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An acrylic resin was synthesized by the radical copolymerization with methyl methacrylate, butyl acrylate and methacrylic acid monomers in solution using benzoperoxide as initiator. Appropriate parameters of monomer ratio, monomer concentration, solvent, and reaction temperature were found by experiment.

以过氧化二苯甲酰为引发剂,采用溶液聚合合成了甲基丙烯酸甲酯-丙烯酸丁酯-甲基丙烯酸树脂,通过实验确定了自由基共聚合适宜的单体配比、单体浓度、引发剂浓度、溶剂以及反应的升温速度。

It is manufactured through kneading, cold pressing and post-treatment; and the materials for the synthetic brake shoe include butadiene-acrylonitrile rubber, phenolic resin, graphite, iron powder, barium sulfate, potash feldspar powder, composite fiber, sulfur, hexamethine tertramine, polymethylene aniline, 2-mercaptan benzothiazole, zinc oxide and toluene.

同时本发明的提供了采用捏合、冷压、后处理工艺来制造新型高摩擦系数合成闸瓦。组成新型高摩擦系数合成闸瓦的各组分重量百分比如下:丁腈橡胶为6.20%,酚醛树脂为10.00%,石墨为15.00%,铁粉为11.03%,硫酸钡为30.00%,钾长石粉为5.00%,复合纤维为20.20%,硫磺为1.00%,六次甲基四胺为1.00%,聚亚甲基聚苯胺0.12%,2-硫醇基苯并噻唑0.15%,氧化锌0.30%,甲苯8.0%。

Di(3,4-dimethyl)benzylidene xylitol as synthesized in the lab from 3,4-dimethyl benzaldehyde and xylitol, and a series of polypropylene samples were prepared based on the amount of the nucleating agent, DMDBX used.

以3,4-二甲基苯甲醛和木糖醇为原料合成1,3-2,4-二(3,4-二甲基)亚苄基木糖醇,将DMDBX作为成核剂使用溶液沉淀法制备DMDBX质量分数分别为0、0.1%、0.3%、0.5%、0.7%、0.9%的聚丙烯样品,采用红外光谱仪、差示扫描量热仪、X射线衍射仪和偏光显微镜等方法,研究了DMDBX对PP结晶结构和结晶性能的影响。

The observation that 2-Alkylidene or Benzylidene cyclopentanones had little anticancer activity and 2-dimethylaminomethylcyclopentanone hydro- chloride (T59) had low anticancer activity proved that the existance of α,β-unsaturated carbonyl group could enhance the anticancer activity of cyclopentanone Mannich bases.

2-亚烷基、苯亚甲基环戊酮无抗癌活性,2-二甲胺甲基环戊酮盐酸盐(T59)抗癌活性较低,这些事实说明Ⅰ类化合物中的环外不饱和双键是一个增效基团,它的存在能明显增强环戊酮Mannich碱的抗癌活性。

The use of chemically-methyl phenol and chloroacetic acid to synthesize methyl-phenoxyacetic acid.

利用化学方法将间甲基苯酚和氯乙酸合成为间甲基苯氧乙酸。

Synthesis of Antidote of N-Dichloroacetyl-2-methyl-1-oxa-4-aza-spiro-4.4-nonane BI Hong-mei, ZHANG Jin-yan, LIANG Ying, SHEN Yong (College of Arts and Sciences Heilongjiang August First Reclamation University, Daqing 163319, Heilongjiang, China) Abstract: N-Dichloroacetyl-2-methyl-1-oxa-4-aza-spiro-4.4-nonane was synthesized by one pot method with isopropanolamine, cyclopentanone and dichloroacetyl chloride. The optimum reaction conditions obtained are as follows:the proportion in moles of the above materials is 1∶1∶1.2, reaction solvent is toluene, reaction temperature is -15 to -10 ℃,reaction time is 3 h, under the optimum condition, the yield of the compound is 50.0%.

除草剂解毒剂N-二氯乙酰基-2-甲基-1-氧杂-4-氮杂-螺[4.4]壬烷的合成毕洪梅,张金艳,梁英,沈勇(黑龙江八一农垦大学文理学院,黑龙江大庆 163319)摘要:以33%的氢氧化钠水溶液为缚酸剂,异丙醇胺、环戊酮和二氯乙酰氯为原料,采用&一锅法&合成了N-二氯乙酰基-2-甲基-1-氧杂-4-氮杂-螺[4.4]壬烷,采用正交实验法得到最佳反应条件:反应原料摩尔比为1∶1∶1.2,苯作溶剂,反应的温度为-15 ℃~-10 ℃,搅拌时间为3 h,产率达到50.0%。

Polyelectrolyte hydrogels based on n -alkyl methacrylate esters,acrylic acid and acrylamide cross-linked with 4,4′-diazobenzene were prepared.

合成了不同疏水链长的甲基丙烯酸酯、甲基丙烯酰胺及丙烯酸与 4 ,4′-二偶氮苯交联共聚的聚电解质凝胶。

Hydrogels based on n -alkyl methacrylate esters,acrylic acid and acrylamide cross-linked with 4,4′-diazobenzene were preparared.

合成了带不同疏水侧基的甲基丙烯酸酯、甲基丙烯酰胺及丙烯酸与 4,4′二偶氮苯交联共聚的凝胶。

Hydrogels based on n -alkyl methacrylate esters,acrylic acid and acrylamide cross-linked with 4,4′-diazobenzene were preparared,and their deswelling kinetics was studied.

研究了甲基丙烯酸十二烷或丁酯、甲基丙烯酰胺及丙烯酸与4 ,4′-二偶氮苯交联共聚凝胶的消溶胀动力学。

The title nano-sized polymeric microgels were synthesized by emulsion polymerization method,using divinyl benzene as crosslinking agent and methyl methacrylate,hydroxyl ethyl methacrylate,butyl acrylate as monomers.

通过乳液聚合的方法,以二乙烯基苯为交联剂,用甲基丙烯酸甲酯、甲基丙烯酸-β-羟乙酯、丙烯酸丁酯等丙烯酸酯类单体合成纳米尺寸的聚合物微凝胶粒子。

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