色质

In present study, a liquid-liquid extraction method was employed to extract the volatile components in mulberry fruit sparkling wine. The analysis with gas chromatography-mass spectrometry detected 69 peaks, among which 63 volatile components were identified. The first 9 volatile components with high relative content were benzyl alcohol, 2-methyl-1-butanol, mono-(2-ethylhexyl)-1, 2-benzene dicarboxylic acid, 3-methyl-1-butanol, toluene, acrylic acid butyl ester, 1H-indole-3-ethanol, isodecyl octyl phthalate and decyl octyl phthalate.

采用液－液萃取法提取桑椹汽酒中的挥发性成分，经气相色谱－质谱联机分析，共检测出69个峰，鉴定出63种挥发性化合物，其相对含量排在前9位的挥发性化合物分别是苯乙醇、2-甲基－1-丁醇、1，2-苯二酸单（2-乙基）己酯、3-甲基－1-丁醇、甲苯、丙烯酸丁酯、1H-吲哚－3-乙醇、邻苯二甲酸异癸基辛基二酯、邻苯二甲酸癸基辛基二酯。

This study developed a new method on the determination of carcinogenic disinfection by-products-trace dichloroacetic acid and trichloroacetic acid in tap water by ion chromatography-electrospray-tandem mass spectrometry(IC-ESI-MS/MS).

建立了一种采用离子色谱-串联电喷雾四级杆质谱联用技术检测自来水中可致癌的饮用水消毒副产物二氯乙酸和三氯乙酸的方法。

MethodsThe constituents of volatile oil from Dictamnus dasycarpus was investigated by SPME/GC/MS.

方法利用固相微萃取/气相色谱/质谱联用技术对白鲜皮的挥发油成分进行了研究。

ObjectiveTo analyze constituents of volatile oil from Dictamnus dasycavpus.

作者：吴琴，叶冲，宋培浪，韩伟白鲜皮；，，挥发油；，，固相微萃取；，，气相色谱/质谱联用摘要：目的分析白鲜皮挥发油成分。

High performance liquid chromatography-photodiode array detection-elctrospray ionization mass spectrometry (HPLC-PAD-ESI-MS) method was used to determine secoisolariciresinol diglucoside qualitatively and quantitatively. Precision, stability, limits of quantification, SDG recovery and sample preparation method were studied.

采用高效液相色谱－二极管阵列检测－电喷雾质谱(HPIC-PAA-ESI-MS)法对开环异落叶松树脂酚二葡萄糖苷进行定性和定量检测，研究方法的精密度、稳定性、定量检测限及加样回收率，并考察样品制备方法对定量检测结果的影响。

The fish samples were cleaned up by Florisil, then analyzed by GC-EI-MS to determine eight phthalic acid esters, diethyl phthalate, dipropyl phthalate, dibutyl phthalate, butyl benzyl phthalate, dipentyl phthalate, dicyclohexyl phthalate, dihexyl phthalate and diethyl hexyl phthalate.

鱼肉样品以Florisil硅藻土层析柱净化后，经气相色谱-电子轰击离子源-质谱法分析其中8种邻苯二甲酸酯含量：邻苯二甲酸二乙酯、邻苯二甲酸二丙酯、邻苯二甲酸二丁酯、邻苯二甲酸丁基苄基酯、邻苯二甲酸二戊酯、邻苯二甲酸二环己基酯、邻苯二甲酸二己酯、邻苯二甲酸二(2-乙基己基)酯。

Six-factor and three-level orthogonal experimental design was used to optimize the SFE co nditions as guided by the content of total coumarins in the extract. Constituent s of the coumarins were analyzed by GC-MS, and their relative contents were det ermined by normalization method of areas.

采用正交试验设计方法，以提取液中总香豆素含量为考察指标，对总香豆素提取条件进行优化，并用气相色谱质谱联用技术对超临界样品进行分析鉴定，利用面积归一法测定其相对含量。

ConclusionThe method is reliable, stable and repeatable and can be used for the analysis of the volatile constitiuents of Evodia lepta leaves.

结论此方法稳定可靠，重现性好，可用于三叉苦叶挥发性成分的分析。三叉苦叶；挥发油；气相色谱-质谱联用

In this study was carried out in the greenhouse of Shandong Agricultural University,'Fragaria×ananassa Duch.

中文摘要：本研究在山东农业大学日光温室进行，以盆栽'丰香'和'罗莎'草莓为试材。采用顶空固相微萃取-气谱-质谱联用技术测定果实中芳香物质，DTNB比色法测定果实醇酰基转移酶活性。

A static headspace GC-MS method was used to detect sulfur in the fumatory Radix Bupleuri,the authentic samples free of sulfur was detected as reference.

运用静态顶空毛细管气相色谱-质谱联用技术进行检测市售柴胡是否经硫黄熏蒸，并从产地采集未经硫黄熏蒸的柴胡作为阴性对照药材与市售柴胡进行比较。

This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。