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苯乙二醇

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The optimum reaction conditions are as follows: diphenylmethanethiol : methyl chloroacetate is 1:1.5, and the reaction carried out at 100℃ for 4 h, 2- acetamide can be carried out in the room temperature for 20 h, the yield of 2- acetamide was 76%, hydrogen dioxide: 2- acetamide is 1:1, and the reaction carried out at 60℃ for 3 h, the yield of modafinil was 79%, the total yield of reaction can be reached 48%.

研究表明,采用氯乙酸甲酯作为醚化试剂,反应时间4h,反应温度100℃,二苯甲硫醇:氯乙酸甲酯=1:1.5,室温下氨解反应20h,二苯甲硫乙酰胺收率76%;采用过氧化氢作为氧化试剂,反应时间3h,反应温度60℃,过氧化氢:二苯甲硫乙酰胺=1:l,莫达非尼收率79%,反应总收率可达48%。

Main Ingredients: Water,Hamamelis Virginiana Water,Glycerin,Propylene Glycol,Gm Euglena Gracilis Polysaccharide,Betaine,Aloe Barbadensis Leaf Juice,Hydrolyzed Wheat Protein,Sodium Pca,Tocopheryl Acetate,Polysorbate 20,Creatine,Hyaluronic Acid.

主要成分:去离子水,金缕梅蒸馏液,甘油,丙二醇,细小裸藻多糖,甜菜碱,芦荟叶提取物,水解小麦蛋白,吡咯烷酮羧酸钠,生育酚乙酸酯,聚山梨醇酯-20,肌酸,透明质酸,乙二胺四乙酸四钠,香精,苯氧乙醇,辛二醇,山梨酸。

For the synthesis reaction of chalcone, cyclohexanone aldolization and biodiesel,γ-Al_2O_3-NaOH-Na solid superacid has a satisfactory catalytic activity. With hypnone and phenylaldehyde as raw material, amount of catalyst 7.5% wt% of material, mole ratio of hypnone and phenylaldehyde 1:1.1, reaction temperature 40℃, after 3 hours, the yield of chalcone can be up to 96.88%. With cyclohexanone as raw material, amount of catalyst 10% wt% of material, reaction temperature 190℃, after 3 hours, dimmer of cyclohexanone can be up to 85.66%.

将该固体超强碱催化剂应用于查尔酮、环己酮自缩合以及生物柴油的合成反应中,该改性固体超强碱催化剂表现出了良好的催化活性:以苯乙酮和苯甲醛为原料,反应温度为40℃,催化剂用量为反应物总质量的7.5%,苯甲醛与苯乙酮摩尔比为1:1.1,反应3h查尔酮产率可达96.88%;以环已酮为原料,催化剂用量为原料总质量的10%,反应温度为190℃,反应3h,二聚物的总收率可达85.66%;以动物油和甲醇为原料,醇油摩尔为9:1,催化剂用量为动物油质量的2%,反应温度为70℃,反应3h后,生物柴油的收率可达91.8%。

Ingredients: Water,Hamamelis Virginiana Water,Glycerin,Propylene Glycol,Glyceryl Polymethacrylate,Betaine,Aloe Barbadensis Leaf Juice,Hydro-lyzed Wheat Protein,Sodium Pca,Tocopheryl Acetate,Polysorbate 20,Creatine,Hyaluronic Acid,Tetrasodium Edta,Perfume,Phenoxyethanol,Caprylyl Glycol,Sorbic.

成分:去离子水,金缕梅蒸馏液,甘油,丙二醇,甘油聚甲基丙烯酸酯,甜菜碱,芦荟叶提取物,水解小麦蛋白,吡咯烷酮羧酸钠,生育酚乙酸酯,聚山梨醇酯-20,肌酸,透明质酸,乙二胺四乙酸四钠,香精,苯氧乙醇,辛二醇,山梨酸。

Ingredients: water,glycerin,caprylic/capric triglyceride,cetyl alcohol,squalane,glyceryl stearate,panthenol,betaine,dimethicone,lavandula angustifoliaoil,allantoin,carbomer,xanthan gum,parfum,triethanolamine,tocopheryl acetate,hyaluronic acid,methyl paraben,propyl paraben,creatine,tetrasodium edta,phenoxyethanol,caprylyl glycol,sorbic.

成分:去离子水,甘油,辛酸/葵酸三甘油酯,鲸蜡醇,角鲨烷,硬脂酸甘油酯,泛醇,甜菜碱,聚二甲基硅氧烷,薰衣草精油,尿囊素,卡波姆,汉生胶,香精,三乙醇胺,生育酚乙酸酯,透明质酸,对羟基苯甲酸甲酯,对羟基苯甲酸丙酯,肌酸,乙二胺四乙酸四钠,苯氧乙醇,辛二醇,山梨酸。

Ingredients:Water,Glycerin,Caprylic/Capric Triglyceride,Cetearyl Alcohol,Squalane,Glyceryl Stearate,Panthenol,Betaine,Dimethicone,Oiea Europaea Oil,Allantoin,Glyceryl Stearate Se,Carbomer,Xanthan Gum,Parfum,Triethanolamine,Tocopheryl Acetate,Hyaluronic Acid,Methyl Paraben,Propyl Paraben,Creatine,Tetrasodium Edta,Phen-oxyethanol,Caprylyl Glycol,Sorbic.

成分:去离子水,甘油,辛酸/葵酸三甘油酯,鲸蜡硬脂醇,角鲨烷,硬脂酸甘油酯,泛醇,甜菜碱,聚二甲基硅氧烷,橄榄油,尿囊素,自乳化硬脂酸甘油酯,卡波姆,汉生胶,香精,三乙醇胺,生育酚乙酸酯,透明质酸,对羟基苯甲酸甲酯,对羟基苯甲酸丙酯,肌酸,乙二胺四乙酸四钠,苯氧乙醇,辛二醇,山梨酸。

Ingredients:Water,Glycerin,Caprylic/Capric Triglyceride,Myristyl Myristate,Butyrosper-mum Parkii Butter,Glyceryl Stearate,Panthenol,Betaine,Dimethicone,Oiea Europaea Oil,Allantoin,Polysorbate-60,Carbomer,Xanthan Gum,Parfum,Triethanolamine,Tocopheryl Acetate,Hyaluronic Acid,Methyl Paraben,Propyl Paraben,Creatine,Tetrasodium Edta,Phenoxyethanol,Caprylyl Glycol,Sorbic.

成分:去离子水,甘油,辛酸/葵酸三甘油酯,肉豆蔻酸肉豆蔻酯,乳木果油,硬脂酸甘油酯,泛醇,甜菜碱,聚二甲基硅氧烷,橄榄油,尿囊素,聚山梨醇酯-60,卡波姆,汉生胶,香精,三乙醇胺,生育酚乙酸酯,透明质酸,对羟基苯甲酸甲酯,对羟基苯甲酸丙酯,肌酸,乙二胺四乙酸四钠,苯氧乙醇,辛二醇,山梨酸。

Ingredients:water,glycerin,caprylic/capric triglyceride, cetyl alcohol ,propylene glycol,glyceryl stearate,panthenol,betaine dimethicone,simmondsia chinensis, rosa rugosa flower extract,allantoin,carbomer,parfum,triethanolamine,tocopheryl acetate,methyl paraben,propyl paraben,creatine,tetrasodium edta,phenoxyethanol,caprylyl glycol,sorbic.

成分:去离子水,甘油,辛酸/葵酸三甘油酯,鲸蜡醇,丙二醇,硬脂酸甘油酯,泛醇,甜菜碱,聚二甲基硅氧烷,霍霍巴油,玫瑰花提取液,尿囊素,卡波姆,香精,三乙醇胺,生育酚乙酸酯,对羟基苯甲酸甲酯,对羟基苯甲酸丙酯,肌酸,乙二胺四乙酸四钠,苯氧乙醇,辛二醇,山梨酸。

To synthesize the octreotide, Phe-Leu-Glu-Glu-Leu and C_(15)H_(31)-CO-Lys-Thr -Thr-Lys-Ser peptides, the strategies are as followings: Fmoc- group as protective group for α-NH_2; TBTU, DIEA and HOBt as coupling reagent; and ethanedithiol -phenol - thioanisole - H_2O - TFA ( 2.5:5:5:5:82.5 , V/V ) as cleaving solution.

采用Fmoc固相合成法,以苯并三哗四甲基脲四氟硼酸盐、二异丙基乙胺和1-羟基苯骈三氮唑为缩合剂;苯酚—乙二硫醇—苯甲硫醚—水—三氟乙酸(5:5:2.5:5:82.5,V/V)为切割试剂,合成了奥曲肽、Phe-Leu-Glu-Glu-Leu及C_(15)H_(31)-CO-Lys-Thr-Thr-Lys-Ser三种小分子多肽,并对奥曲肽的合成规模进行了放大。

In these components, 2-methyl-1-propanol, ethyl acetate, 3-methyl-1- propanol, 2,3-butanediol, phenylethyl alcohol, butanedioic acid diethyl ester, ethyl hydrogen succinate, 2-hydroxy-ethyl propanoic acid and 4-hydroxy-benzeneethanol were main aroma components, these volatile componds provided the typical sensory style of wine.

其中,2-甲基-1-丙醇、乙酸乙酯、3-甲基-1-丙醇、2,3-丁二醇、2-羟基丙酸乙酯、苯乙醇、丁二酸二乙酯、乙基-氢化琥珀酸和4-羟基苯甲醇等成分构成了葡萄酒的主体香气,这些主体香气与其他风味成分一起构成葡萄酒的典型风味特征。

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