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Methods:Dehydration of D-mannitol,followed by a reaction sequence of selective protection,benzylation,deprotection,tritylation,benzylation and removal of the trityl group,afforded the title compound.

以D-甘露醇为原料构建2,5-脱水-3,4,6-O-三苄基-D-葡萄糖醇的手性分子骨架,通过选择性地对多羟基的保护和脱保护达到对产物分离的目的。

This paper has studied preparation of Grignard reagents under phonochemistry and optimum technologic conditions is: the power of ultrasonic is 500W and frequency is 250KHZ, having twelve energy conversion devices, water bath temperature being 20C, solvent being THF,unstirred.

本文探讨了超声波合成格利雅试剂的机理,研究了声化学法制备格利雅试剂氯化苄基镁的最佳工艺条件为:在超声波的功率为500W,频率为25KHZ,有12个换能器的条件下,水浴温度为20℃,以THF为溶剂,不搅拌。

Benzylmercaptide, antimony trioxide have been used to synthesize antimony tri with 90%,95% of the yield respectively, and the optimal synthetic conditions were studied.

苄基硫醇、三氧化二锑等为原料,研究了三锑的最佳合成工艺条件,产率分别达到90%和95%。

N-Benzylacryl amide was synthesized using acrylonitrile and benzyl alcohol as raw materials and sulfuric acid as catalyst.

以丙烯腈和苯甲醇为原料,浓硫酸作催化剂,合成了N-苄基丙烯酰胺。

A new complex, [(C6H6N2O)2Co(H2O)2] Br2 was prepared from picolinamide, Co(NO3)2 and benzyl bromide, and characterized by X-ray diffraction.

用皮考林酰胺、六水合硝酸钴和苄基溴反应制得一种新配合物[(C6H6N2O)2Co(H2O)2]Br2,通过红外光谱、元素分析及X射线晶体衍射对化合物进行了表征。

QN 〓PHAL,〓PHAL and 〓PHAL were quaternized by refluxing with benzyl bromide to give ligands 8, 9 and 10 respectively. 2. The chiral ligands were applied to the AD reaction of olefins with NMO as co-oxidant and PEG (400 MW) or PF〓 as reaction media.

以奎宁和奎尼定为原料分别与1,4-二氯-2,3-二氮杂萘反应制备〓PHAL和〓PHAL,然后通过〓PHAL、〓PHAL及〓PHAL与苄基溴的季铵化反应制备单季铵盐手性配体8、9和10。

Aim To study the synthesis of phase transfer catalyst-triethyl benzyl ammonium chloride and its catalytic activity in phase transfer catalytic reactions.

目的 研究相转移催化剂TEBAC(Triethyl Benzyl Ammonium Chloride,三乙基苄基氯化铵)的合成以及在相转移过程中的催化性能。

The feasibility of electrocarboxylation of benzyl chloride has been investigated at silver cathode in CO2-saturated room-temperature ionic liquid 1-butyl-3-methylimidazolium tetrafluoroborate (BMIMBF4) solution for the first time.

在饱和了CO2的室温离子液体中,首次在银电极上研究了苄基氯电羧化的可行性。

Separation of racemic mixtures of benzyl glycidyl ether was achieved with HPLC by using Chiralcel OD as chiral stationary phase and hexane/2-propanol mixture of different ratios as eluents.

在 Chiralcel OD多糖类手性固定相上,以各种不同配比的正己烷-异丙醇为洗脱剂,对苄基缩水甘油醚的外消旋体进行对映体拆分,考察了不同洗脱剂配比、柱温和流速对分离度和出峰时间的影响。

Structural differences among the three gelators are only in the varied amount of methyl groups on the benzene ring.

从分子结构的差异、亲溶剂作用、分子几何构型、相转变热焓以及溶剂极性等方面研究了三种亚苄基山梨醇衍生物凝胶剂在有机溶剂中的自组装和凝胶化机理。

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推荐网络例句

Now, however, all children continue in "comprehensive" schools, and the eleven-plus determines which courses of study the child will follow.

然而现在,所有的孩子都要在综合学校继续学习,所以这次考试只是决定他们将要学习哪些课程。

Cultivatable land , and led to a general recognition that development must not be carried at the cost of agriculture .

城区的迅速扩大在很多情况下侵占了宝贵的可耕地,使人们普遍认识到发展不能以牺牲农业为代价。

Detailed Intrinsic Reaction Coordination calculations were carried out to guarantee the optimized transition-state structures being connected to the related tautomers.

同时,做了详尽的内禀反应坐标计算,以保证所得到的过渡态连接相应的始末异构体。