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To further study the chemical constitutes of lipophilic active parts, we prepared Alc95% and Alc50% according to original literature. 20 compounds were isolated by using macroporous resin, silica gel, polyamide, Sephadex LH-20, Rp-18, preparative TLC and preparative HPLC chromato-graphy. The structures of them were elucidated by means of physical and chemical properties, modern spectroscopic analysis techniques—UV、IR、 EI/MS、ESI/MS、〓H-NMR、〓C-NMR、DEPT、HMQC、HMBC. They are nine anthraquinones: chrysophanol (95-1), physcion (95-2), emodin (95-5), aloemodin (95-7), rhein (50-1), sennoside A or B (50-6),ω-hydroxylemodin (95-10), chrysophanol-8-0-β-D-glucoside (95-12), aloemodin-ω-0-β-D-glucoside (95-13); three phenanthaquinones: tanshinone ⅡA (95-3), cryptotanshinone (95-6), tanshinone Ⅰ(95-4); one isoflavone: 7, 3'-dihydroxyl-5' methoxyisoflavone (95-14) and protocaechuic aldehyde (95-9), protocaechuic acid (95-11), astragaloside Ⅳ(50-4), amygdalin (50-5), 2, 3, 5, 4'-tetrahydroxylstilbene-2-0-β-D-glucoside (50-3),-catechin (50-2), cinnamic acid (95-8). Among them, 3'-dihydroxyl-5' methoxyisoflavone (95-14) is a new compound.

经过溶剂萃取、大孔吸附树脂富集、Sephadex LH-20精制、制备TLC及Semi-pre HPLC等手段从中分离了20个化合物,利用理化性质和波谱技术(UV、IR、EI/MS、ESI/MS、〓H-NMR、〓C-NMR、DEPT、HMQC、HMBC)相结合鉴定了它们的结构,分别为9种蒽醌类化合物:大黄酚,大黄素甲醚,大黄素,芦荟大黄素,大黄酸,番泻苷A或B,ω-羟基大黄素(ω-hydroxylemodin),大黄酚-8-0-β-D-葡萄糖苷(chrysophanol-8-0-β-D-glucoside),芦荟大黄素-ω-0-β-D-葡萄糖苷(aloemodin-ω-0-β-D-glucoside);3种菲醌类化合物:丹参酮ⅡA(tanshinoneⅡA),隐丹参酮,丹参酮Ⅰ(tanshinone Ⅰ);1种异黄酮:7,3'-二羟基-5'-甲氧基异黄酮(7,3'-dihydroxy-5' methoxyisofla-vone)以及原儿茶醛,原儿茶酸,黄芪甲苷(astragaloside Ⅳ),苦杏仁苷,2,3,5,4'-四羟基二苯乙烯-2-0-β-D-葡萄糖苷(2,3,5,4'-tetrahydroxylstilbene-2-O-β-D-g1ucoside),Z—儿茶素,桂皮酸。

Iodobenzene, bromobenzene and their derivatives reacted smoothly with n-butyl acrylate or styrene under phosphine-free reaction conditions in the presence of palladium acetate and fluoroquinolones.

碘苯、溴苯和其它芳基卤衍生物与丙烯酸丁酯、苯乙烯等取代乙烯类化合物在钯和氟喹诺酮的催化下发生Heck反应。

The monomer ofbromostyrene was synthesized fromβ-bromobenzene by eliminating hydrogenbromide under sodium hydrate.

溴乙基溴代苯在氢氧化钠的作用下,发生溴化氢脱除反应,得到溴代苯乙烯单体。

Synergetic antifungal effects were observed in the combination of albicanyl caffeate or 3,4'-difluorostilbene and fluconazole, whereas additive antifungal effects were revealed when catechin or resveratrol combined with fluconazole.

当与氟康唑联合时,albicanyl caffeate和3,4'-二氟二苯乙烯显示出协同抗真菌活性,而儿茶素与白藜芦醇显示出相加的抗真菌活性。

Catalytic oxidation of styrene with aqueous hydrogen peroxide (ω=26%) indicates that Mo-MCM- 48 is catalytically active.

苯乙烯催化氧化结果表明Mo-MCM-48具有一定的催化氧化活性。

The gel acid cinnamene resin of HP1110Na was selected as the best desalination resin.

确定HP1110Na型凝胶强酸苯乙烯树脂为较为理想的脱盐树脂。

The molecule has a typical D-π-A structure with terminal units of electron donor and accepter groups. The triphenylamine group, as the electron donor, is connected to the oxadiazole group which is the electron accepter through the cinnamene group.

该分子具有典型的D-π-A型推拉电子结构,三苯胺基团作为给电子基通过苯乙烯共轭链桥接到吸电子基1,3,4-恶二唑基团。

Methods CBP 20 capillary column was used and the temperature was increased with a program to separate and determine 7 kinds of benzenes series,namely,benzene,toluene,ethylbenzene,p-xylenol,inter-xylenol,cinnamene and ortho-xylenol.

利用CBP-20毛细管色谱柱,采用程序升温实现苯、甲苯、乙苯、对二甲苯、间二甲苯、苯乙烯、邻二甲苯等7种苯系物的分离测定。

The magnetic microbeads with 1μm diameter are synthesized by ultrafine γ-Fe2o3, cinnamene, diethylene benzene monocase combined suspendd polymerize and ultrasonic technology. The magnetic microbeads are composed of ultrafine magnetic powders, polymer and single-antibody.

采用超细r-Fe2O3粉对界面进行处理,利用苯乙烯、二乙烯基苯单体,采用悬浮聚合法和超声波技术,合成粒径为1μm左右的磁性微珠,该磁性微珠由超细磁粉、高分子材料和单抗功能基团组成。

The magnetic microbeads with 1um diameter were synthesized by ultrafined r-Fe2O3, cinnamene, diethylene benzene moncase combined suspend polymerize and ultrasonic technology. The magnetic are composed of ultrafine magnetic powders, polymer and single-antibody.

采用超细r-Fe2O3粉界表面进行处理,利用苯乙烯、二乙烯基苯单体,采用悬浮聚合法和超声波技术,可以合成粒径为1um左右的磁性微珠,该磁性微珠由超细磁粉、高分子材料和单抗功能基团组成。

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The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

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