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With the same content of templates,the pore diameter of the generated material withglycerol as template is bigger than the one with pentaerythrite. The photocatalytic degradationof phenol,methyl orange and dodecylbenzene—sulfonate are studied.

利用所制得的中孔纳米二氧化钛粉体应用于甲基橙、苯酚和十二烷基苯磺酸钠的模拟废水溶液的处理中,探讨了二氧化钛的降解特性和光催化效率的影响因素。

One of these compounds, 2-diethyl- aminoethyl-5--(4-methoxybenzylidene) cyclo- pentanone hydrochloride (T81) possessed sig- nificant antiinflammatory and analgesic ac- tivity when administered orally.

Ⅲ类化合物完全无抗癌活性,对其中一个化合物2-二乙胺乙基-5--(4-甲氧基苯亚甲基)环戊酮盐酸盐(T81)试验结果表明,它经口给药时具有显著的抗炎、镇痛活性。

Synthesis of Organic Pigmet Intermidiate N, N'- bisacetylaceto - 2 - methyl - 5 - chloro -1,4- Phenylenediamine

有机颜料中间体N,N′-双乙酰乙酰基2-甲基-5-氯代-1,4-苯二胺的合成

Collisional induced dissociation technique is applied to characterize cucurbituril supramolecule structures complexed with 1,4-diaminobutane, phenylenediamine and lysine.

运用碰撞激发解析技术确定了葫芦脲[6]与1,4-丁二胺,二甲基苯以及赖氨酸分子形成轮轴结构的超分子复合物,即线性分子穿入葫芦脲[6]的空腔内形成的稳定超分子复合物。

Herein, a series of compounds, BP-C〓-NBD (n=2, 3, 4, 5, 6, 8, 10), was synthesized. Nanosecond flash photolysis, phosphorescence emission and lifetime, as well as photoisomerization reaction of norbornadiene were used to understand the intramolecular triplet energy transfer in detail.

我们设计、合成了以多亚甲基连接的二苯酮与降冰片二烯(BP-C〓-NBD,n=2,3,4,5,6,8,10)系列化合物,利用纳秒时间分辨技术、低温磷光发射、磷光寿命以及光敏异构化的方法,对其分子内三重态能量传递过程进行了详细地研究。

The effect of components including tetracholrophthalic acid, phthalazine and antifoggant with tribromomethyl sulfone groups on photographic properties of FTG materials was investigated in different pH, using polyvinyl alcohol as a hydrophilic binder, in situ formed AgBr as light sensitive component.

本文以水性聚乙烯醇为粘合剂,原位法合成的AgBr作为光敏元,考察了组分四氯邻苯二甲酸、酞嗪以及三溴甲基砜类防灰雾剂在体系不同pH值时对PTG材料感光性能的影响。

The invention is characterized in that phthalide of general formula, wherein n and X have the meaning cited in the description, is reacted with nitrogen heterocycles of general formula: H-Z, wherein Z has the meaning cited in the description, or with nitrogen heterocycle metal salts of general formula in the presence of an aprotic polar diluent and optionally in the presence of a basic auxiliary reaction agent.

本发明涉及制备通式的2-杂环基甲基苯甲酸衍生物的新的方法,其中n、X和Z具有说明书中给出的意义,该方法提供高收率和高纯度,其特征是,通式的2-苯并呋喃酮,其中n和x具有说明书中给出的含义,与通式的氮杂环:H-Z,其中Z具有说明书中给出的意义,或与通式的氮杂环的金属盐在质子惰性极性稀释剂中并任选在碱性反应助剂存在下反应。

A synthetic method for N-(5-nitro-6-chloro-3-pyridine methyl) phthalimide is studied.

研究了N-(5-硝基-6-氯-3-吡啶甲基)邻苯二甲酰亚胺的合成方法。

Then, N-(5-nitro-6-chloro-3-pyridinemethyl) phthalimide is obtained after the nitrating reaction of N-(6-chloro-3-pyridine methyl) phthalimide. The yield of the obtained product is 90.5%, and its melting point is 143.1~143.8℃.

缩合产物再经过硝化,合成N-(5-硝基-6-氯-3-吡啶甲基)邻苯二甲酰亚胺,其熔点为143.1~143.8℃,收率为90.5%。

The synthetic route starts from penicillin G, peroxyacetic acid(8.5%) as Oxidizing Agent to get penicillin G sulfoxide; esterifided with p-nitrobenzyl bromine to synthesize penicillin G sulfoxide ester; we synthesize 3-exomethylenecepham sulfoxide ester with phthalimide potassium and 4A molecular sieve as acid scavenger to open the ring, SnCl_4 as catalyzation to close the ring. The yield is over 60%.

本研究采用的合成路线为:以青霉素G钾盐为原料,选用工业过氧化氢制备的过氧乙酸(22.3%)稀释至8.5%为氧化剂,氧化得青霉素亚砜;采用对硝基溴苄为酯化试剂,制备青霉素亚砜酯;以NCP(N-氯代邻苯二甲酰亚胺)为开环试剂,酞酰亚胺钾和4A型分子筛为酸清除剂,顺利开环;再经无水SnCl_4催化闭环得3-环外亚甲基头孢亚砜酯,最终产率在60%以上。

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Now, however, all children continue in "comprehensive" schools, and the eleven-plus determines which courses of study the child will follow.

然而现在,所有的孩子都要在综合学校继续学习,所以这次考试只是决定他们将要学习哪些课程。

Cultivatable land , and led to a general recognition that development must not be carried at the cost of agriculture .

城区的迅速扩大在很多情况下侵占了宝贵的可耕地,使人们普遍认识到发展不能以牺牲农业为代价。

Detailed Intrinsic Reaction Coordination calculations were carried out to guarantee the optimized transition-state structures being connected to the related tautomers.

同时,做了详尽的内禀反应坐标计算,以保证所得到的过渡态连接相应的始末异构体。