芳基化

The sulfonated polyetherketone with cardo group films made by different sulfonation degrees and solvent evaporation shows different microstructure by PALS and atomic force microscopy.

利用对高分子材料纳米量级自由体积空洞极为灵敏的正电子探针，并辅之原子力显微镜法研究了磺化及溶剂蒸发对酚酞侧基聚芳醚硐膜制备的影响。

Mannich reaction occurred directly between arylamine and pyrroli- zinone on hydrogen chloride/ethyl alcohol solution.

芳胺和吡里酮在氯化氢乙醇溶液中直接发生Mannich反应，但胺甲基化不是发生在羰基的α-位，而是发生在吡咯结构部分的5-位。

Myristic monoethanolamide ammonium sulfatewas synthesized from myristic acid and monoethanolamide with sulfamic acid as sulfating agent .

在芳烃类溶剂与羰基化合物催化剂存在下，以肉豆蔻酸和乙醇胺为原料，氨基磺酸作硫酸化剂，制备了肉豆蔻酸单乙醇酰胺硫酸酯铵盐。

heological properties at a low shear rate range(10-2-10s-1) and the glass transition temperatures for PEK-C with different moleCular weithts have been studied by using a cone/plate rheometer and DSC' The activation energy for melt flow increases with Mw The dependence of Tg on molecular weight exhibits two linear range and the value of nitersect agrees with the critical molecular weight , Mc' which is first reported for PEK-C' Mc value obtained according to η0 is about 8× 104 g/mol and the relation between Mc and temperature was dis-cussed.

用锥权流变仪及DSC的方法研究了5种不同分子量的酞侧基聚芳醚酮在低剪切速率区（10－2－10s－1）的流变行为及其分子量与玻璃化转变温度的关系。结果表明，样品的粘流活化能随分子量的增加而增大，Tg随分子量的变化是二个线性区，其交点值与所求的样品的临界分子量值相对应。利用测得的零剪切粘度值（η0）首次求得了PEK—C的临界分子量值。同时也讨论了Mc与温度及η0和Tg与分子量的关系。

Breath, muscle contraction of the buttocks; arch body, as far as possible to hold his head, right leg straight towards the ceiling (peg-leg knee in order to avoid muscle tension).

呼气，收缩臀部肌肉；拱起身体，尽量抬起头来，右腿伸直朝向天花板（膝微屈，以避免肌肉紧张）。

The cost of moving grain food products was unchanged from May, but year over year are up 8%.

粮食产品的运输费用与5月份相比没有变化，但却比去年同期高8％。