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The main collagens in skin are type I and III. In this research, total collagens were separated from rat skin by enzymatic digest and acetum methods. The collagens were denatured at 60℃ and digested with trypsin. Characteristic peptides typical for collagen type I and III were identified with high performance liquid chromatography/mass spectrometry.

哺乳动物皮肤真皮中胶原蛋白含量约为70%,主要为是I型、III型胶原蛋白,本实验利用稀酸溶解和酶法提取了大鼠皮肤中的总胶原蛋白,将胶原蛋白粗提品在60℃变性后用胰蛋白酶进行降解,液相色谱/质谱联用法分析了两种胶原蛋白的特征多肽,利用特征多肽比较了不同生长期大鼠皮肤中I型和III型胶原蛋白相对含量。

The aliquot was determined and confirmed by gas chromatography-negative chemical ionization mass spectrometry using external standard method.

样品中三唑醇残留物由正己烷饱和的乙腈(含1%冰醋酸)提取,加入无水硫酸镁与无水醋酸钠振荡促使提取液分层后进行固相分散萃取净化,用气相色谱-负化学离子源质谱法进行测定与确证,外标法定量。

Methods Detecting bile acid metabolites with high performance liquid chromatography-mass spectrometry to serum samples of five patients of consuming amanita verna.

采用高效液相色谱联合质谱技术检测了5例不同预后的白毒伞中毒患者的多种胆汁酸代谢产物。

Foliaceous egg form, foliaceous radical department is small inclined, xie Se has green, amaranthine, or green ribbon is violet dizzy wait for change; Provide stipule a pair, film is qualitative.

叶卵形,叶基部微斜,叶色有绿、紫红、或绿色带紫晕等变化;具托叶一对,膜质。

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High performance liquid chromatography, carbon-13 nuclea magnetic resonance, chemical ionization mass spectrometry and gas chromatography with flame ionization detection have been employed for the identification and quantitative deter mlnation of the epimers of amygdalin.

高效液相色谱法、carbon-13 nuclea 磁场共振电离质谱、化学品与气相层析法,以氢火焰离子化检测被用来识别和定量的威慑 mlnation差向异构体的苦的。

Simultaneous Scan-Selected ion monitoring mode is a new improvement method of data acquisition of gas chromatography mass spectrometry. The determination method of alkaloids in tobacco was established by Scan-SIM of GC/MS. Nicotine, nornicotine, anabasine and anatabine were determined with Scan mode, and myosmine, nicotyrine, 2,3'-Bipyridyl and cotinine were determined with SIM mode.

建立了应用气相色谱-质谱全扫描-选择离子监测数据采集方式同时测定烟草中8种含量相差较大的生物碱的方法,采用Scan模式分析烟碱、降烟碱、新烟碱、去氢新烟碱,同时采用SIM模式分析麦斯明、二烯烟碱、2,3′-联吡啶、可铁宁。

In this review, the application of anion exchange chromatography to pharmaceutical plasmid analysis was reviewed.

本文对阴离子交换色谱在药用质粒分析方面的应用与研究进展进行综述。

Gas chromatograpHy/mass spectrometry was used to analyze the chemical constituents of TKC antiknock .

采用气相色谱质谱联用技术分析抗爆剂 TKC辅助剂的成分。

The auxiliaries of gasoline antiknock additive TKC were analysed by means of gas chromatography/mass spectrometry.

采用气相色谱/质谱联用技术对汽油抗爆剂 TKC的辅助剂进行了组分分析。

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Yang yinshu、Wang xiangsheng、Li decang,The first discovery of haemaphysalis conicinna.

1〕 杨银书,王祥生,李德昌。安徽省首次发现嗜群血蜱。

Chapter Three: Type classification of DE structure in Sino-Tibetan languages.

第三章汉藏语&的&字结构的类型划分。