苯并

Four non-ionic europium complexes,〓-phen(11),〓·bipy(12),〓·dia(13) and 〓(14)(TTA=2-thenoyltrifluoroacetone, DBM=dibenzoylmethane, phen=phenanthroline, bipy=2,2'-bipyridine, dia=4,5- diazafluoren-9-one, dmbp=4,4'-dimethyl-2,2,-bipyridine), were synthesised and the triboluminescent phenomena of 12, 13 and 14 were firstly observed. Structure determinations of 11,12 and 14 were carried out. The triboluminescence maxima of 12 and 13 are similar to those of their photoluminescence. X-Ray structure analyses show that Eu atoms all exhibit eight-coordinate tetragonal antiprismatic geometries and complexes 11, 12 and 14 are all centrosymmetric.

二、合成了四个非离子型的铕的配合物：〓、〓、和〓(14)[HTTA=2-噻吩三氟甲酰丙酮，DBM=二苯甲酰基甲烷，phen=邻菲罗啉， bipy=2，2'-联吡啶，dia=4，5-二氮杂芴-9-酮，dmbp=4，4'-二甲基-2，2'-联吡啶]，首次报道了12、13及14的摩擦发光性质，测定了11、12及14的晶体结构，并系统地讨论了晶体结构和摩擦发光活性之间的关系。12及13的摩擦发光光谱的极大值均类似与其相应的光致发光光谱，表明它们有相同的激发态。

Due to their applications in magnetic, optical, electronic and catalyst, polynuclear lanthanide clusters are of importance. In this part, a series of nanowheel-shaped nonanuclear lanthanide clusters,〓〓(Ln=Sm~Tm; BA=benzoylacetone), were prepared and characterized. Each complex can exist in three phases, i. e., cubic, tetragonal and triclinic.

本论文第二部分在醇溶液中以三乙胺调变溶液pH，利用β-二酮配位方式的灵活性成功地构筑了一系列结构稳定、纳米尺度轮状的九核稀土配合物〓〓（Ln=Sm~Tm；BA=苯甲酰丙酮），并在不同溶剂中重结晶分别得到了三斜、四方以及立方三种晶型的晶体。

About 100% yield of cyclohexanemethanol could be obtained in the presence of triethylamine if adding more catalyst and prolonging the reaction time.

在三乙胺存在下，增大催化剂用量并延长反应时间，苯甲醛可以100％的收率转化为环己基甲醇，没有出现任何副产物。

The chemical plant of it ,which has more than 20 years history of triphenyl phosphate production and with capacity of 4,000 tons/year,is our fine chemical production base and the biggest professional TPP plant.It is also the only one of refine naphthalene producer in Hebei Province with yields of 10,000 tons/years,Our group has sufficient raw material supply for its own production.

其中，化工厂作为精细化工生产基地，生产磷酸三苯酯已有20余年历史，其规模为4000吨/年，目前在国内属于最大专业生产厂，精萘是河北省唯一生产厂家，现生产规模10000吨/年，并有充足的自备原料。

Some approved aneugens Trip terygiuwlIypogaucum (evelHutch, colchicine, thiabendazole, a tropine sulfate,d-ubocurarine was added into the reactive system respectively and the changes of their absorption values were taken down during different periods under the conditions of 37 0C and 350nm .

本研究通过多步聚合和解聚合反应从猪脑中分离纯化微管蛋白，建立微管蛋白的体外聚合和解聚合反应平衡体系，并将已证实的非整倍体诱发剂（昆明山海棠根部水抽提物、2-（4′-噻唑）苯丙咪唑、硫酸阿托品、d-筒箭毒碱）分别加入此反应平衡体系中，于37℃、350nm条件下，记录此体系不同时期的吸光值变化，与阳性对照物和溶剂对照处理平衡体系后的吸光值在相同时间点作比较，以此评估这几类非整倍体诱发剂对离体条件下的微管蛋白聚合的影响，寻求这几类非整倍体诱发剂是否可通过抑制微管蛋白聚合作用途径而诱发非整倍体。

The structures and configurations of other components weredetermined too.The results show that the structure of components ofChinese lacquer urushiol are the same as components of Japaneselacquer. In this work,2D-heteronuclear relayed coherence transferspectroscopy plays an important role in determining molecularskeleton carbon linkage.

研究结果表明，中国生漆漆酚中含量最大并起关键作用的两双键共轭的三烯漆酚的结构与构型与日本漆中的该组分完全相同，即都有末端甲基的3—十五碳烯烃（8′Z，11′E，13′Z）邻苯二酚，而没有末端双键的存在，其它几个漆酚主要组分的结构也与日本漆酚对应组分基本相同。

Using white rot fungi Mn-dependent peroxidase as main enzyme, the nitrobenzene compounds are degraded. And the unique degradation mechanism is studied.

以白腐真菌锰过氧化物酶为主导酶处理硝基苯化合物，并研究了其独特的降解机理。

If earlier forCorsair was necessary to create aseparat PCB for series XMS2, XMS 2Proand XMS 2,DHX, then now it will be able to create modules on the base of uniform design.

如果早作必要创造一个海盗系列xms2多氯联苯分离，并xms2proxms2、中DHX，那么现在能够创造统一的基础模块设计。

For 480 days of decomposition, the decomposition rate was highest in soil with medium fertility and lowest in soil with low fertility among three type of fertility. The decomposition of water soluble factions and lignin were promoted in medium fertility soil. However, alcohol-benzene soluble fraction, and semi-cellulose and cellulose fraction were decayed acceleratedly in soil with high fertility. Furthermore, more humic substance was formed and energy states of decayed corn stalk was highest in soil with high fertility.

腐解480 d，3种肥力间比较发现，玉米秸秆在中等肥力田块上矿化率最高，低肥力田块上的最低；中等肥力土壤能够促进玉米秸秆中的水溶性有机组分和木质素的分解，而高肥力土壤能够促进苯–醇溶性组分和半纤维素、纤维素分解，并有利于腐殖物质的形成，而且腐解物的能态最高。

Methods: Streptomycin and the derivatization reagent o-phthalaldehyde occur Amine Acetalization generating derivative product with UV absorption and determined the absorbance in special wave length, obtained streptomycin residues in samples then compare with high-performance liquid chromatography.

将试样与衍生化试剂邻苯二甲醛进行胺缩醛反应，即化学衍生处理，生成具有特定波长的紫外吸收的衍生产物，测定其吸光度，求出样品中链霉素残留量，并与高效液相色谱法比较。

This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。