苯并

Through condensing o-aminobenzoic acid, ethyl oxalyl chloride and ethylenediamine(or 1,2-propylenediamine), two new ligands N-benzoato-N′-(2- aminoethyl)oxamido(H3oxbe) and N-benzoato-N-(2-amino-2-methylethyl)oxamido(H3oxbt) have been synthesized. Their mononuclear complexes Na·1.5H2O and Na·1.5H2O have also been obtained.

2以邻氨基苯甲酸、草酸乙酯酰氯和乙二胺(或1，2-丙二胺)缩合制得了两种具有不对称草酰胺结构配体N-(2-苯甲酰基)-N&-(2-氨乙基)草酰胺(H3oxbe)和N-(2-苯甲酰基)-N&-(2-氨丙基)草酰胺(H3oxbt)，并得到了它们的单核配合物：Na·1.5H2O和Na·1.5H2O。

The main pollutants from this chemical plant is perchloroethane, pentachloroethane, hexachlorobutadiene and HCB, and such pollutants are present in the soil with high densities, some as high as 1%- 95%, of which the perchloroethane is near the purity of the corresponding product, and especially this part of the soil contains comparatively high-density persistent organic pollutant HCB, which makes it suitable to be disposed of together with other soils. Therefore it is suggest that this part of soil should be separately dug out and transported outside of the site.

化工厂的主要污染物质是六氯乙烷、五氯乙烷、六氯丁二烯和六氯苯，土壤中上述污染物的浓度非常高，有些达到1%至95%，其中六氯乙烷接近相应的产品的纯度，特别是这一部分含有较高浓度的持久性有机污染物六氯苯，不利于与其它土壤混合处理，建议将这一部分单独开挖出来并运出场外。

In the presence of O〓, peroxyl radicals formed under neutral condition are either directly oxidized to non-aromatic acids, or forms aromatic intermediates, which are further oxidized to non-aromatic acids; peroxyl radicals formed under alkaline conditions are directly oxidized to non-aromatic acids.

有氧状态下的羟基自由基氧化体系中，过氧自由基在氧气的催化作用下既可开环形成有机酸，也可形成4-氯邻苯二酚和对苯二酚，进而氧化开环成有机酸，并最终矿化；碱性条件下的过氧自由基则直接开环降解。

The reaction furnishes a rapid and direct construction of substituted phenanthridine rings from readily available starting materials via a one-pot cascade process, provided a 30-member library of 6-aryl-phenanthridines with yields 31～95%.

在此基础上，我们还考察了用PEG支载的苯甲醛实现该反应的可能性，实验结果表明，由于反应过程中苯炔容易发生自身聚合，并与聚合物支载体夹杂在一起，中间体的纯化相当困难。

Four series and sixteen solid complexes of rare earth chloride with 1-naphthoic acid (L_1),benzoic acid (L_2),phenylacetic acid (L_3) and Mandelic acid (L_4) have been synthesized by method of solid state reaction at low temperature,and then these complexes were characterized by chemical analysis methods.

本文采用低温固相合成法，以稀土氯化物、1—萘甲酸(HL_1)、苯甲酸(HL_2)、苯乙酸(HL_3)、苯羟乙酸(HL_4)为原料，以六次甲基四胺为质子受体，合成并表征了四个系列十六种固态配合物。

The novel methods for the synthesis of Camptothecin intermediates were described as Friedlandle. Second, we synthsized the key compound—BI, and then made some improvements and innovations of the methods from the reference. The method of using more economically phenylaldehyde derivatives and phenylamine derivatives instead of o-aminobenzaldhyde was worked out.

然后成功合成重要的中间体BI，并且在参考原始文献的基础上作出了改进和创新，使用更便宜的苯甲醛衍生物和苯胺衍生物代替了邻氨基苯甲醛，合成了一系列未关B环的喜树碱中间体衍生物，并获得成功。

The effects of solid content of latex, reaction temperature, the amount of phenylhydrazine and pepegal O on the viscosity-average relative molecular mass M(subscript n of LNR were investigated, and the optimization of these influence factors was conducted by orthogonal test.

以天然橡胶浓缩胶乳为原料，在热氧条件下采用苯肼为催化剂通过化学降解法制备液体天然橡胶，考察了胶乳的总固物质量分数、反应温度、稳定剂平平加O和苯肼用量对LNR黏均相对分子质量M(下标 n的影响，并通过正交实验进行优化。

First, the in vitro metabolism of 6-chloro butyl phthalide was investigated and a HPLC method for the study of the in vitro metabolism of butyl phthalide analogues was developed.

首先研究了6-氯正丁苯酞的体外代谢，建立了研究氯丁苯酞及其类似物体外代谢转化的HPLC分析方法，并弄清了它们代谢转化的一般规律。

The measuring of conductivity of the copolymers also indicates that addition of phthalie acid did not destroy the conjugation system of homopolymer of propargyl alcohol.

产物电导率的测量亦说明邻苯二甲酸的加入，并没有破坏聚丙炔醇的共轭体系，但共聚物的电导牢随邻苯二甲酸的含量增加而略有降低。

In the third chapter, the synthesis of5-[(1"S)-1",2"-diacetyl-oxyethyl]-1-phenylpyrazol-3-carboxaldehyde oxime(2) from5-[(1"S)-1",2"-diacetyl-oxyethyl]-1-phenylpyrazol-3-carboxaldehyde(1) and phenyl-hydrazine were introduced firstly. The synthesis of nine dioxapyrrolino[3,4-c]pyrazoles containing chiral pyrazolyl moiety(6a-i) from 2 with N-substituted-phenylmaleimide by nonmetal oxidant IBD-initiated intermolecular 1,3-dipolarcycloaddition was described in detail.

第三章首先以5-[(1′S)-1′，2′-二乙酰氧基乙基]-1-苯基吡唑-3-醛(1)和苯肼为原料，合成了化合物5-(1′S)-1′，2′-二乙酰氧基乙基1-1-苯基吡唑-3-醛-苯腙(2)；再用化合物(2)与N-取代苯基马来酰亚胺反应，利用无金属氧化剂—IBD引发1，3-偶极反应，发生分子间的环加成，合成了9种新型手性吡唑连二氧代吡咯啉并

This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。