色烯

The reaction mechanism of pure olefin compounds and that of olefins in gasoline under different conditions were analyzed.

在自制的微反-色谱装置上，进行了单体烯烃和催化裂化汽油在不同条件下的催化裂化反应实验。

The constituents were extracted by some solvents. 18 constituents were isolated from Chloroform fraction by different chromatography. 15 constituents were identified by IR ,MS and NMR as follows: 3-sitosterol, P-sitosterylpalm itate,succinate acids, 1, 4-benzenediol, 1, 2-benzenediol, p-hydroxybenzaldehyde, syringaresinol, oleanolic acid, usolic acid, ethyl caffeate , Rosmarinic acid ethylster and etc. In such constituents ,nine compounds were isolated for first time from Origanum vulgare L..

牛至药材经水煮醇沉法所得浸膏，利用溶剂法和色谱法从中分离得到18个单体成分，通过IR、MS、NMR等波谱技术鉴定了其中的15个化合物，分别为β-谷甾醇(1)、β-胡萝卜苷(2)、琥珀酸(3)、对-二苯酚(4)、邻-二苯酚(5)、对羟基苯甲醛(6)、1.2-二羟基-4-异丙基-5-甲基苯(7)、新木脂素(8)、丁香脂素(9)、齐墩果酸(10)、乌苏酸(11)、4-二十六烯(12)、正二十六醇(13)、咖啡酸乙酯(14)、迷迭香酸乙酯(15)等，其中化合物3、4、5、6、7、8、9、14、15等9种化合物均为首次从该属植物中分离得到。

It was applied to analyze the structures of ashless dispersants and their derivatives. The results were obtained and correlated. The molecular weight distribution and dipersity of ashless dispersant, number of polyisobutene R and polymeric degree of R polymerism in addition agent were obtained.

以Ultrastyragel为固定相，四氢呋喃作流动相，用普适标准校正曲线及凝胶渗透色谱法对无灰分散剂及其对应衍生物的结构进行了分析测定，并将测定结果相关联，计算出了无灰分散剂的相对分子质量分布、分散度及添加剂所含聚异丁烯R基的个数及R基聚合度。

The sample was isolated by sephadex G-25 gel filtration column after concentration. Then bioactivity was assayed by Candida albicans. The chemical components were isolated and identified by GC-MS. GC determined the relative percentage content of the extract, nine kinds of components were separated, identified and accounted for about 82.12%, the major compound was propenyl methyl disulfide.

浓缩后的样品通过Sephadex G-25凝胶柱分离提纯其中的有效成分，以白色念球菌进行生物活性测定，并用气相色谱-质谱法对其化学成分进行分离鉴定，GC法测定各种化合物的相对百分含量，共鉴定了9种成分，约占总提取物的82.12％，其中，主要物质是甲基丙烯基二硫化物。

A method for the determination of squalene in seawater was developed by using solid-phase microextration with 100 μm polydimethylsiloxane coating and gas chromatography-mass spectrometry.

摘 要 首次报道了应用聚二甲基硅氧烷纤维作为固相微萃取的萃取头，色-质联用法快速测定海水中角鲨烯的方法。

In the paper,the essential oil of Syringa oblate Lindl var affinis Lingelsh bud from Qinghai was extracted by the method of water vapor distillation.

采用水蒸气蒸馏法提取了产自青海的白丁香花蕾的挥发油，应用GC/MS方法对其化学成分进行了分析，分离出47个色谱峰，鉴定了26个化合物，占总峰面积的88.7%，主要成分是丁香酚、丁香醇、石竹烯、苯乙醇等化合物。

In the paper,the essential oil of Syringa oblate Lindl var affinis Lingelsh bud from Qinghai was extracted by the method of water vapor distillation. After detected by GC-MS,47 peaks were separated from the oil. Among them,26 compounds taken up 88.7% of total peak areas were identified.

采用水蒸气蒸馏法提取了产自青海的白丁香花蕾的挥发油，应用GC/MS方法对其化学成分进行了分析，分离出47个色谱峰，鉴定了26个化合物，占总峰面积的88.7%，主要成分是丁香酚、丁香醇、石竹烯、苯乙醇等化合物。

In these chromophores, the ring-locked triene employed as a conjugation bridge and the thiobarbituric acid moiety was as an electron acceptor in a D-π-A units.

在这些发色团中，环锁定的三烯和9，10-二氢蒽用作共轭桥，巴比妥酸和甲氧其分别作为吸电子和给电子基，组成非共轭的两个D-π-A单位。

Unguis Hominis ; lipids ; squalene ; GC/MSD Analysis

人指甲；脂类；角鲨烯；气相色谱-质谱分析

ABSTRACT To study the antibacterial constituents from the fermentation broth of endophytic fungus Penicillium sp. 0935030 from mangrove plant Acrostichum aureurm. The separation procedure was guided by antibacterial bioassay. Seven compounds were isolated and purified by column chromatography, and their structures were identified as cyclo (1), cyclo (2), 1(2Furanyl)1,2ethanediol (3),(3β,4β,22β)olean12ene3,22,23triol (4), mannitol (5), uridine (6), and liquiritigenin (7) by physicochemical and spectral data.

为研究红树林植物卤蕨内生真菌Penicillium sp.0935030发酵物中的抗菌活性成分，采用活性追踪的方法，用多种色谱技术对化合物进行分离纯化，通过理化性质和光谱数据鉴定出7个化合物，分别为：环(1)，环(2)，1呋喃基1，2乙二醇(3)，(3β，4β，22β)12烯3，22，23三羟基齐墩果烷(4)，甘露醇(5)，尿苷(6)和甘草素(7)。

But we don't care about Battlegrounds.

但我们并不在乎沙场中的显露。

Ah! don't mention it, the butcher's shop is a horror.

啊！不用提了。提到肉，真是糟透了。