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The preparation method comprises monomer synthesis and polymer synthesis. The polymer synthesis is that cyclopentadienyl sodium monomer is added into metallic cobalt complex-triphenyl phosphorus cobalt chloride under strict oxygen-free and water-free conditions, and then double inner alkyne or outer alkyne conjugate monomer is added in, and after reaction, the precipitation, filtering, abstersion and vacuum-drying are carried out, the large molecules polymer containing cyclopentadienyl cobaltocenium organometallic cobalt is obtained.

制备方法,包括单体合成和聚合物的合成,聚合物的合成是在严格无氧无水条件下,在金属钴配合物三-三苯基磷氯化钴,加入环戊二烯钠单体,随后加入双内炔或双外炔共轭单体,反应后沉淀,过滤,洗涤,真空干燥,得到含环戊二烯茂钴有机金属钴的大分子聚合物。

Under appropriate conditions, the conversion of acetophenone could be as high as 100% and the enantiomeric excess of-1-phenylethanol exceeded 99.0%.

在合适的条件下底物苯乙酮的转化率高达100%,产物-1-苯基乙醇的对映体过量值大于99.0%。

The catalyst includes: supported Ziegler-Natta catalyst of titanium halide compound and organic electron donor compound supported with MgCl2 alcoholate carrier; aluminoxane prepared with trialkyl aluminum and water; and one kind of organic electron donor, such as organosilicon compound R2Si(OCH3)2, where R is phenyl, isopropyl, isobutyl or cyclopentyl.

该催化剂包括,a一种负载型的Ziegler-Natta催化剂,即将卤钛化合物和有机给电子体化合物负载在氯化镁醇合物载体上得到的固体催化剂,b一种通过三烷基铝与水反应而制备得到的铝氧烷和c一种有机电子给体,如有机硅化合物R 2 Si(OCH 3 ) 2 ,其中R为苯基、异丙基、异丁基或环戊基。

The course of reaction was monitored by estimating the amount of isopropanol liberated in benzene-isopropanol azeotrope in each case.

合成是在苯溶液中采用了金属/非金属的异丙氧基化合物和N-(2-甲基)苯基甘氨酸按1:1和1:2的配比完成的。

It was shown that the phenyl site index of straight chain alkylbenzene isomers and low-carbon alkylbenzenes is a useful topological index and can be applied to structure- property correlation.

结果表明:直链烷基苯的异构体和低碳烷基苯的苯基位置指数作为一种拓扑指数,可应用于结构-性质相关关系的研究。

Spear Heads or Pheons - Dexterity and nimbleness of wit to penetrate and understand matters of highest consequence.

枪尖或Phenos(这个词在词典里的解释是&苯、苯基&)-以敏锐思维对事物予以最深刻理解的智慧。

Then, it was condensed with-valine methyl ester to form a chiral imine, which was reacted with allyl zinc bromide in the presence of CeCl3·7H2O to afford the corresponding chiral homoallylic amine with high optical activity.

-N-Boc-3-苯基-2-氨基丙醛与-缬氨基酸甲酯缩合生成手性亚胺,在七水合三氯化铈(CeC13·7H2O)催化以及底物的手性诱导作用下,该手性亚胺与烯丙基溴化锌经不对称加成反应合成了高光活性的单烯丙基化手性胺。

Part 2 : extraction of fat, pesticides and pcbs, and determination of fat content.

第2部分:脂肪、农药和联苯基多氯化物的提取及脂肪含量的测定

Employing CuI(5 mol%), N,N-dimethylglycine hydrochloride(10 mol%) and K_2CO_3(2 equiv.) in refluxing THF as the optimized reaction conditions,the four-membered 4-alkylidene-2-azatidinones could be efficiently synthesized.

当以3-溴-3-N-苯基-丁烯酰胺为底物,在5 mol%CuI为催化剂,10 mol%N,N-二甲基甘氨酸盐酸盐为配体,2当量K_2CO_3作碱,THF回流的反应条件下,可以高效的合成2-亚甲基-4-氮杂环丁酮类化合物。

Amino-3-cyan-N-(2,6-dichloro-4-trifluoromethylphenyl)pyrazole was the important intermediate which was used to synthesize the efficient insecticide "Regent", which was researched and gone in to operation firstly by French Phone Poulenc company.

中文摘要: 5-氨基-3-氰基-N-(2,6-二氯-4-三氟甲基苯基)吡唑是合成高效杀虫剂&锐劲特&的重要中间体,最先由法国罗纳普朗克公司研发并投产,在国内鲜有相关的合成报道。

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What would he tell Judith and the children?

他将怎样告诉朱迪丝和孩子们呢?

I this is at that time, the opinion with peacockish true girl is full of in a heart.

这就是当时的我,一个心中布满虚荣的女孩子真实的想法。

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哦,我还给我自己买了一个新笔记本"他说。"