苯甲基

A novel planar chiral diferrocenylimine-diols 6 was synthesized by the condensation of R, S(subscript p-1-(2-diphenyl hydroxyl methyl) ferrocenylethylamine [R, S(subscript p-4] with phthaldehyde in anhydrous ethanol, and was crystallographically characterized.

通过R，S(下标 p-1-（2-二苯基羟甲基）二茂铁乙胺[R，S(下标 p-4]和对苯二甲醛在无水乙醇中的缩合反应合成了一种新型平面手性双二茂铁亚胺二醇化合物6，并经X-射线衍射分析它的晶体结构。

The photocycloaddition of 1-naphthonitrile (1-NpCN) and 2,3-dimethyl-2-butene in cyclohexane or benzene gave cyclobutane 3 primarily,but that of 2-NpCN gave azetine 6 asthe major and cyclobutane 5 as the minor product in low conversion photolysis.

在低转化光解情况下，1-萘甲腈(1-NpCN)和2，3-二甲基丁烯-2在环已烷或苯中的光环加成反应主要得到环丁烷3，但2-NpCN主要得到氮杂环丁烯6和少量的环丁烷5，三氟醋酸量增加抑制1-NpCN和DMB的光环加成反应，表明TFA与基态及单激发态1-NpCN生成非光反应的复合物，它也淬灭(1-NpCN-DMB)激基复合物。

The photocycloaddn. of 1-naphthonitrile (1-NpCN) and 2,3-dimethyl-2-butene in cyclohexane or benzene gave cyclobutane I primarily, but that of 2-NpCN gave azetine II as the major and cyclobutane III as the minor product in low conversion photolysis. The photocycloaddn. of 1-NpCN with DMB is retarded by increasing amts. of trifluoroacetic acid which is shown to form non-photoreactive complexes with ground state as well as with singlet excited state 1-NpCN. It also quenches the *(1-NpCN-DMB) exciplex.

在低转光解情况下，1-萘甲腈(1-NpCN)和2，3-二甲基丁烯-2在环已烷或苯中的光环加成反应主要得到环丁烷3，但2-NpCN主要得到氨杂环丁烯6和少量的环丁烷5，三氟醋酸量增加抑制1-NpCN和DMB的光环加成反应，表明TFA与基态及单激发态1-NpCN生成非光反应的复合物，它也淬灭^*(1-NpCN-DMB)激基复合物。

Sixteen target compounds were designed and synthesized, basing on 2--(4-hydroxy-3-methoxybenzylidene)cyclopentanone as the lead compound, all of which are innovative and have not been reported yet.

本文以2--(3-甲氧基-4-羟基苯亚甲基)环戊酮为先导化合物，设计并合成了16个目标化合物，均为未见文献报道的新化合物。

It is apt to produce the crystalline component at the low temperature to remove in the raw materials of lubricating oil, mainly point the paraffin wax, dewax and adopt the cold crystallization law, stay in order to overcome glueing

是除去润滑油原料中易在低温下产生结晶的组分，主要指石蜡，脱蜡采用冷结晶法，为克服低温下粘度过大，石蜡结晶太小不便过滤，常加入对蜡无溶解作用的混合溶剂，如甲苯-甲基乙基酮，故脱蜡常称为酮苯脱蜡。

Double chain naphthyurea/thiourea piperazine derivatives complex with linear dicarboxylate anions with a high stability constant and 1∶1 stoichiometry of the complex-and the complex was formed through six hydrogen bonds.2 Photophysical behaviors and anion binding of three N,N-dimethylaminochalcone derivatives were studied.

二研究了三种N，N-二甲基氨基查耳酮衍生物的光物理行为及与阴离子的结合能力。4'位不同的取代基-氨基和苯脲基对查耳酮的的分子内电荷转移能力有一定的影响，它们减弱了查耳酮衍生物的分子内电荷转移能力，导致发射光谱蓝移。

The ultraviolet photosensitive initiating system is composed of 4,4"-bis(N,N"-dimethylamino) benzophenone, 2-chlorohexaarylbiimidazole and a hydrogen donor coinitiator n-dodecyl mercaptan.

用光敏剂4，4′-二(N，N′-二甲基-氨基)苯甲酮、引发剂邻氯代六芳基双咪唑和氢给体助引发剂十二烷基硫醇组成光敏引发体系。

Leuco crystal violet lactone was prepared by heating the mixture of dimethylaniline, p- dimethylaminobenzaldehyde and m- dimethylaminobenzoic acid at 60 ℃ for 5 hours in presence of hydrochioric acid and unea and in the nitrogen atmosphere with 72% yield of LCVL.

等摩尔比的N，N-二甲基苯胺和对二甲氨基苯甲醛在盐酸和脲的存在及氮气保护下，80℃反应0.5h，加入间二甲氨基苯甲酸于90℃反应5h。将反应混合物中和，抽滤，得到无色结晶紫内酯，产率为72%。

Leuco crystal violet lactone was prepared by heating the mixture of dimethylaniline, p-dimethylaminobenzaldehyde and m-dimethylaminobenzoic acid at 60℃ for 5 hours in presence of hydrochloric acid and urea and in the nitrogen atmosphere with 72%yield of LCVL.

等摩尔比的N，N-二甲基苯胺和对二甲氨基苯甲醛在盐酸和脲的存在及氮气保护下，80℃反应0.5h，加入间二甲氨基苯甲酸于90℃反应5h。将反应混合物中和，抽滤，得到无色结晶紫内酯，产率为72%。

The polyetherurethane was synthesized by one-step method for cosmetic applications by coupling poly(PTMG,Mn=2000) and poly(PEO,Mn=2000) with 4,4'-diphenylmethane diisocyanate.

聚醚型聚氨酯用于化妆品中，由聚四亚甲基醚二醇和聚环氧乙烷与4，4-二苯甲烷二异氰酸酯采用一步法合成，结果表明PEU暴露在60℃酒精/水(80/20，体积比)溶液中放置4周后发生降解，PEU发生变质，其相对分子质量、粘度和机械性能都发生改变。

Now, however, all children continue in "comprehensive" schools, and the eleven-plus determines which courses of study the child will follow.

然而现在，所有的孩子都要在综合学校继续学习，所以这次考试只是决定他们将要学习哪些课程。

Cultivatable land , and led to a general recognition that development must not be carried at the cost of agriculture .

城区的迅速扩大在很多情况下侵占了宝贵的可耕地，使人们普遍认识到发展不能以牺牲农业为代价。