色环

A method is introduced for quantitative determination of cinmethylin by gas chromatography on 5 % ov - 101 packed column and flame - ionigation detector using dipropyl phthalate as internal standard The method was simple, rapid, accurate and practical.

采用气相色谱法， 5％ OV— 101填充柱和氢火焰离子化检测器，以邻苯二甲酸二丙酯为内标，对环庚草醚进行定量测定。

The Pt-Sn/CCA and Pt-Sn/γ-Al2O3 catalysts were prepared by impreg nation method. The acti vity at 300 ℃ or 350 ℃ and the stability at 450 ℃ of the catalysts were evalu ated, and the structure of Pt-Sn/CCA catalyst was generally studied.

采用共浸法制备了Pt-Sn/CCA催化剂，利用在线色谱微反实验装置评价了此类催化剂对甲基环己烷脱氢反应的活性和抗炭性能，初步研究了Pt-Sn/CCA催化剂的物理化学结构。

A separation model of ionizable and neutral enantiomer s with cyclodextrin-sodium dodecyl sulphate micellar electrokinetic chromatography was established.

建立了环糊精-十二烷基硫酸钠胶束电动色谱中可电高及电中性-光学异构体的分离模型。

Modern systems consist of one or more computer-controlled metering pumps that can be programmed to vary the ratio of mobile phase components, as is required for gradient chromatography, or to mix isocratic mobile phases (i.e., mobile phases having a fixed ratio of solvents).

后者有一个装样品瓶的转盘或者架子，瓶子顶部用可以穿孔的隔膜或者塞子密封，和一个注射装置来把样品从样品瓶转移到定量环，从那里注入到色谱分离系统。

A reversed-phase high performance liquid chromatographic method was established for determination of isothiocyanates in human urine , which used the reaction of propyl isothiocyanate with 1,2-benzenedithiol as reference instead of the synthesis of 1,3-benzodithiole-2-thione.

省去合成1，3 苯二硫杂环五烯 2 硫酮这一步骤，直接用异硫氰酸丙基酯与1，2 苯二硫酚反应作标准，建立了尿液中异硫氰酸酯的反相高效液相色谱测定方法。

The present doctoral dissertation was carried out to study the chemical constituents isolated from stems of two medicinal schisandraceous plants.34 compounds were isolated from the ethanol extracts of the stems S.henryi collected in the Jiangxi province by various column chromatographies.27 of them were identified on the basis of spectral analysis.There are 18 lignans,(including 5 dibenzocyclooctadienes,6 aryltetralins,2 tetrahydrofurans,3 diarylbutanes,2 other lignans),3 flavanols,2 glyceroesters,1 naphthoquinone,1 xanthine and 2 steroids,of which 6 compounds were new compounds,and 7 compounds were isolated from this family for the first time.

采用多种色谱技术进行分离纯化，从翼梗五味子藤茎的乙醇提取物中分离到34个化合物，综合运用现代波谱学技术鉴定了27个化合物，包括木脂素类化合物18个(其中联苯环辛烯类木脂素5个，芳基四氢萘类木脂素6个，四氢呋喃类木脂素2个，二芳基丁烷类3个，其他类型木脂素2个)，黄烷醇类化合物3个，甘油酯类化合物2个，萘醌类化合物1个，黄嘌呤类化合物1个，甾体类化合物2个，其中，5个为新化合物，7个为本科首次报道。

The results indicated that the decoloration of three orcein dyes on EPI-DMA/Bt were much better than on Na-Bentonites. The relationship between adsorptive capacity and equilibrium concentration fitted the isothermal adsorption equations of Langmuir and Freundlich. The adsorption dynamics followed the law of Langmuir equation.

结果表明，聚环氧氯丙烷二甲胺/膨润土对三种染料的吸附脱色能力明显大于钠基膨润土，平衡吸附量 q e与平衡浓度 C e之间的关系均符合Langmuir和Freundlich等温吸附模型，吸附动力学行为遵循Langmuir方程所述规律。

Determination of Polycyclic Aromatic Hydrocarbons in Drinking Water by Liquid-Solid Extraction and HPLC with Coupled Ultraviolet and Fluorescence Detection.

测定多环芳烃的饮用水中液固萃取和高效液相色谱耦合紫外线和荧光检测。

Determination of Polycyclic Aromatic Hydrocarbons in Drinking Water By b Liquid-Liquid Extraction and HPLC with Coupled Ultraviolet and Fluorescence Detection.

测定多环芳烃的饮用水中的B液液萃取和高效液相色谱耦合紫外线和荧光检测。

The corresponding thiochromanones were synthesized from β-arylthioethers of propionic acid under microwave irradiation in the presence of polyphosphoric acid. Their structures were confirmed by IR, 1H NMR, MS spectra and elemental analysis.

关于这些化合物合成曾有一些报道：以硫酚及卤代羧酸为原料在回流或超声作用下合成β-芳硫丙酸，芳硫丙酸在浓硫酸或磷酸作用下环化制备硫色满酮[1，2]。

Do you know, i need you to come back

你知道吗，我需要你回来

Yang yinshu、Wang xiangsheng、Li decang,The first discovery of haemaphysalis conicinna.

1〕 杨银书，王祥生，李德昌。安徽省首次发现嗜群血蜱。