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Result The results showed that its components were quite complex, and 89 organic compounds were identified. There were 72 kinds of oxygen-containing organic compounds which included esters, phenols, aethers, ketones and alcohols in the depolymerization product, small amounts of alkanes, alkenes, arenes, thiophenol and nitrogen-containing organic compounds were also detected, which showed that characteristics of the product with high oxygen content, low nitrogen and sulphur content.

结果]超临界乙醇解聚产物成分十分复杂,GC/MS分析鉴定出89种有机化合物,其中72种为含氧化合物,主要有酯、酚、醚、酮和醇等,还检测出少量烷烃、烯烃、烃、苯硫酚和含氮化合物,反映了解聚产物的高含氧量和低含氮硫量的特性。

CH3OH could attack the phosphor atom in 1,3,2-dioxaphopholane of compiound (1) to give O-methyl O-hydroxyethyl-O-phthalimidoethyl thiophosphate in 85% yield; in the presence of potassium hydroxide aryl selenol could attack the carbon atom in 1,3,2-diox-aphopholane of the cyclic phospholipid conjugate of N^1-(2-furanidyl)-N^3--5-fluorouracil to give the corresponding product of ring-opening in high yields.

在室温下,以异丙醇作溶剂,苯硒酚与化合物2不反应。在氢氧化钾存在下,以异丙醇/水作溶剂(体积比20:1,在室温下,硒酚可以有效地进攻中化合物2中1,3,2-二氧磷杂环戊烷中的碳原子生成相应的开环产物。按照这一反应条件,顺利实现了硒酚对N^1-(2-呋喃基)-N^3-羟烷基-5-氟脲嘧啶硫代环甘油磷脂缀合物的亲核开环,生成甘油骨架的端碳原子上带有硒基新颖的磷脂核苷缀合物。

O-(1-Arylseleno-3-azido)isopropyl-O-2-(N3-tegafur)alkyl thiophosphate (3a~3f) were obtained via nu-cleophilic ring-opening of sodium azide to 2a~2f in dry DMF at room temperature, and their antitumor activities were tested.

以无水N,N-二甲基甲酰胺作溶剂,室温下,叠氮化钠中对2a~2f进行亲核开环,得到O-(1-硒基-3-叠氮基)异丙基-O-2-(N3-替加氟)乙基硫代磷酯。

The New York company said Friday that its internal investigation into possible bribery of foreign government officials, which began two years ago after a tipster mailed allegations to Chief Executive Andrea Jung, has expanded beyond China into four other international units.

这家总部位于纽约的公司上周五表示,对可能存在的向外国政府官员行贿的内部调查已经从中国子公司扩大到另外四个国际子公司。这项内部调查开始于两年前,在那之前雅的首席执行长钟彬娴收到一封线人的举报邮件。

He's trying to win her over.

他在努力赢得她的心。

The joint toxicity was evaluated by different methods, including toxicity unit,additive index, similarity parameter and mixtures toxicity index. The results show that the binary joint effects of phenol and toluol mixed with SDS are synergistic, while the binary joint effect of SDS and nitrobenzene is antagonistic. The environment risk of some compounds will be enhanced because of the joint of SDS.

研究结果表明: 4种不同的评价方法对SDS与取代烃苯酚、甲苯和硝基苯的联合效应评价结果具有较好的一致性,即SDS与苯酚、甲苯的二元混合体系的毒性表现为不同程度的协同作用,而与硝基苯则表现为弱拮抗作用;对环境存在风险性的阴离子表面活性剂SDS,当与一些有毒有害物质共存时会增加该类物质的环境风险性。

A copper-chromium bimetal plate having a surface chromium layer of 2 μ was coated with a 4 percent solution in toluol of a light-sensitive polymer containing light-sensitive aryl sulphonylazide groups and a minor amount of hydroxyl groups attached to the polymer backbone.

阿铜铬双金属板具有2μ铬层表面涂有在一轻甲苯百分之四解决敏感的聚合物含有光敏感sulphonylazide团体和一个连接到聚合物骨架羟基小数额。

Phenyl or m -tolyl selenoamides reacted with functionalized α-haloacetic acid in 1∶1 or 1∶2 molar ratio with no catalyst in various alcohols to undergo a selenium transfer reaction. This reaction in dif-ferent molar ratios furnished the same C—Se—Se—C coupling products with a special structure bis diselenide. A new and facile method for synthesis of such bis(alkoxycarbonyl-methyl) diselenides with the advantages of mild reaction conditions, high yields, easy availability of starting materials and good chemical selectivity was provided.

基硒代酰胺与氯乙酸在各种醇中无催化剂下以1∶1和1∶2的比例投入,发生硒转移反应,不同原料投入比下的反应生成了同一种C—Se—Se—C偶联产物——具有多功能团的二烷氧羰基甲基二硒醚,提供了一种新的合成二烷氧羰基甲基二硒醚的简便方法,且反应具有条件温和、产率高、原料易得和选择性好等优点。

TORSION'S come out only in the 5 year have been self-identity abroadly ,afterward the France YABANGinternationalization cosmetic study institution come into existence in Hongkong ,meanwhile Hongkong yabang internationalization cosmetic study institution being developed deeply market in Asia and Asian's the skin specialty and demand of the bazaar ,and so , to open up a product that TORSION of contain sweetness essence oil.

TORSION问世不到5年得到了市场的广泛认同,随后雅邦国际化妆品研究机构在香港成立"香港雅邦国际化妆品研究机构"开始大力拓展亚洲市场,并结合亚洲人皮肤特点和市场需求,开发出了饱含非常注重精良选材的香精油在内的TORSION透香品牌。

Mine tremblingly; thy dark eyes threw

浇洒在垂危的花朵,你的

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But we don't care about Battlegrounds.

但我们并不在乎沙场中的显露。

Ah! don't mention it, the butcher's shop is a horror.

啊!不用提了。提到肉,真是糟透了。

Tristan, I have nowhere to send this letter and no reason to believe you wish to receive it.

Tristan ,我不知道把这信寄到哪里,也不知道你是否想收到它。