加电压下,以含0.5 mmol/L六亚甲基四胺的45%甲醇溶液为泵载流,电渗泵的流量和输出压强分别为0.58 mL/min和0.79 MPa,以泵载流为流动相,该系统对苯和萘进行了反相色谱分离。

Preliminary experiment for organic waste water treatment illustrated that the COD removal efficiency for methanol,toluene and metanilic acid was 91.3%,89.28% and 84.53%,respectively.

在初步处理有机废水的实验中,甲醇、甲苯、间氨基苯磺酸COD的去除率分别达到91.3%、89.28%和84.53%。

Reactor Construction: Multitube reactor systems for chemical industry ( all technical heat transfer fluids,particularly mkoltensalt 50 years experience) for production of:phthalic anhydride,maleic anhydride,acrolein,methyl methacrylate,methanol,ethylene oxide and other endothermic and exothermic catalytic gasphase processes.

反应器制造部:列管反应器系统,用于化学工业(所有工业用热交换流体,特别是熔盐传热)中生产苯酐,顺酐,丙烯醛,丙烯酸,甲基丙烯酸甲酯,甲醇,环氧乙烷及其他放热与吸热气相催化生产工艺。

Reactor Construction: Multitube reactor systems for chemical industry ( all technical heat transfer fluids,particularly mkoltensalt 50 years experience) for production of:phthalic anhydride,maleic anhydride,acrolein,methyl methacrylate,methanol,ethylene oxide and other endothermic and exothermic catalytic

简介: 反应器制造部:列管反应器系统,用于化学工业(所有工业用热交换流体,特别是熔盐传热)中生产苯酐,顺酐,丙烯醛,丙烯酸,甲基丙烯酸甲酯,甲醇,环氧乙烷及其他放热与吸热气相催化生产工艺。

We have investigated on the chemical constituents of Nepeta partite collected from Gansu Zhuanglang, and twenty eight compounds were isolated from the methanol extraction of this species by chromatography techniques. Twenty five compounds were identified by means of chemical and spectra methods IR, FABMS, EI-MS,〓, DEPT, and 2D NMR), among which four compounds were new as isopimar-15-en-3β, 8β, 20-triol; phenylethanal-3-O-(2'-glycerin)-5-O-β-D-glucopyranoside; 3-O-linolenoylglyceryl-6'-O-(α-D-galactopyranosyl)-β-D-galactopyranoside; ethyl rosemarinate.

我们对采自甘肃庄浪的康藏荆芥进行了化学成分的研究,利用层析手段从该植物的甲醇浸膏中分离出二十八个化合物,经化学方法和波谱技术(红外,质谱,一维和二维核磁共振谱)鉴定了二十五个化合物的结构,其中四个为新的化合物,它们分别是:异海松-15-烯-3β,8β,20-三醇;苯乙醇-3-O-(2'-甘油基)-5-O-β-D-吡喃葡萄糖甙;3-O-亚麻酰基甘油-6'-0--β-D-吡喃半乳糖甙;迷迭香酸乙酯。

MPH plastic magnetic pump complies with JB/T7742-1995Standard for Small Magnetic Transmission Centrifugal Pump. Its flow-through parts adopt PPS with corrosion resistance to most acid, alkali and salt (except oxidable acid like strong sul-furic acid, nitric acid and aqua regia). Its performance is close to the chemical performance of F4, which can resist to most organic solvents under 100℃, especially to the mixture of gas and carbinol. Thus it is an ideal pump for acid and alkali industries.

MPH型塑料磁力泵符合JB/T 7742-1995《小型磁力传动离心泵》标准,过流部件采用聚苯硫醚,不受大多数酸、碱、盐的侵蚀(除氧化性酸如浓硫酸、硝酸和王水等),其性能接近于聚四氟乙烯的化学性能,在100℃以下能耐大多数有机溶剂,特别能耐汽油和甲醇的混和液,是酸碱工业中的理想用泵。

Several types of ligand reactions observed under hydrothermal condition were summed up:(1) hydrolysis of pyridine nitrile, aldehyde and ester in mixed water and alcohol into pyridine-carboxylate;(2) replacement of carboxylate group with sulfonic group;(3) coupling of phenanthroline by dehydrogen;(4) oxidative coupling of methanol into oxalic acid;(5) hydroxylation of isophthalate.

总结了以往在水热条件下观察到的几类配体反应:(1)吡啶腈、醛和酯在醇和水混合溶液中水解成吡啶羧酸;(2)磺基取代羧基反应;(3)邻菲啰啉的脱氢的聚合:(4)甲醇被氧化偶合生成草酸:(5)间苯二甲酸的羟基化反应。

Waste oil category: Waste oil, waste hydraulic oil, waste oil, waste oil injection, waste kerosene, waste of white mineral oil, white waste oil, waste oil sparks, the repeal of toluene, waste cutting oil, gear oil, lubricants, batteries oil, spindle oil, zorra, oil, turpentine oil, solvent oil, gear oil, oil rails; waste chemical categories: one, the repeal of toluene, xylene waste, spent 2 pure benzene, acetone waste, waste Ding ketone, cyclohexanone 3 waste, waste dichloromethane, dichloroethane waste, waste Dichloropropane 4, solvent categories: soluble oil 6 #, 120 # dissolving agents, dissolving agents 200 # 5, trichloro ethylene, dichloromethane, trichloroethane; tetrachlorethylene, trichloromethane 6, the repeal of methanol, ethanol, waste, waste alcohol, isopropyl alcohol waste 7, the repeal of ethylene glycol, diethylene glycol waste, spent three 8 glycol, waste butyl acetate, ethyl acetate wastewater, waste acetate 9, the repeal of ethyl ether, acetonitrile waste, waste petroleum ether 10, cleaning categories: cleaning agent, washing machine water, days that water; wash board water,×oil wastewater liquid 11, the supply of tires category: special supply of fuel oil, non-standard oil, burner oil, waste oil and other refined crude oil.

废油类:废机油,废液压油,废柴油,废注塑机油,废煤油,废白矿油,废白电油,废火花机油,废甲苯,废切削油,齿轮油,润滑油,废电池机油,锭子油,索拉油,松节油,溶剂油,齿轮油,导轨油等;废化工类:1、废甲苯、废二甲苯、废纯苯2、废丙酮、废丁酮、废环已酮3、废二氯甲烷、废二氯乙烷、废二氯丙烷4、溶剂类: 6#溶油剂, 120#溶油剂, 200#溶油剂5、三氯乙烯,二氯甲烷,三氯乙烷;四氯乙烯,三氯甲烷6、废甲醇、废乙醇、废丁醇、废异丙醇7、废乙二醇、废二甘醇、废三甘醇8、废醋酸丁酯、废醋酸乙酯、废醋酸甲酯9、废乙醚、废乙腈、废石油醚10、清洗类:清洗剂,洗机水,天那水;洗板水,去渍油等废液废水11、废轮胎类供应:特价供应燃料油,非标油,烧火油,废油提练的原油等。

Unoxidated and oxidized wheat stalks were extracted sequentially with CS2, benzene, methanol, acetone and THF, and the extraction solutions were analyzed with GC/MS. The relative contents and compositions of fractional extracts of un-oxidized and oxidized wheat stalks were compared.

采用二硫化碳、苯、甲醇、丙酮和四氢呋喃对未氧化和氧化的麦秆进行分级萃取,比较麦秆各级萃取物的相对含量和组成差异,并对各级萃取物的组成进行GC/MS分析。

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