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Ce2(SO4)3 was used as an inexpensive and effective catalyst for the Friedel-Crafts alkylation of aromatic compounds with benzyl alcohol s, allyl alcohols and benzyl chlorides.

硫酸亚铈作为一种便宜的和有效的催化剂催化芳香化合物与苄基醇、烯丙醇类化合物和苄基氯的傅-克烷基化反应。

Ce2(SO4)3 was used as an inexpensive and effective catalyst for the Friedel-Crafts alkylation of aromatic compounds with benzyl alcohols, allyl alcohol s and benzyl chlorides.

硫酸亚铈作为一种便宜的和有效的催化剂催化芳香化合物与苄基醇、烯丙醇类化合物和苄基氯的傅-克烷基化反应。

Study prepared method of dimethylbenzyl carbinol and seek the best technologic conditions and craft route of dimethylbenzyl carbinol.

研究二甲基苄基甲醇制备方法,寻找制备二甲基苄基甲醇的最佳工艺条件和工艺路线。

A new chiral quaternary ammonium salt 1a was synthesized by the reaction of cinchonine and(2,4,6-)trimethyl benzyl chloride.Etherification between 1a and benzyl bromide,allyl chloride,or methyl give corresponding etherified quaternary ammonium salts 1b,1c,and 1d.

由辛可宁和2,4,6-三甲基苄氯,合成了一种新的手性季铵盐(1a),并进一步用苄基溴、碘甲烷和烯丙基氯对分子中的羟基进行醚化,得到相转移催化剂1b、1c和1d。

Under the microwave radiation, makes the catalyst with the potassium iodide,The sodium hydroxide makes the neutralization agent, synthesized the phenmethyl -2- naphthyl ether, take 2- naphthol and the chlorination animal pen as the raw material, Uses the single factor cut-and-try method, To a reactant mole of ratio, the catalyst and the solvent amount used, the microwave power, the radiation time and so on have conducted the research to the product receiving rate influence.

在微波辐射下,以2-萘酚和氯化苄为原料,用氢氧化钠作碱剂,碘化钾作催化剂,水-DMF为溶剂合成了苄基-2-萘基醚;采用单因素实验法,对反应物的摩尔比、催化剂及溶剂用量、微波功率、辐射时间等因素的影响进行了研究。

With trimethyl,4-dodecylbenezyl ammonium chloride and 18-crown-6 as pase-transfer catalysts, the azidation of polyepichlorohydrin in poly and H2O were studied. The reaction discipline and mechanism were discussed. The results show that the system with trimethyl, 4-dodecylbenezyl ammonium chloride as phase transfer catalyst and PEG as medium is a safe and effective approach to glycidyl azide polymer preparation, and azidational ratio of PECH can reach 97% above within 15 h.

研究了氯化十二烷基苄基三甲基铵和18-冠-6为相转移催化剂时端羟基聚环氧氯丙烷在聚环氧乙烷和水为介质中的叠氮化反应,探讨了反应规律和反应机理,结果表明:以PECH为介质,十二烷基苄基三甲基氯化铵(TMDA-1)为相转移催化剂的反应体系,可在15h内使PECH叠氮化转化率达到97%以上,无主链断裂等副反应,是一条较为安全快速的制备叠氮粘合剂的方法。

Chapter 4: Synthesis of 1,5-diary 1-1,4-pentadien-3-ones from acetone or benzalacetone with aromatic aldehydes results in 86-97% yield with potassium hydroxide as catalyst under ultrasound irradiation in 5-60min.

为合成氰基环己醇找到一条方便高效的合成方法。第四章:研究了超声辐射下,以氢氧化钾为催化剂,芳香醛与丙酮及亚苄基丙酮之间反应合成1,5-双苄基-1,4-戊二烯-3-酮。

Based on broad information collection, author compared and studied on the old synthesis process, and proposed the better process that started from benzyl chloride, then according to the sequence of " synthesis of benzylamine, synthesis of N-benzyl-N--acetamine, synthesis of 2-chloro-5-methylpridine ,2-chloro-5-trichloromethylpyridine,2-chloro-5-trifluropyridine " five steps to get the final product, CTFP.

本文在查阅大量文献资料和对2-氯-5-三氟甲基吡啶合成路线进行分析比较的基础上,提出了较佳合成路线,即以氯化苄为原料,合成的反应步骤为&苄胺&合成、&N-苄基-N--乙酰胺&合成、&2-氯-5-甲基吡啶&合成、&2-氯-5-三氯甲基吡啶&合成、&2-氯-5-三氟甲基吡啶&合成五步。

A process for preparingp-fluo-2-(2-methyl-3-propionyl)-4-oxy-N,3-diphenyl-phenylbutylamide includes such steps as Friedle-Craft acylating of newly prepared phenylacetyl chloride and fluorobenzene under catalysis of AlCl3 to obtain 4-fluoro-phenylbenzyl ketone, brominating at carbonyl alpha position under catalysis of less AlCl3 to obtain alpha-bromo-4-fluo-phenylbenzyl ketone, and condensing with isobutyryl acetanilide under action of sodium ethoxide.

本发明涉及一种制备对氟-2-(2-甲基-3-氧丙基)-4-氧-N,3-二苯基-苯丁酰胺(1)的方法,其包括以下步骤:新制的苯乙酰氯与氟苯在AlCl3催化下进行Friedle-Craft酰化反应,得到对4-氟-苯基苄基酮(4);化合物(4)在少量AlCl3催化下进行羰基α位溴化,得到α-溴-4-氟-苯基苄基酮(5);然后(3)异丁酰乙酰苯胺在乙醇钠作用下与化合物(5)进行缩合。

Several glycosyl phosphate and phosphonates, as inhibitors of AGPase, were synthesized.In the synthesis of β〓-6 linked oligosaccharide phosphonates, A new method was developedfor preparation of 〓,6-〓-di-acetyl-2,3,4-〓-tri-benzyl-D-hexoses by acetylation of benzylatedmethyl glycosides in high yield under the conditions of 〓 and cat.〓.

合成了一些磷酸酯及其类似物作为嗜热AGPase的抑制剂,在研究β 1-6连接的寡糖膦酸酯的合成中,发现了制备1,6-〓-二乙酰基-苄基保护糖的新方法:苄基保护的糖苷在醋酐和催化量的硫酸作用下,在0℃反应进行7-10 min,可以选择性、高收率地得到此化合物。

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Now, however, all children continue in "comprehensive" schools, and the eleven-plus determines which courses of study the child will follow.

然而现在,所有的孩子都要在综合学校继续学习,所以这次考试只是决定他们将要学习哪些课程。

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Detailed Intrinsic Reaction Coordination calculations were carried out to guarantee the optimized transition-state structures being connected to the related tautomers.

同时,做了详尽的内禀反应坐标计算,以保证所得到的过渡态连接相应的始末异构体。