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It was reported that benzylidenemalononitrile did not react with 1-benzyl-1,4-dihydronicotinamide. However, similar reaction easily takes place under the same condition when the phenyl group is replaced by the pyridyl group.

本课题组之前报道了苯亚甲基丙二腈在室温下不能被BNAH所还原,本论文将反应底物中的苯基换成吡啶基之后,在同样的实验条件下,反应可以比较顺利的进行。

In this paper,pyromellitic dianhydride,1,2,3,4-cyclobutanetetracarboxylic dianhydride,4[(4-aminophenyl)-bis(4-methoxyphenyl)methyl]benzeneamine,4-hexyloxy-biphenyl-3′,5′-diaminobenzoate,and additive ADD-34 were used to synthesize four PIs.

文章用均苯四甲酸二酐,4[(4-氨基苯基)-二(4-甲氧基苯基)甲基]苯胺,1,2,3,4-环丁烷四羧酸二酐,4-己烷氧基联苯酚-3′,5′-二胺基苯甲酸酯和不同含量的添加剂制备了聚酰亚胺液晶取向剂。

The solid-liquid reaction method was used for the preparation of HPLC aryl-bonded silica gel stationary phases, including 3, 5-dinitrobenzyl, quinolinyl ether and 1, 1'-di(2-naphthol) ether bonded silica gel stationary phases by using N-(β-aminoethy1)-γ-aminopropylmethyldimethoxy silane and 3-glyci-doxypropyl trimethoxylsilane as coupling reagents, respectively.

采用固液相连续反应,以N--γ-氨丙基甲基二甲氧基硅烷和γ-丙基三甲氧基硅烷为偶联剂,分别制备了二硝基苯甲酰胺基、喹啉醚基和联萘酚醚基三种芳基键合硅胶固定相。

A new fullerene derivative containing energy-producing groups was prepared, and the reaction conditions affecting the yield were studied by the kroenecker method. The optimal reaction conditions with a 53.5% yield (based on consumed C60) are: 1:3:6 of molar ratio of C60 , o–nitrobenzaldehyde and sarcosine , 55℃ of reaction temperature, 12 h of reaction time, 40mL of toluene solvent.

利用N-甲基甘氨酸、邻-硝基苯甲醛和C60反应,合成分离出了含有硝基的新型富勒烯吡咯烷衍生物,通过正交试验对其工艺条件进行了研究,探讨了反应物剂量比、温度、时间和溶剂体积对产物产率的影响,得到了合成产物的最佳工艺条件:反应物剂量比为1:3:6、温度为55℃、反应时间为12h、溶剂甲苯体积为40mL,此时产物产率可达到53.5%(以消耗的C60计)。

In the invention, normal reversible absorbing transfer material for solar energy which are mixture of cobalt chloride and sextic methyl tetramine, phthalandione lipid compound and trilateral methane lactone compound, said material are produced to micro cachet that colour changes as stemp, changing reversely in normal temp, then said micro cachet are compounded with common white silicate cement to produce the invention cement base material.

本发明采用对太阳能呈常温可逆吸收转换材料:氯化钴与六次甲基四胺混合物、邻苯二甲酸酯类化合物和三芳甲烷内酯类化合物,将上述材料制成微胶囊,再将所制出的常温可逆温致变色微胶囊与普通白色硅酸盐水泥复合,即可制备出常温可逆温致变色水泥基材料。

The cis-decalin 79 was obtained from 2-methoxy-4-methylphenol (77) via a sequence of reactions involving intermolecular Diels-Alder reaction of masked o-benzoquinone derived from 77 and ethyl vinyl ketone, silyl enol ether formation and Cope rearrangement.

第一部份:以2-甲氧基-4-甲基酚(77)为起始物,经由二乙醯基亚碘苯氧化、分子间Diels-Alder反应、烯醇矽醚的形成及Cope重排反应得到具有十氢萘骨架化合物79。

The result showed that the thermal decomposition temperature of chlorinated paraffin reached 133℃ by adding 0.3% composite stabilizer in which the weight percentages of ethylene glycol diglycidyl ether, methyl stannic, triphenyl phosphate, exoxidized soybean oil were 72%, 3%, 10%, 15%, respectively. It is 15℃ more than that of using pure ethylene glycol diglycidyl ether.

结果表明:当复合稳定剂中乙二醇二缩水甘油醚、甲基锡、亚磷酸三苯酯、环氧大豆油的质量分数分别为72%,3%,10%,15%,复合稳定剂的添加量为氯化石蜡的0.3%时,氯化石蜡的热分解温度为133℃,比单独使用乙二醇二缩水甘油醚提高了15℃,热稳定效果较好。

The composite stabilizer of chlorinated paraffin was made from ethylene glycol diglycidyl ether, methyl stannic, triphenyl phosphate, exoxidized soybean oil. The influences of components in the composite stabilizer for thermal stability of chlorinated paraffin were investigated.

以乙二醇二缩水甘油醚和甲基锡为主稳定剂、亚磷酸三苯酯和环氧大豆油为助稳定剂制备了氯化石蜡复合稳定剂,研究了各组分配比对氯化石蜡热稳定性的影响。

Our company specializes in operating plating materials: sulfamic acid nickel, nickel sulphate, nickel chloride, nickel carbonate, etc.; environmentally friendly sewage treatment materials: polyacrylamide, polypropylene acid sodium, ferrous sulfate, etc.; washing cleaning materials: OP - 10, TX-10, NP-9, K-12, JFC, sodium carboxymethyl cellulose, etc.; cosmetic raw materials: Triclosan, Resorcinol, stearic acid and so on, basic chemical raw materials: Industrial salt, soda ash industrial ammonium chloride, ammonium chloride agriculture, Sodium Sulfate, Sodium Molybdate, Ammonium Molybdate, as well as chemical products such as UV-absorbers.

本公司专业经营电镀原料:氨基磺酸镍,硫酸镍,氯化镍,碳酸镍等;环保污水处理原料:聚丙烯酰胺,聚丙烯酰钠,硫酸亚铁等;洗涤清洗原料:OP-10,TX-10,NP-9,K-12,JFC,羧甲基纤维素钠等;化妆品原料:三氯生,间苯二酚,硬脂酸等,基础化工原料:工业盐,纯碱,工业氯化铵,农业氯化铵,元明粉,钼酸钠,钼酸铵等以及紫外线吸收剂等化工产品。

Using Maleic anhydride and 1-Octadecanol as raw material, synthesize octadecanol maleic monoester.The influence of p-toluence sulphonic acid were investigated.

以马来酸酐和十八醇为原料合成了马来酸单十八酯,研究了催化剂对甲基苯磺酸的加量产物的影响。

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Now, however, all children continue in "comprehensive" schools, and the eleven-plus determines which courses of study the child will follow.

然而现在,所有的孩子都要在综合学校继续学习,所以这次考试只是决定他们将要学习哪些课程。

Cultivatable land , and led to a general recognition that development must not be carried at the cost of agriculture .

城区的迅速扩大在很多情况下侵占了宝贵的可耕地,使人们普遍认识到发展不能以牺牲农业为代价。

Detailed Intrinsic Reaction Coordination calculations were carried out to guarantee the optimized transition-state structures being connected to the related tautomers.

同时,做了详尽的内禀反应坐标计算,以保证所得到的过渡态连接相应的始末异构体。