色环

The results showed that Celtis julianae 'Aurea' belongs to chl-deficient type. The main cause of turning yellow was the blockage of chlorophyll biosynthesis which could be somewhere in the formation of Pchlide.

导致金叶珊瑚朴叶色金黄的原因是叶绿素的合成受阻，受阻部位可能在Mg插入卟啉环后合成原叶绿素酯时。

Objective To establish gas chromatographic method for determination of air methylcyclohexane in workplace.

目的 建立工作场所空气中甲基环己烷的气相色谱测定方法。

The data such as the Hα-spectrum-spectroheliographic observations, the Hα-chromospheric observations, etc., of a flare loop prominence which occurred on the western solar limb on 1981 April 27 have been obtained at Yunnan Observatory, Academia Sinica.

云南天文台摄取1981年4月27日太阳西边缘的一个耀斑环珥的H_α光谱太阳分光照像(S~2HG)和H_α色球照像等资料。

The recoveries of seawater and sediment are :naphthalene 73. 0% and 75. 3%, phenanthrene79. 2%and78. 0%, fluoranthene 88. 1% and 80. 7%, pyrene 73. 8% and 70. 2%, chrysene 77. 6% and 72. 8%, benzofluoranthene 87. 6% and 83.6%, benzo pyrene 120. 3% and 110. 0%, respectively.

通过对7种多环芳烃标准样品的高效液相色谱法的定性、定量分析，结果表明，该方法可有效分离PAHs，回收率较高，海水和沉积物中的回收率分别为：萘73.0％和75.3％，菲79.2％和78.0％，荧蒽88.1％和80.7％，芘73.8％和70.2％，屈77.6％和72.8％，苯并荧蒽87.6％和83.6％，苯并芘120.3％和110.0％。

The synthesis of 4,5,7-trichloroquinoline makes use of ethyl orthoformate, cyanoacetic ester and 3,5-dichloroaniline as the raw materials. The synthesis is completed by four steps: condensation, cyclization, hydrolyzation and chlorination. Several conditions concerned in the process are studied, the whole yield of 4,5,7-trichloroquinoline is about 53%, and the purity of it is about 96%. All the products are testified by IR, NMR and HPLC.

介绍了以3，5-二氯苯胺、原甲酸三乙酯和氰乙酸乙酯为原料，经过缩合、成环、水解和氯代4步反应制备4，5，7-三氯喹啉的方法，对相关的试验条件进行了考察，通过红外光谱、核磁共振谱和液相色谱对4，5，7-三氯喹啉的结构和纯度进行表征和测定，试验结果为4，5，7-三氯喹啉的纯度大于96%，总收率达到53%。

Keywords alkane; cyclane ;aliphatic alcohol;aliphatic ketone;gas chromatography retention index;molecule shape index;electrotopological state index

烷烃；环烷烃；脂肪醇；脂肪酮；色谱保留指数；分子形状指数；电性拓扑状态指数

To establish a method for determination of cyclopentadiene,dimethylformamide and N-methylpyrrolidone simultaneously in isoprene by GC.

用毛细色谱法建立异戊二烯中各组分定性分析方法及环戊二烯，N-甲基吡咯烷酮，N，N-二甲基甲酰胺的测定方法。

The UV and IR spectroscopic studies of the monomer films showed that the photoreaction ratio of monomer (about 50%) was higher than the corresponding photosensitive polymer (about 10%, PVCi). The polarized IR spectra proved that obvious anisotropic absorption was displayed in the irradiated photosensitive film. With polarizing microscopy method, we found that these kinds of photoalignment films exhibited good alignment ability, and the stability of the photoalignment film could reach about 100℃. 2 A photosensitive self-assembled monolayer was fabricated that contained photo-cycloadditable groups, such as, coumarin and cinnamate. The reaction process were detected by contact angle method because the IR absorption of monolayer was very weak. The photosensitive self-assembled monolayer promote uniform alignment of nematic liquid crystals by LPUV, and it thermal stability could reach about 130℃. 3 A cationic bolaform amphiphiles was synthesized that had two photosensitive double bonds, and can be polymerized by ultraviolet. A layer-by-layer self-assembled deposition film was prepared in aqueous solution by using this material and poly (sodium 4-styrenesulfonate). The UV-Vis. spectra proved that the multilayers film was uniform and layer-by-layer. When LPUV irradiated the film, the photopolymerizable double bond underwent [2+2] cycloaddition, and the production of the reaction distributed along the polarized direction of incident LPUV. Polarized UV-Vis. spectra indicated that the irradiated self-assembled multiplayer film was anisotropic, and the dichromic ration is about 0.09, it is higher than the spin-coating method of photosensitive polymer or monomer. We used this anisotropic film as alignment layer of nematic liquid crystals, and obtained a uniform and stability alignment result, the static contrast ratio is about 100, which is very close to application of liquid crystal device. This thesis is an instance that the photochemical material was used in the physics region of liquid crystals, the route that was from photosensitive monomer, self-assembled monolayer film to self-assembled multiplayer film was undergone, by this logical research method photoailgnment of liquid crystal was extended and consummated.

围绕上述思路开展了如下工作：1合成了三种可进行光二聚反应的光敏小分子单体，LPUV 辐照制作了光控取向膜；用紫外-可见光谱法和红外光谱法分析了薄膜中的光化学反应，发现小分子的光反应程度可达到50%以上，至少比光敏高分子高出5倍；薄膜的偏振红外光谱证实，经过LPUV 辐照后薄膜出现了明显的各向异性；将小分子光控取向膜制成液晶器件，在偏光显微镜下观察看到均匀一致的液晶取向；并且热稳定性达到100℃左右，接近实用化要求。2制备了含肉桂酸、香豆素基团的自组装单层膜；采用接触角的方法监测自组装反应的动力学过程；紫外-可见光谱证实了自组装单层膜在石英基板表面形成；自组装单层膜经LPUV 辐照后能诱导液晶均匀取向，而且热稳定性可达130℃，热稳定性进一步提高。3合成了含有光敏双键的双季铵盐，在水溶液状态下将它和聚乙烯基苯磺酸钠沉积生成layer-by-layer 自组装多层膜，紫外-可见光谱证实这是一个逐层均匀的沉积；在LPUV 照射下，自组装膜中的光敏双键按照偏振方向发生[2+2]环加成反应，形成取向膜，用二向色性值评价的分子取向度高于高分子及小分子光控取向膜的水平；实验证明用自组装多层膜制成的液晶器件亮暗态均匀，静态对比度约为100，达到实用化器件的水平。

The aminolignin flocculant was prepared based on calcium lignosulfonate, diethylamine and epichlorohydrin by amino grafting.

摘要以木质素磺酸钙、二乙胺和环氧氯丙烷为原料，通过接枝氨基，合成了木质素胺脱色絮凝剂。

High performance liquid chromatography-photodiode array detection-elctrospray ionization mass spectrometry (HPLC-PAD-ESI-MS) method was used to determine secoisolariciresinol diglucoside qualitatively and quantitatively. Precision, stability, limits of quantification, SDG recovery and sample preparation method were studied.

采用高效液相色谱－二极管阵列检测－电喷雾质谱(HPIC-PAA-ESI-MS)法对开环异落叶松树脂酚二葡萄糖苷进行定性和定量检测，研究方法的精密度、稳定性、定量检测限及加样回收率，并考察样品制备方法对定量检测结果的影响。

Do you know, i need you to come back

你知道吗，我需要你回来

Yang yinshu、Wang xiangsheng、Li decang,The first discovery of haemaphysalis conicinna.

1〕 杨银书，王祥生，李德昌。安徽省首次发现嗜群血蜱。