苯甲醇

A novel method for the synthesis of α-bromo acetophenone s by the reaction of 1,3-dibromo- 5,5-dimethylhydantoin with p-toluenesulfonic acid in methanol at 20～60 ℃ was described.

报道了使用1，3-二溴-5，5-二甲基海因和对甲苯磺酸在甲醇中和20～60℃的温和条件下合成α-溴代苯乙酮的新方法。

An aliquot of the reaction mixture was injected into a C18-column with a mobile phase consisting of 0.05 molL^(-1) phosphate buffer (pH 5.5)-methanol (65:35, V/V) and detected at 235 nm.

土壤样品用0.6 molL^(-1) KOH提取，经对甲基苯磺酰氯衍生化后，注入C18柱中分离，用紫外检测器在235 nm波长检测，流动相组成为0.05 molL^(-1)磷酸盐缓冲液(pH 5.5)：甲醇＝65：35。

Results: Using of handy infrared gas spectrometer, the ammonia, sulphur dioxide, acetone, butanone, ethyl acetate, chloroform, benzene, toluene, methyl alcohol, ethyl alcohol, isopropanol, and other harmful gases can be carried out quickly Online Testing. The arsine, hydrogen chloride, hydrogen cyanide, hydrogen sulfide can not be detected online.

结果：可利用便携式红外气体分析仪对氨、二氧化硫、丙酮、丁酮、乙酸乙酯、氯仿、苯、甲苯、甲醇、乙醇、异丙醇等有害气体可进行快速的在线检测，不能对砷化氢、氯化氢、氰化氢、硫化氢进行快速在线检测。

Carbinol, ethylene, propylene, and benzene are called one of four basic organic chemical raw materials.

甲醇、乙烯、丙烯和苯被称为四大基本有机化工原料之一。

The paper presents that 7-chloro-4-nitrobenz-2-oxa-1,3-diazole and isoniazide can produce an orange condensation product in carbinol medium and a new determination way of isoniazide is found based on it.

研究了异烟肼与7氯 4 硝基苯并 2 氧，3 二氮唑在甲醇介质中生成橙色缩合产物的最佳条件，并由此建立了一种间接分光光度法测量药物中异烟肼的新方法。

Then, N-for-aspartame was obtained from the reaction of 3-formyl-4-carboxymethyl-1,3-oxazolidine-5-one and L-phenylalanine methylester hydrochloric acid under sodium acetate anhydrous in ethyl acetate, and the target product was prepared after removing formyl in the mixture system of hydrochloric acid, methanol and water, the yield of aspartame reaches 89.2%.

最后，用3-甲酰-4-羰基口恶唑烷-5-酮乙酸与L-苯丙氨酸甲酯盐酸盐在溶剂中进行接肽反应，然后在甲醇/盐酸混合体系中进行脱甲酰保护基，从而得到最终目标产物，产率为89.2%。

A preferred form of the invention is a process comprising adding to a quantity of sodium which is covered with a hydrocarbon solvent boiling above 100°C., at least a chemically equivalent proportion of methyl, ethyl or a propyl alcohol, subsequently adding an approximately equivalent proportion of a dialkyl carbonate and of an alkyl phenylacetate, the alkyl groups in these two last-mentioned compounds being preferably the same as the alkyl radical of the above-mentioned lower aliphatic alcohol, heating the mixture to induce reaction and continually distilling out the alcohol formed from the reaction zone.

本发明的理想形式包括下面的工艺过程：把至少处于化学平衡的甲醇，乙醇或丙醇添加到覆盖着沸点超过一百摄氏度的碳氢化合物溶剂中，接着加入大约相同当量的二烷基碳酸酯和烷基乙酸苯酯，在刚才提到的化合物中，其烷基集团最好是和刚才提到的低级别脂肪族醇相同，然后加热反应混合物从而引导反应的进行，在反应区域通过连续蒸馏移除形成的醇类。

Process for the manufacture of a dialkylphenylethylmalonatewhich comprises adding to a quantity of sodium which is covered with a hydrocarbon solvent boiling above 100°C, at least a chemically equivalent proportion of methyl, ethyl or a propyl alcohol, subsequently adding an approximately equivalent proportion of a dialkylcarbonate and of an alkyl phenylacetate, the alkyl groups in these two last-mentioned compounds being preferably the same as the alkyl radical of the above –mentioned lower aliphatic alcohol, heating the mixture to induce reaction and continually distilling out the alcohol formed from the reaction zone and finally causing the sodio diethyl phenylmalonate so formed to interact with an ethylating agent.

生产二烷基苯基丙二酸酯的工艺过程：这包括这包括把至少处于化学平衡的甲醇，乙醇或丙醇添加到覆盖着沸点超过一百摄氏度的碳氢化合物溶剂中，接着加入大约相同当量的二烷基碳酸酯和烷基乙酸苯酯，在刚才提到的化合物中，其烷基集团最好是和刚才提到的低级别脂肪族醇相同，然后加热反应混合物从而引导反应的进行，在反应区域通过连续蒸馏移除形成的醇类。最后使所形成的钠代二乙基苯基丙二酸酯和乙基化试剂反应。

The engine ran on a special mixture of methyl alcohol (63%), benzene (16%), ethanol (12%), acetone (4.4%), nitrobenzene (2.2%), avgas (2%), and ether (0.4%) with MW (methanol-water) injection for charge cooling and as an anti-detonant.

特别混合物燃料为引擎运转提供动力，甲醇(63%)，苯(16%)，对氨基苯甲酸二(12%)，丙酮(4.4%)，硝基苯(2.2%)，飞机用燃料(2%)和乙醚(0.4%)，以100W充电冷却射入并作为抗爆剂。

The major occupational hazards factors in printing ink were benzene, toluene, xylene, ethylbenzene, solvent gasoline, methanol, alcohol, isopropyl alcohol, ethyl acetate, butyl acetate, butyl acetate, dichloromethane, etc. 10 of 1224 samples (0.82%) exceeded the national occupational health standards.

印刷油墨中存在的职业病危害因素种类主要有苯、甲苯、二甲苯、乙苯、溶剂汽油、甲醇、乙醇、异丙醇、乙酸乙酯、乙酸丁酯、二氯甲烷等，检测样品总数1224件，超标样品数10件，超标率为0.82%。

My first article for Screen Power Magazine, which is to this day is the official magazine of Jackie Chan, was a DVD review of the Hong Kong actioner Gen-X Cops, starring Nicholas Tse and Daniel Wu.

我的第一篇文章为屏幕力量杂志，在对这天是Jackie Chan 正式杂志，是香港actioner Gen X 警察的DVD 回顾，担任主角Nicholas Tse 和丹尼尔吴。

His lips grazed hirs, Now what are you going to do?

他的唇使吃草了 hirs，现在你将要做什麼？