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The geometric structures of the ground states of anisole and anisole cation also are optimized at HF/6-31G level, furthermore, the stable structure is acquired. In addition, we also calculate the energy of anisole and its main fragment ions.

应用高斯软件采用HF/6-31G 方法对苯甲醚分子和苯甲醚阳离子基态的几何构型进行优化得到其稳定构型，并计算了苯甲醚分子离子及其初级解离产物的能量。

Firstly, the reactivity of benzaldehyde is studied utilizing the autoclave designed by us in near-critical water.

通过对苯甲醛在近临界水中反应后产物的分析检测认为，苯甲醛在有限的温度范围内微量的发生了Cannizzaro反应，并同时伴随有苯甲醛自身的羟醛缩合反应等其他副反应的发生。

The processes for preparation of tribenuron-methyl and its key intermediates were reviewed. Comparing the yield, quality, cost, safety and environmental protection and other aspects, the best production process of tribenuron-methyl is to use the methyl 2-benzoate and sodium cyanate as raw materials.

综述了苯磺隆及其关键中间体的主要生产工艺，并对各生产工艺在收率、质量、成本、安全环保等方面进行了比较和评价，指出了以邻甲酸甲酯苯磺酰氯、乙腈和氰酸钠为原料的工艺是苯磺隆的最佳生产工艺。

Based on the intelligentized algorithms and Matlab,simulation regarding optimization of benzene-toluene flash vaporization process is made. The simulation result shows that the amount of benzene in vapor phase product reaches the maximum on the condition of effective adjustment of temperature,pressure and diffluence coefficient and the production process is optimized.

对基本蚁群算法进行了智能化改进，并运用智能蚁群算法和Matlab语言，对化工生产过程中的实际优化问题，苯-甲苯闪蒸过程进行了优化仿真计算，仿真结果表明，在有效地调整温度、压力及分流系数的条件下，使得汽相产物中苯的产量达到最大，实现了苯-甲苯闪蒸过程的最优化，同时也证明了蚁群算法可以有效地解决化工生产过程中的优化问题。

1 To mimic the active centers of tyrosinate iron enzymes whichcontain phenolate donors, new tripodal ligand, N-(2-hydroxybenzyl)-N, N-bis(2-benzimidazolymethyl) aminewhich contain imidazoleand phendate groups were designed and synthesized and its iron com-plexes 〓(2)(where Mim=N-Methylimidazole) and Fe 〓(3) were prepared andcharacterized by various spectroscopic methods.

1.1 为了模拟酪酸铁酶活性中心，设计并合成了含有酚羟基和苯骈咪唑基四齿配体N，N-(2-羟基苯)-N，N-二氨，并合成它的铁配合物：Fe〓、Fe〓〓(2)和Fe〓，并经各种谱学手段表征了这些铁配合物。

The crystallization behavior of polyethylene terephthalate ; random poly (ethylene/tetramethylene terephthalate) P (ET/BT ; poly (ethylene terephthalate/ isophthalate) P (ET/EI and poly (ethylene terephthalate/adipate) P (ET/EA copolyesters; and block polyethylene terephthalate/polyethylene glycol and polyethylene terephthalate/polytetramethylene glycol were studied by DLI ; DSC; WAXD; PLM and IR technique.

本文通过缩聚反应合成了不同分子量的聚对苯二甲酸乙二酯；聚对苯二甲酸酯P(ET／BT、聚（对苯二甲酸／间苯二甲酸）乙二醇酯P(ET／EI和聚乙二醇酯P(ET／EA等系列的无规共聚酯以及PET／PBG和PET／PEG等系列的嵌段共聚酯，并采用DLI、DSC、WAXD、IR和NMR等实验技术着重研究了它们的结晶行为与共聚酯的序列结构。

The crystallization behavior of polyethylene terephthalate ; random poly (ethylene/tetramethylene terephthalate) P (ET/BT ; poly (ethylene terephthalate/ isophthalate) P (ET/EI and poly (ethylene terephthalate/adipate) P (ET/EA copolyesters; and block polyethylene terephthalate/polyethylene glycol and polyethylene terephthalate/polytetramethylene glycol were studied by DLI ; DSC; WAXD; PLM and IR technique.

中文题名PET及其共聚酯的结晶行为副题名外文题名 The crystallization behavior of PET and its copolyesters 论文作者边界导师封麟先叶胜荣教授学科专业高分子化学与物理研究领域\研究方向学位级别博士学位授予单位浙江大学学位授予日期2001 论文页码总数10，159页关键词聚对苯甲酸乙二酯聚酯结晶馆藏号BSLW /2003 /O633 /1 本文通过缩聚反应合成了不同分子量的聚对苯二甲酸乙二酯；聚对苯二甲酸酯P(ET／BT、聚（对苯二甲酸／间苯二甲酸）乙二醇酯P(ET／EI和聚乙二醇酯P(ET／EA等系列的无规共聚酯以及PET／PBG和PET／PEG等系列的嵌段共聚酯，并采用DLI、DSC、WAXD、IR和NMR等实验技术着重研究了它们的结晶行为与共聚酯的序列结构。

As to the high polarity, high boiling point resultant—trimesic acid, the analysis methods of infrared spetrum, gas chromatography-mass spectroscopy, vapour-phase chromatography, acid number titration and so on are seperately used to characterize its property. Infrared spetrum and gas chromatography-mass spectroscopy are used to have a qualitative analysis on the resultant and are compared with the stand diagram. Sulfuric acid-methanol esterification and rapid esterification are used to prepare the trimesic acid trimethyl-ester and have a FID quantitative analysis. So that we make sure the purity of trimesic acid in the resultant and also we have an acid alkali titration on the resultant to get its acid number, in order to verify the purity of trimesic acid in the resultant.

对于高极性、高沸点的固体产物均苯三甲酸，分别采用红外光谱、气质联用、气相色谱、酸值滴定等分析手段进行了表征：利用红外光谱、气质联用的方法进行产物的定性分析，并与在同一仪器、同一条件下做出的标准谱图进行比对；采用硫酸-甲醇酯化法和快速酯化法制备出均苯三甲酸三甲酯，对其进行气相色谱FID定量分析，进而确定固体产物中均苯三甲酸的纯度；用酸碱滴定法确定固体产物的酸值，以对固体产物中均苯三甲酸的纯度进行验证。

And then high performance liquid chromatography method was used to delect the blood plasma concentration of Ivermectin and Albendozale with Dual λ Absorbance Detector at the same time, which have the good lineal relation in the range of 40-640ng/ml, the equation of Ivermectin is y=0.0077+0.0117C (r=0.9994), Albendozale is Y=0.0578+0.0027C (r=0.9680). With the same method the recovery of Ivermectin and Albendozale in blood plasma concentration 60. 240. 480ng/ml were 93.5%.

然后用HPLC方法采用双波长检测器同时测定伊维菌素和阿苯达唑的血浆药物浓度，伊维菌素和阿苯达唑在40-640ng／ml范围内线性关系良好，伊维菌素的回归方程为Y=0.0077+0.0117C(r=0.9994)，阿苯达唑的回归方程为Y=0.0578+0.0027C(r=0.9680)，并测定了阿苯达唑和伊维菌素在60、240、480ng／ml的回收率分别为94.2％、97.6％、101.40％和93.5％、98.3％、98.7％，表明回收率较高。

Phthalic acid esters are widely used in the many fields of industry. So many countries including China have come to pay attention to them and make up the codes for limiting the content in some products such as textile. By combining international codes, the thesis selects coating and textile that have close relative with people as objections. The research results are as follows:1. The thesis has established the textiles preparation method by a series of experimentations such as extraction solvent, extraction time, solid-phase extraction. The average recoveries of eleven phthalates are from 80.30% to 98.00%, and the relative standard deviations from 0.59% to 2.56%, the results show that this method is accurate and credible.2. The thesis set up the simultaneous determination of benzene, toluene, xylenes and phthalates in coatings.

邻苯二甲酸酯类化合物被广泛地应用在工业领域的各个方面，国际上已经开始重视邻苯二甲酸酯作为一种内分泌干扰素的危害性，对在一些产品中的用量作出了限制，但没有具体的分析测定方法，本论文结合国际法规选择了与人们生活密切相关的涂料和纺织品来研究其中邻苯二甲酸酯类环境激素的测定方法，研究内容如下：(1)通过对提取溶剂、提取方式、提取时间的选择实验以及固相萃取的一系列条件实验，首次建立了纺织品中测定邻苯二甲酸酯类环境激素的前处理方法，并对分析方法作了准确度、精密度验证。

This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。