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A new photochromic organic compound of thiosemicarbazone, 4-( p -bromo-α-methylaminothiocarbonyl hydrazonobenzal)-2,5-dihydro-3-methyl-5-oxo-1-phenyl pyrazole, was synthesized and characterized by elemental analyses, IR, 1H NMR spectra, and X-ray single-crystal diffraction analysis.

文章合成了一个新的有机化合物1-苯基-3-甲基-4-对溴苯亚甲基-吡唑啉酮-5 缩甲基氨基硫脲(1),并分别用元素分析、红外光谱、氢核磁共振及X-射线单晶衍射对化合物的结构进行了确证和表征。

Eight complexes of light rare earths with dioctyldithiocarbamate,〓 xH〓O (RE=La-Tb, except for Pm) and Nine complexes of rare earths with 5-phenyl pyrazoline dithioformate, Na RE〓·xH〓O (RE=La-Dy, Y, except for Ce and Pm) have been synthesized in air and dry N〓atmosphere, respectively.

分别在空气和氮气保护条件下,合成出八种稀土与二正辛基二硫代氨基甲酸形成的配合物〓(RE=La-Tb,除Pm外)和九种稀土与5-苯基吡唑啉二硫代甲酸的固态配合物NaRE〓(La—Dy、Y、除Ce、Pm外)。

A series of polys based on pyromellitic dianhydride, biphenylyl tetracarboxylic dianhydride, thiodiphthalic dianhydride bis benzene dianhydride and oxydiphthalic dianhydride were prepared in different solvents.

以所合成的AB_2单体为原料,合成了一系粘度较低、溶解性良好,带端酚羟基、苯甲酰基、乙酰基、氰代苯基和苯酰苯亚胺基的芳香族超支化聚酰亚胺,通过核磁波谱、红外光谱分析和元素分析对其结构进行确证。

Stuay on electronic structures and spectra properties of 3-phenly6-aryl-1,2,4 triazolo[3,4-b]thiadiazole with time-dependent density functional theory.

李会学,萧泰。3-苯基-6-芳基-1,2,4-三唑并[3,4-b]-1,3,4-噻二唑的电结构和光谱性质的含时密度泛函理论研究。

Pentanediol reacted with phosphorus tribromide to make it mono-bromination, under the catalytic action of PPTs it reacted with 2,3-dihydropyran to protect another hydroxy group, then to react with triphosphine, produced quarterphossal.

再以1,5-戊二醇为原料,三溴化磷使之单溴代,得到5-溴-1-戊醇,在对甲苯磺酸吡啶盐的催化下与2,3-二氢吡喃反应保护其另一端的羟基,与三苯基膦反应生成季磷盐。

A silver ion selective electrode was prepared and characterized with trimethylene bis (N-ethyl-N-phenyldithiocarbamate) as ionophore.

制备并考察了以双(N-乙基-N-苯基氨基二硫代甲酸)1,3-丙二醇酯为载体的银离子选择电极的性能。

The different enzyme protecting agent had effected on the liquid alkaline protease under the dissimilar condition. Taking the living rate of enzyme as the target, we obtained one high effective alkaline protease stabilizing agent formula through orthogonal experiments as following: 5 mmolL^(-1) Ca(superscript 2+), 15mgmL^(-1) trimethylene glycol-single methyl ether, 0.015% 4-formyl phenyl-boron dihydroxide, 1% glycerine.

在此基础上,进行L13(3^7)正交实验,以相对酶活率为指标,考察了不同酶活性保护剂在不同条件下对液体碱性蛋白酶活力的影响,筛选到一种优质高效的碱性蛋白酶稳定剂配方为:5mmolL^(-1) Ca(上标 2+),15mgmL^(-1)丙二醇-单甲醚,0.015% 4-甲酰苯基硼酸,1%甘油。

Hydroesterification of tert-butyl alcohol with ethanol catalyzed by transition metal triphenylphosphine complexes was first investigated in room temperature ionic liquids.

反应温度为100~140 ℃,CO初始压力为2~6 MPa条件下,研究了室温离子液体与过渡金属三苯基膦配合物构成的催化反应体系中,叔丁醇与乙醇的氢酯基化反应。

One mixed-ligand complex ofnH2Otpa=terephthalate, tripy=4'-(4methyoxyphenyl-2,2':6',2-terpyridine was synthesized and characterized by IR, elemental analysis and thermo-gravimetric analysis. The crystal structure of the product was established by single-crystal X-ray diffraction.

采用水热法合成了新的维链状锌的配位聚合物nH2O(tpa=对苯二甲酸,tripy=4'-(4-甲氧基苯基)-2,2':6',2-三联吡啶),通过红外光谱和元素分析对该配位聚合物进行了结构表征,用X射线单晶衍射测定了晶体结构。

In the process, 2, 4-difluoroaniline is used to carry out ammoniated reaction. Then through a series of similar reactions, the important intermediate of temafloxacin, which is called 7-chloro-6-fluoro-1-(2, 4-difluorophenyl)-1, 4-dihydro-4-oxo-3-quinoline acid, is gained.

与环丙沙星和二氟沙星类似,用2,4-二氟苯胺进行胺化反应,再进行一系列类似的反应,制得合成替马沙星的关键中间体7-氯-6-氟-1-(2,4-二氟苯基)-1,4-二氢-4-氧代喹啉-3-羧酸。

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What would he tell Judith and the children?

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I this is at that time, the opinion with peacockish true girl is full of in a heart.

这就是当时的我,一个心中布满虚荣的女孩子真实的想法。

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