苯甲基

In this paper, the effects of processing and heat treatment of terephthalate/polyte-traoxymethylene block copolymer on their dynamic mechanical temperature spectra were studied.

本文首先研究了成型方法和热处理对聚对苯二甲酸乙二酯与聚氧四亚甲基嵌段共聚物动态力学温度谱的影响，结合应力-应变曲线讨论了微相分离与力学性能的关系。

We also tested the ligands in the asymmetric epoxide ring opening reaction with thiophenol, and as high as 67%ee was gained while using L7. 3. Studies on the reaction of α-hydroxyketone with nitroalkene.

此外我们还初步尝试了将配体应用于催化苯硫酚对环氧的不对称开环反应中，当使用甲基取代H8-BINOL衍生的配体L7时最高取得了67%ee的结果。

Two series of thirty-two aryl arylmercury studies were synthesized by the reaction of arylmercuric chloride with thiophenol or 4-methylthiophenol in ethanol.

芳汞基氯化汞和苯硫酚或对甲基硫酚在乙醇中反应合成了两个系列共32种芳汞基芳基硫化合物，其中22种为新化合物。

According to the H NMRstudy, it was found that the protons on the cyclopentadienyl ring of 〓 were not splitted, but when one proton on the cyclopentadienylring was substituted by methyl, that is in〓 complexes, thefour protons on the ring were splitted into four groups,the 〓 between the onesignal and the others is large, the total splitting is over 2ppm. The splittings werealso affected by the halides linked with the titanium, they increase according to theorder of CI, Br, I. By the study of the 〓 Sn NMR, it is found that the chemicalshifts of 〓 are present in low field. It is assume that the large space strain causesthe angles of the tin linked with ligands deviate from the normal tetrahedral anglesresults low field shift for 〓Sn. And by MS study,there were no molecular ions for 〓 complexes in the spectra. However, for 〓 when X=CI,Br,NCO and Ar is tolyl or phenyl group,there were molecular ions,but theirabundances were very small,and no that for the iodide was found.

钛上的卤素对茂环氢的裂分也有影响，依〓，Br，I顺序，卤素对茂环氢的裂分依次加大；通过对〓的研究发现，以上这些化合物〓的化学位移都出现在低场，认为大的空间张力造成的锡的键角偏离正常的锡的四面体键角是造成〓化学位移出现在低场的原因；对这些化合物质谱的研究发现，〓系列化合物得不到分子离子峰，而〓系列的化合物，当X=〓，NCO和苯环上不带取代基或只带甲基时，则出现分子离子峰，但丰度很低，而相应的碘化物和其它化合物则没出现分子离子峰。

Adopting self-developed glycidyl amine-type high temperature resistant epoxy resin,MTHPA curing agent,toughener,active microsilica fillers and other additives as the basic materials,the high temperature resistant casting material s which have better mechanical strength,electrical insulating properties and capability of crack-resistant were prepared.

采用缩水甘油胺型耐高温环氧树脂、甲基四氢苯酐固化剂为主要原料，加入海岛型结构增韧剂与活性硅微粉填料及其他助剂，制备出具有良好力学、电气性能与耐开裂性能的耐高温环氧树脂浇注料。

Adopting self-developed glycidyl amine-type high temperature resistant epoxy resin ,MTHPA curing agent,toughener,active microsilica fillers and other additives as the basic materials,the high temperature resistant casting materials which have better mechanical strength,electrical insulating properties and capability of crack-resistant were prepared.

采用缩水甘油胺型耐高温环氧树脂、甲基四氢苯酐固化剂为主要原料，加入海岛型结构增韧剂与活性硅微粉填料及其他助剂，制备出具有良好力学、电气性能与耐开裂性能的耐高温环氧树脂浇注料。

Four non-ionic europium complexes,〓-phen(11),〓·bipy(12),〓·dia(13) and 〓(14)(TTA=2-thenoyltrifluoroacetone, DBM=dibenzoylmethane, phen=phenanthroline, bipy=2,2'-bipyridine, dia=4,5- diazafluoren-9-one, dmbp=4,4'-dimethyl-2,2,-bipyridine), were synthesised and the triboluminescent phenomena of 12, 13 and 14 were firstly observed. Structure determinations of 11,12 and 14 were carried out. The triboluminescence maxima of 12 and 13 are similar to those of their photoluminescence. X-Ray structure analyses show that Eu atoms all exhibit eight-coordinate tetragonal antiprismatic geometries and complexes 11, 12 and 14 are all centrosymmetric.

二、合成了四个非离子型的铕的配合物：〓、〓、和〓(14)[HTTA=2-噻吩三氟甲酰丙酮，DBM=二苯甲酰基甲烷，phen=邻菲罗啉， bipy=2，2'-联吡啶，dia=4，5-二氮杂芴-9-酮，dmbp=4，4'-二甲基-2，2'-联吡啶]，首次报道了12、13及14的摩擦发光性质，测定了11、12及14的晶体结构，并系统地讨论了晶体结构和摩擦发光活性之间的关系。12及13的摩擦发光光谱的极大值均类似与其相应的光致发光光谱，表明它们有相同的激发态。

Triphenyl phosphite provided prominent stabilization only when used in combination with other stabilizers. Good results have been obtained for both polyether-urethane and nitrate esters when using 2,6-di-t-butyl-4-methyl-phenol as stabilizer.

亚磷酸三苯酯单独使用时效果较差，但与其它种类的稳定剂混合使用能得到较好的效果。2，6-二叔丁基-4-甲基酚对硝酸酯和聚氨酯粘结剂均具有良好的稳定作用。

The structures and configurations of other components weredetermined too.The results show that the structure of components ofChinese lacquer urushiol are the same as components of Japaneselacquer. In this work,2D-heteronuclear relayed coherence transferspectroscopy plays an important role in determining molecularskeleton carbon linkage.

研究结果表明，中国生漆漆酚中含量最大并起关键作用的两双键共轭的三烯漆酚的结构与构型与日本漆中的该组分完全相同，即都有末端甲基的3—十五碳烯烃（8′Z，11′E，13′Z）邻苯二酚，而没有末端双键的存在，其它几个漆酚主要组分的结构也与日本漆酚对应组分基本相同。

The results showed that there were 8 kinds of aliphatic, 5 kinds of esters, 2 kinds of aldehydes, 2 kinds of nitrogen sulfur heterocyclic rings and one kind of hydrocarbon, alcoholics, ketone, lactones respectively in the analyzed 21 kinds of aroma components, and the content of furfural,β-methyl valeric acid, palmitic acid, nicotine, neohytadiene were higher, next were acetyl ethyl propionate, caleric acid, phenyl ethyl acetate, hydroxylic diethyl succinate.

结果表明，在分析出的21种香气成分中，分别有脂肪酸类8种，酯类5种，醛类2种，氮硫杂环类2种，烃类、醇类、酮类、内酯类各l种，其中相对含量较高的物质成分是糠醛、β-甲基戊酸、十六碳酸、烟碱、新植二烯，其次是乙酰丙酸乙酯、异戊酸、苯乙酸乙酯、羟基丁二酸二乙酯等。

My first article for Screen Power Magazine, which is to this day is the official magazine of Jackie Chan, was a DVD review of the Hong Kong actioner Gen-X Cops, starring Nicholas Tse and Daniel Wu.

我的第一篇文章为屏幕力量杂志，在对这天是Jackie Chan 正式杂志，是香港actioner Gen X 警察的DVD 回顾，担任主角Nicholas Tse 和丹尼尔吴。

His lips grazed hirs, Now what are you going to do?

他的唇使吃草了 hirs，现在你将要做什麼？