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In this dissertation, we choosed anisole as starting material, via chloromethyla tion, cyanogenation, to prepare methoxybenzeneacetonitrile, then fractionated in a fractionating tower, and finally...

本论文也对两步的反应条件进行了探索,获得了比较理想的反应条件。文中还对对甲氧基苄氯自聚的原因与机理进行了探讨,并找到了比较理想的阻聚剂,使得粗品收率提高了10%。

A series of novel dendrons with 1,3,5-triazine structure were synthesized by convergent strategy using cyanuric chloride, p-hydroxyazobenzene,β-naphthol, 1-hydroxyanthraquinone, 3,5-dihydroxybenzyl. They were the first generation p-phenyl-azo-phenyloxy-terminated dendron G1.0, the first generation naphthyloxy-terminated dendron G1.0, the first generation naphthyloxy-terminated and 1-anthraquinonoxy-cored dendron G, and the second generation naphthyloxy-terminated dendron G2.0.

以对羟基偶氮苯、β-萘酚为端基,三聚氯氰、3,5-二羟基苄醇为支化单体,1-羟基蒽醌为核心,用收敛法合成了一系列新型结构的含均三嗪环的树枝块:第一代端基为偶氮苯的树枝块G1.0、端基为萘氧基的树枝块G1.0、端基为萘氧基、中心为蒽醌的树枝块G、第二代端基为萘氧基的树枝块G2.0。

It is to say that the patch of RAFT agent on the hairy chains.PS particles with the shell of copolymer of styrene and vinylbenzyl chloride were prepared by similar seeded and starved addition processes. RAFT agent with carboxyl end-group attached on the shell surface of PS particles by group reaction. Adding NIPA and photo-initiator into the continuous phase of polymerization system, hairy PNIPA were obtained.

最后,以表面负载一层乙烯基苄氯的亚微米级单分散聚苯乙烯微球为基质,将水溶性RAFT试剂与聚苯乙烯微球表面的官能团反应以负载到其表面,再在连续相中直接引入NIPA和光引发剂,RAFT聚合得到PNIPA毛发。

Moreover, the principle of the p-methoxybenzyl chloride polymerism and its cause have been analysised in this dissertation.

文中还对对甲氧基苄氯自聚的原因与机理进行了探讨,并找到了比较理想的阻聚剂,使得粗品收率提高了10%。

Methyl-2,3,5,6-tetrafluoro-benzene methanol was synthesized by chlorination, acylation, fluorination, esterifica- tion, reduction, bromization, reduction from terephthalic acid. Tefluthrin was obtained from-(1RS,3RS)-3-(2-chloro-3,3,3-trifluoro-1-propenyl)-2,2-dimethyl cycolpropa-necarboxylate acid by reacting with 4-methyl-2,3,5,6-tetrafluoro-benzene methanol.

以对苯二甲酸为原料,经氯化、酰氯化、氟化、酯化、还原、溴化、还原七步反应合成了4-甲基-2,3,5,6-四氟苄醇,甲基苄醇与-(1RS,3RS)-3-(2-氯-3,3,3-三氟丙-1-丙烯基)-2,2-二甲基环丙甲酸一步酯化合成了七氟菊酯。

N-Carbobenzoxy-L-homoserinelactone was prepared via N-alkylation reaction of L-methionine and iodoacetamide with benzyl chloroformate as amino protecting agent.

以L-蛋氨酸为原料,氯甲酸苄酯为氨基保护试剂,与碘乙酰胺(I2微量)内酯化反应,合成N-苄氧羰基-L-高丝氨酸内酯。

Aqua, Sorbitol, PPG-1 PEG-9 Lauryl glycol ether, Hydrolyzed elastin, Hydrolyzed wheat gluten, Hydrolyzed collagen, Hydrolyzed glycosamino-glycans, Humulus lupulus, Propylene glycol, Triethanolamine, Sodium hydroxide, Carbomer, Maris limus extract, Ostrea extract, Imidazolidinyl urea, Parfum, Benzyl salicylate, Coumarin, Alpha isomethyl ionone, Hexyl cinnamal, Buthylphenylmethylpropionate, Linalol, Methylisothiazolinone, Methylchloroisothiazolinone.

水,山梨醇, PPG 公司- 1聚乙二醇- 9十二烷基醇醚,水解弹性蛋白,水解小麦面筋蛋白,水解胶原蛋白水解粘多糖,多聚糖,啤酒花提取物花,丙二醇,三乙醇胺,氢氧化钠,卡波姆,马里斯提取物,牡蛎提取物,咪唑烷基脲,香水,水杨酸苄酯,香豆素,阿尔法 l 紫罗兰酮,己基肉桂醛,丁苯基甲基丙醛,芳樟醇,甲基异噻唑啉酮,甲基氯异塞唑晽酮。

OBJECTIVE To study the specific absorptivity and the formation ratio of ampicillinum natricum and p nitrophenol charge transfer compound.

目的 研究氨苄西林钠与对硝基苯酚形成电荷转移化合物的表观百分吸收系数、形成比及不经分离测定注射用氨氯青霉素钠中氨苄西林钠的含量的方法。

We screened a set of Lewis base organocatalysts derived from chiral pipecolinic acid and tert-butanesulfinamide for the reduction of-N-Cbz-1- phenylpropenamine, including newly designed ones and some of those previously developed in our lab. However, only moderate stereoselectivities, albeit high yields were obtained.

在本课题组前期研究的基础上,我们筛选并设计了一系列以手性哌啶酸和叔丁基亚磺酰胺为母体的有机小分子路易斯碱催化剂,它们能催化三氯氢硅对-N-苄氧羰基-1-苯基丙烯胺的不对称还原,获得很高的收率和中等的对映选择性,并且具有很好的底物普适性。

All of the tripodal schiff base ligands and their complexes were characterized.

以三乙醇胺、巯基苯胺、巯基乙胺为初始原料,设计合成了六个三脚架结构的化合物,其合成路线如下:三乙醇胺与氯化亚砜反应得到三(2-氯乙基)胺(1),然后与巯基苯胺或巯基乙胺在碱性条件下反应生成三脚架结构的三{[2-(2-氨基苯基)硫代]乙基}胺(2)或三{[2-(2-氨基乙基)硫代]乙基}胺(3),然后再与水杨醛、2-甲酰基-8-羟基喹啉(8)、2-甲酰基-8-苄氧基喹啉(7)反应得到六种新型的含硫西佛碱化合

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Now, however, all children continue in "comprehensive" schools, and the eleven-plus determines which courses of study the child will follow.

然而现在,所有的孩子都要在综合学校继续学习,所以这次考试只是决定他们将要学习哪些课程。

Cultivatable land , and led to a general recognition that development must not be carried at the cost of agriculture .

城区的迅速扩大在很多情况下侵占了宝贵的可耕地,使人们普遍认识到发展不能以牺牲农业为代价。

Detailed Intrinsic Reaction Coordination calculations were carried out to guarantee the optimized transition-state structures being connected to the related tautomers.

同时,做了详尽的内禀反应坐标计算,以保证所得到的过渡态连接相应的始末异构体。