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Adopting TPB as catalyzer of solidifying chemical reaction,it can distinctly quicken reactive rate. It is relatively reasonable for controling reactivetemperature at 50℃. Vacuumized and deposited one day at normal temperature before hightemperature solidifying chemical reaction, which is propitious to remove air bubble frompropellant columniation.

采用三苯基铋作固化催化剂,可明显加快固化反应的速度,固化反应的温度控制在50℃比较合理,在高温固化前抽真空和常温下放置一天有利于排除药柱中的气泡。

When ATRP of styrene was investigated with 1-phenylethyl bromide/benzyl a,a-dibromide mixture as initiator, the GPC chromatogram shows two elution peaks and the molecular weighs of the peaks are approximately in a 2/1 ratio. It suggests that benzyl dibromide is a difunctional initiator of ATRP of styrene. The analysis of end group using 1H-NMR also proves the result above.

采用1-苯基溴乙烷/α,α-二溴化苄混合引发剂进行苯乙烯的ATRP反应时,所得聚苯乙烯的GPC谱图为双峰,分子量相差一倍,初步证明了α,α-二溴化苄引发苯乙烯ATRP反应时是双官能引发剂,并用~1H-NMR对聚合物结构进行分析,进一步证明了α,α-二溴化苄引发苯乙烯ATRP时是双端同时增长的。

The synthesis method of p-menthylphenyl mercuric chloride was carried out.

研究了合成对甲苯基氯化汞的方法,考察了反应物料比、反应温度等对合成的影响,给出了合成的最佳反应条件。

Modifications of alkylation, chlorination and Vilsmeier reaction were employed for the synthesis of aromatic aldehydes bearing nitrogen mustard derivatives and halogenoalkylpiperazinyl.

通过对Vilsmeier反应、烷基化反应和氯化反应的改进提出了以简单易得的苯胺和苯基哌嗪为原料制备氮芥和哌嗪芳香醛的方法。

We examined the effects and mechanisms of methyl pentyl 1,4-dihydro-2,6-dimethyl-4-(3-notrophenyl)-3,5-pyridinedicarboxylate (Mn9202), a novel DHPs calcium antagonist and lacidipine on the 5-HT2B receptor in cultured rat stomach fundus smooth muscle cells.

本研究以富含5-HT_(2B)受体的大鼠胃底平滑肌细胞为模板,观察了二氢吡啶类钙拮抗剂2,6-二甲基-4-(3-硝基苯基)-1,4-二氢-3,5-吡啶二羧酸-3-甲酯-5-正戊酯(Mn9202)、拉西地平对 5-HT_(2B)受体功能的影响,并对其影响机制进行了较为深入的研究。

The purpose of this paper is to synthesize some phosphonium salts with PPh3 and some chiral quaternary ammonium salts with L-Valine. And we also use L-Valine and L-Phe-OMe to synthesize a new type catalyst —2,5-diketopiperazine , the simplest compound of cyclo-peptide.

本文利用廉价易得的三苯基磷和手性L-缬氨酸作为起始原料,合成了几种普通季鏻盐和手性季铵盐,并且利用L-缬氨酸与L-苯丙氨酸甲酯反应,合成了一种新型的相转移催化剂——2,5-二酮哌嗪环类的化合物。

In the synthesis process of ligands and their rare earth complexes, metal lithium is used to substitute for n-butyllithium, such as the synthesis of fluorenyl lithium, piperonal dimethyl acetal lithium, and bis (9-fluorenyl) silylene lithium.

合成配体和配合物的中间体均采用金属锂代替正丁基锂,如芴锂、溴代胡椒醛二甲基缩醛基锂盐、甲基苯基双芴基硅烷双锂盐的制备,方法简单,操作简便,副反应少,且锂盐的浓度和用量易于控制。

Based on the tissue culture, the effect of N-phenyl-N'-1,2,3-thiadiazol-5-ylurea, 6- benzyla minoprine(6-BA) and 1-Naphthylacetic acid on spore germination, protonema develop- ment and bud differentiation in Entodon challenged was investigated in this paper. The whole process was observed and taken pictures. The results show that TDZ, 6-BA and NAA have no significant effect on the spore germination. During the process of protonema development, 1.0 mg/L NAA can promote the primary development of protonema significantly, and 0.4 mg/L TDZ promotes branches formation in inter- mediate stage of the protonema development.

:研究了3种植物生长调节剂苯基噻二唑基脲、6-苄基腺嘌呤(6-BA)、萘乙酸对密叶绢藓孢子萌发、原丝体发育及芽体发生的影响,并对整个发育过程进行了显微观察和照相,结果表明:(1)3种植物生长调节剂对密叶绢藓孢子萌发影响不显著;(2)在原丝体发育阶段,1.0mg/LNAA对原丝体初期的发育促进效果显著,0.4mg/LTDZ对原丝体发育中期分枝的形成促进效果显著,6。

There are two stages in the thermal oxidative degradation of the thermally cured polymethylphenylsiloxane resin.

热固化的聚甲基苯基硅树脂的侧基显示出不同的热氧化稳定性。

The reactivities of 1 and other long chain oximes with p nitrophenyl diphenyl phosphate, p nitrophenyl diethyl thiophosphate, and O ethyl ( s β diisopropylaminoethyl) methyl phosphonothiolate were studied.

报道了一种新的高亲核长链咪唑肟N 十四烷基咪唑 2 甲醛肟的设计与合成,并比较了它及其他长链咪唑肟与有机磷酸酯二苯基、对硝基苯基磷酸酯、对硫磷及 Vx 的反应活性。

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What would he tell Judith and the children?

他将怎样告诉朱迪丝和孩子们呢?

I this is at that time, the opinion with peacockish true girl is full of in a heart.

这就是当时的我,一个心中布满虚荣的女孩子真实的想法。

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