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The development and application of supramolecular chemistry and NMR were reviewed.Based on that,several benzimidazole derivatives were synthesized from o-phenylenediamine.

本文在总结超分子化学及核磁共振的发展及应用的基础上,以邻苯二胺为原料,合成了几种苯并咪唑衍生物,作为分子识别中的客体小分子。

The organic compounds obtained from the first step reaction are mainly benzophenone,9,10-anthraquinone and 1,3-Diphenylisobenzofuran and so on.

第一步中生成的有机化合物主要成分为二苯甲酮、9,10-蒽醌和1,3-二苯基异苯并呋喃等。

One UV absorber is a benzotriazole derivative, and the other UV absorber is a benzophenone derivative.

一种紫外吸收化合物是苯并三唑衍生物,另一种紫外吸收剂为二苯酮衍生物。

In this thesis, a type of biphenyl rod-like liquid crystals and two types of triphenylene discotic liquid crystals were synthesized.

本文报道了一类新的联苯类棒状液晶化合物和两类苯并菲盘状液晶化合物的合成。

Ethyl 4-[(1-hydroxy-1-methyl)ethyl]-2-propyl-1H-imidazole-5-carboxylate,the key intermediate of Olmesartan ,was synthesized from butanoic acid and o-phenylenediamine via condensation under microwave-irradiation,oxidation,esterification and the Gringard reaction.

用正丁酸与邻苯二胺为原料,在微波照射下缩合成2-丙基苯并咪唑,再氧化开环制得2-丙基咪唑二羧酸,再经酯化、Gringard反应制得抗高血压药物奥美沙坦的关键中间体2-丙基-4-[(1-羟基-1-甲基)乙基]-1H-咪唑-5-羧酸乙酯,总收率32.2%。

This article through the belt hydroxyl aldehyde class material and the chloroacetic acid response, the synthesis intermediate, then with the neighbouring phenylene diamine responded again synthesized 6 kind of benziminazole class compound, including 4 kinds not to report.

本文通过带羟基的醛类物质和氯乙酸的反应,合成中间体,然后再与邻苯二胺反应合成了6种苯并咪唑类化合物,其中有4种还未被报道。

Compound 9 is glycosylated in the presence of TMSOTf with rhamose-derived trichloroacetimidates to provide target trisaccharide Saponin 1, oleanolic acid 3-yl-2,4-di-O-a-L-rhamnopyranosyl -p-D-glucopyranosideCoumpond 18 is prepared with oleanic acid and Bromide 11 through phase-thansfer catalysis glycosylation manner.

三糖皂苷Saponin 1是以葡萄糖齐墩果酸皂苷为起始原料,用BBTZ(1-苯甲酰苯并噻唑)选择性保护葡萄糖3′,6′-羟基得到化合物9,然后以化合物9为糖基受体,进行一步糖苷化可以在化合物9的2′,4′-羟基上同时引入两分子鼠李糖,最后脱掉所有的保护基得到目标化合物Saponin1。

Phthalimide,anthranilic acid,2methyleneglutaronitrile bromina 1bromobutane 1,2benzisothiazole3one.

邻苯二甲酰亚胺,邻氨基苯甲酸,2亚甲基戊二脯,2溴2溴甲基戊二脯,溴代正丁烷,1.2苯并异噻唑3酮。

A bacterial strain using phenol, benzoate, naphthalene, biphenyl and benzothiophene as sole carbon and energy sources was isolated from waste sludge and was identified as Rhodococcus sp. strain DF51 according to morphological, physiological and its 16S rRNA gene sequence.

从太原市郊苯酚污染的土样中分离到一株能以苯酚、苯甲酸、萘、联苯和苯并噻吩为唯一碳源和能源生长,并且具有同时分解单环和双环芳香类物质能力的菌株,经生理生化和16S rDNA基因序列分析鉴定为红球菌DF51Rhodococcus sp。

Therefore, it is important that we must make efforts to explore the research and development of benzotriazole and its derivatives.

本课题首先采用原料廉价易得的邻硝基氯苯法合成苯并三氮唑,对合成过程进行了研究。

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