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The method has been used to determine Phthalic esters in drinking water and seawater sample. 3. Single drop microextraction, followed by gas chromatography with flame ionization detection has been applied to determine Formaldehyde, Acetaldehyde and Acraldehyde in water based on 2,4-Dinitrophenylhydrazine derivatization. Extraction solvent, extraction time and stirrer speed were optimized. Optimal experimental conditions were as follows: 1.6μL toluene microdrop exposed for 30 min in a 3ml aqueous sample placed in 4ml vial and stirred at 600 rpm/min.

以2,4-二硝基苯肼衍生,单滴液相微萃取与气相色谱火焰光度检测器联用测定水样中的甲醛、乙醛、丙烯醛,考察了萃取溶剂、液滴大小、萃取时间、搅拌速度、盐效应等对该方法的影响,并对影响液相微萃取的各种因素进行了系统的阐述,确定了该体系的最佳实验条件,实现了甲醛、乙醛、丙烯醛的提取和富集。

Ophenyl phenol,ophenyl phenol sodium salt tetrahydrate,7ADCA,2ethyl phenyl hydrazine hydrochloride,2,3dihydrofuran,7ethyl3(2hydroxy ethyl)indole,methyl ester of etodolac; 1,8diethyl1,3,4,9tetrahydropyrano[3.4b] indole1acetic acid methyl ester,5chloro2methoxy benzoic acid,4(2aminoethyl)benzene sulfonamide,5cyano phthalide,phthalhydrazide,9thioxanthenone,n[(1,4benzodioxane2yl)carboxyl]piperazine HCL,2chloro4amino6,7dimethoxyquinazoline,2chloro benzimidazole,1(4fluorobenzyl)2chlorobenzimidazole,2methylthio4pyrimidone,5amino4imidazole carboxamide HCL,6chloro2hexanone,11oxo6.11hydrodibenzothiepin,6,11dihydrodibenzooxepin11one,10,11dihydrodibenzocyclohepten5one;dibenzosuberone,dibenzo cyclohepten5one;dibenzosuberenone,3,5dihydroxy benzoic acid,3,5dihydroxy benzyl alcohol,2mercapto benzimidazole,3,4dihydroxy benzaldehyde,3,4dihydroxy benzonitrile,2amino5chloro benzonitrile,2(4chlorophenoxy)ethyl chloride,2(4chloro phenoxy)tert,butane,ditrimethylol propane;DTMP,2,2bis(4hydroxyphenyl)butane; bisphenol B,1,1'bis(4hydroxyphenyl)cyclohexane;bisphenol Z,tetrabromobisphenolS,3,5ditertbutyl salicylic acid,3,4,5trihydroxy benzoic acid stearyl ester,1,2,4trimethoxybenzene.

华业公司产品:邻苯基苯酚,邻苯基苯酚钠盐,7氨基3去乙酰氧基头孢烷酸,邻乙基苯肼盐酸盐,2,3二氢呋喃,7乙基色氨醇,依托度酸甲酯,5氯2甲氧基苯甲酸,4(2氨乙基)苯磺酰胺,5氰基苯酞,双酮酞嗪,9噻吨酮,N〔(1,4苯并二恶烷2基)羰基〕哌嗪盐酸盐,2氯4氨基6,7一二甲氧基喹唑啉,2氯苯并咪唑,1(4氟苄基)2氯苯并咪唑,2甲硫基4嘧啶酮,5氨基咪唑4 甲酰胺盐酸盐,6氯2已酮,11氧6.11二氢苯并〔b.c〕虑平,11氧代6,11二氢二苯并氧杂卓,10,11二氢二苯并环庚烯5酮,二苯并环庚烯5酮,3,5二羟基苯甲酸,3,5二羟基苯甲醇,2巯基苯并咪唑,3,4二羟基苯甲醛,3,4二羟基苯腈,2氨基5氯苯腈,2(4氯苯氧基)1氯乙烷,2(4氯苯氧基)叔丁烷,双丙烷,2,2二(4羟基苯基)丁烷;双酚B,1,1'双(4羟基苯基)环己烷;双酚Z,2[3,5二溴4(2,3二溴丙氧基)]苯砜,3,5二叔丁基水杨酸,3,4,5三羟基苯甲酸十八烷基脂,1,2,4三甲基氧基苯。

Result The results showed that 34 compounds of the volatile oil were identified, which accounted for 90.10% of all. The main chemical compounds were camphene (10.030%), beta-pinene (8.826%), limonene (7.935%), caryophyllene (12.457%). The antibacterial experiments of the volatile oil showed that the volatile oil had antibacterial activities to Staphylococcus aureus, but had no inhibition against Escherichia coil and Rhodotorula glutinis.

结果]经毛细管色谱分析分离,共确认出其中34种成分,所鉴定出化学成分的质量占总量的90.10%以上,应用色谱峰面积归一法分析各成分的质量分数,其主要化学成分是莰烯(10.030%)、-β-蒎烯(8.826%)、柠檬油(7.935%)、丁子香烯(12.457%);并发现其化学成分对金黄色葡萄球菌有较强的抑制作用,对大肠杆菌、红酵母无明显作用。

Objective To establish a HPLC method for determination of diethylstilbestrol and chloramphenicol in compound diethylstilbestrol cream .

目的用高效液相色谱法同时测定复方己烯雌酚乳膏中己烯雌酚和氯霉素的含量。

This invention discloses an intermolecular charge transfer chromogen with triphenylamine group, with a formula indicated by (1), wherein: R1 is hydrogen atom or methyl group or methoxyl group, R2 is hydrogen atom or 2-(5,5-dimethyl-3-vinylcyclohexenyl-2-enylidene)propanedinitrile group.

本发明公开的含三苯胺基团的分子内电荷转移生色团,具有式1所示的结构式,其中R 1 为氢原子或甲基或甲氧基,R 2 为氢原子或2-(5,5-二甲基-3-乙烯环己烯基-2-烯亚基)丙二腈基。

This invention applies mild condition uses substituent group triphenylamine aldehyde or triphenylamine dialdehyde as raw material to react by heating with 2-(5,5-dimethyl-3-vinylcyclohexenyl-2-enylidene)propanedinitrile group to produce the intermolecular charge transfer chromogen with high decomposition temperature, non-coplanar structure, and triphenylamine group.

本发明采用温和的手段,将取代基三苯胺单醛或取代基三苯胺双醛为原料与2-(3,5,5-三甲基环己烯-2-烯亚基)丙二腈共热生成具有高的热分解温度、非共平面空间结构的含三苯胺基团的分子内电荷转移生色团。

Samples were subjected to high pressure ranging from 100 to 500 MPa. After high pressure treatments, the flavour compounds were extracted by Solid-Phase Microextraction. Analysis was carried out by Gas Chromatography-Mass Spectrometry. The key flavour compounds of orange juice were three alkenes (namely limonene, myrcene and α-pinene), two alcohols (linalool and α-terpineol), three aldehydes, one ketone and two esters (ethyl butyrate and 3-OH-ethyl hexanoate).

采用固相微萃取(Solid Phase Microextraction,SPME)方法对不同压力(100~500 MPa)超高压处理的鲜榨橙汁中的香气成分进行富集,并经气相色谱-质谱联用仪(Gas Chromatography-Mass Spectrometry,GC-MS)检测分析,橙汁中的主要香气成分有:3种烯(柠檬烯、月桂烯、α-蒎烯);2种醇;3种醛;1种酮;2种酯(丁酸乙酯、3-OH-己酸乙酯),它们是构成橙汁的主要特征致香成分。

To obtain a flocculant which could effectively remove dyes from dyeing wastewater , the amphoteric polymer was prepared by copolymerization of acrylamide, acrylic acid, cationic monomer and dmethyldiallylammonium chloride or acryloyl oxyethyl trimethyl ammonium chloride.

为制备一种对染色废水有显著脱色效果的絮凝剂,采用溶液聚合法,将两种阳离子单体二甲基二烯丙基氯化铵和丙烯酰氧乙基三甲基氯化铵分别与丙烯酰胺,丙烯酸共聚,合成了两性聚合物。

Compounds were identified by means of physic-chemical property and spectral data including three new compounds: platyphyllin A (1), neochlorgeniclatone (2),(2E,6Z)-2,6-dimethyl-8-O-β-D-glucosyl-2,6-octadienoic acid (3). The known compounds included cyclic diarylheptanoids, phenylic acid, ect.

从白桦叶的水提取物中,利用各种色谱分离手段(硅胶柱色谱、聚酰胺柱色谱、凝胶柱色谱及制备薄层色谱等),分离得到28个化合物,通过理化性质及各种波谱数据(NMR,MS,IR,etc)鉴定了23个化合物的结构,其中新化合物三个:platyphyllin A(1),新绿原酸内酯(neochlorgeniclatone,2),(2E,6Z)-2,6-二甲基-8-O--2,6-辛二烯酸(2E,6Z-2,6-dimethyl-8-O-β-D-glucosyl-2,6-octadienoic acid,3。

The content of conjugated dienes in petroleum products is determined by ultraviolet spectrophotometry.

在化学反应-气相色谱法联合测定含烯汽油中共轭二烯烃质量分数的基础上,建立了用紫外分光光度法测定油品中的共轭二烯烃的含量。

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