色环

RESULTS: High efficiency liquid chromatography showed good resolving power. The absolute recoveries were not lower than 75%.

结果：受者高效液相色谱法分析有很好的分离度，环孢素A绝对回收率均不低于75%。

Disk height index of intervertebral disks on X-ray films, areas and average T2 relaxation time of high intensity zone of disks on T2-weight MRI and histological score on pathological sections （HE staining, Masson staining and safranin O-fast green staining） were measured at 2 months, 4 months and 6 months after operation.

术后2、4、6个月时对正常及模型椎间盘观察X线片上的椎间盘高度指数、MRIT2加权相上的椎间盘高信号区的面积和平均T2弛豫时间、椎间盘纤维环损伤区的形态学变化、组织病理切片（HE染色、Masson三色胶原染色和番红O-固绿染色）椎间盘组织形态学变化、生物化学变化和组织学评分等指标。

A method for the determination of polycyclic aromatic hydrocarbons in smoked meat by gas chromatography/mass spectrometry has been established.

建立了熏肉中多环芳烃的气相色谱/质谱测定方法。

The experimental conditions were optimized to produce following results: good linearity of sulfamethoxazole, norfloxacin, ciprofloxacin, ofloxacin and tetracycline in the range from 1.00 ng/L to 1 000 ng/L and the limits of quantification 1 ng/L, the good linearity of terramycin and aureomycin in the range from 10.0 ng/L to 2 000 ng/L and the LOQ 10 ng/L, the recoveries of deionized water and surface water from 72.1% to 112%, and the RSD from 0.6% to 9.2%.

摘要〗采用超高效液相色谱-电喷雾二级质谱联用技术同时测定水中7种抗生素，优化了试验条件。磺胺甲恶唑、诺氟沙星、环丙沙星、氧氟沙星、四环素在1.00 ng/L ～1 000 ng/L 范围内线性良好，定量下限为1 ng/L ，土霉素、金霉素在10.0 ng/L ～2 000 ng/L 范围内线性良好，定量下限为10 ng/L ，去离子水和地表水样加标回收率为72.1%～112%， RSD 为0.6%～9.2%。

In these chromophores, the ring-locked triene employed as a conjugation bridge and the thiobarbituric acid moiety was as an electron acceptor in a D-π-A units.

在这些发色团中，环锁定的三烯和9，10-二氢蒽用作共轭桥，巴比妥酸和甲氧其分别作为吸电子和给电子基，组成非共轭的两个D-π-A单位。

Objective To establish a HPLC method for the determination of cyclosporin A in whole blood.

目的：建立高效液相色谱法测定环孢素A全血浓度的方法。

Amino-2-methylpropanol was used as the chemical modifying reagent of fatty acids to modify the carboxyl group into nitrogen-containing heterocycle which would effectively prevent the migration of carbon double bonds of the alkenyl in the electron impact source.

以2-氨基－2-甲基－丙醇为脂肪酸的化学修饰试剂，气相色谱－电子轰击质谱分析葵子油脂肪酸。2-氨基－2-甲基－丙醇将脂肪酸羧基修改为含氮杂环，使在EI源中避免了链烯基中碳碳双键的移动。

Components were identified which represented 85.1% of the total essential oil by the silica gel column separately.Conclusion 10 components were identified which included Bicyclo (6,3,0) undeca-dien-3-one, 5,5-dimethyl ect. of the essential oil from Angelica acutiloba Kitag were analyzed for the first time.

结果超临界CO2萃取物为黄棕色油状物，得率为0.9%，用GC-MS联用技术从中鉴定出亚油酸乙酯、5，5-二甲基-双环（6，3，0）-1，7-十一烯-3-酮等30种成分，占挥发油总含量65.66%；萃取物经硅胶柱色谱分离纯化，从中鉴定出十八酸乙酯等11种成分，占总含量的85.1%。

Components were identified which represented 65.66% of the total essential oil includding 9.12-octadecadienoic acid, ethyl ester and ect. 11 components were identified which represented 85.1% of the total essential oil by the silica gel column separately.conclusion 10 components were identified which included bicyclo (6,3,0) undeca-dien-3-one, 5,5-dimethyl ect.

结果超临界co2萃取物为黄棕色油状物，得率为0.9%，用gc-ms联用技术从中鉴定出亚油酸乙酯、5，5-二甲基-双环（6，3，0）-1，7-十一烯-3-酮等30种成分，占挥发油总含量65.66%；萃取物经硅胶柱色谱分离纯化，从中鉴定出十八酸乙酯等11种成分，占总含量的85.1%。

The separation of optical isomers of 2, 2'-dihydroxy-1, 1'-binaphthyl and 2, 2'-diamino-1, 1'-binaphthyl was studied by reversed-phase high performance liquid chromatography on a chiral stationary phase consisting of-hydroxypropyl-β-cyclodextrin (Cyclobond Ⅰ 2000 SP)using methanol/water as the mobile phase. The effects of mobile phase ratio, flow rate and column temperature on separation of optical isomers of DHBN and DABN were investigated.

在S-羟丙基－β-环糊精手性柱(CyclobondⅠ2000 SP)上用反相高效液相色谱法研究了2，2'-二氨基－1，1'-联萘和2，2'-二羟基－1，1'-联萘光学异构体的分离，考察了流动相组成、流速以及柱温等对联二萘胺和联二萘酚光学异构体分离的影响。

Do you know, i need you to come back

你知道吗，我需要你回来

Yang yinshu、Wang xiangsheng、Li decang,The first discovery of haemaphysalis conicinna.

1〕 杨银书，王祥生，李德昌。安徽省首次发现嗜群血蜱。