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Make use of HPLC, can availably classify true or false D-calcium pantothenate, the D-calcium pantothenate sample diagram and standard diagram have similar diagram in same reservation time, the content meets provision;The false D is mainly depend on adding calcium inorganic salt, urea and glucose etc, to make specific optical rotation, calcium content, nitrogen content to attain a nation standard, but these material in the same reserve time have never absorbed diagram to make peak area very small, the content of external standard be low.

本文以市售D-泛酸钙为样品(山东新发药业有限公司生产),对所建立的检测方法进行了验证,通过精密度、准确度和标准曲线等验证项目的实验,结果表明,本文所建立的D-泛酸钙的高效液相色谱检测方法可以准确地检测产品的含量;利用液相色谱图谱,可以有效地区分真假D-泛酸钙,D-泛酸钙样品图谱与标准品图谱在相同的保留时间处,有类似谱图,含量符合规定;搀假的泛酸钙主要靠添加无机钙盐、尿素和葡萄糖等使比旋度、钙含量、氮含量达到国家标准,但这些物质在此处无谱图造成峰面积很小,外标含量低。

The procedure involves the use of a capillary chromatography column (HP-INNOWAX, 30 m×0.53 mm×1.0 um) and FID detector. The result showes that 4 solvents are completely separated, the regression equation coefficients of 4 solvents are above 0.99, the recoveries are 90%~110% and the RSDs are less than 2.0% respectively.

实验的色谱柱为HP-INNOWAX(30 m×0.53 mm×1.0μm)毛细管色谱柱,检测器为氢火焰离子化检测器。4种溶剂均达到完全分离,各溶剂线性实验所得回归方程的相关系数均大于0.99,加标回收率为90%~110%,RSD.0%(n=6)。

The HPLC system column, mobile phase of CH3CN-3%CH3COOH (11∶89) mixture, with detection wave at 270 nm, was used to determine the content of vitexin in Leaf of Crataegus pinnatifida Bge.

应用反相高效液相色谱法测定了山楂叶总黄酮中牡荆素的含量。C18柱作为色谱柱,乙腈-3%醋酸水溶液(11∶89)为流动相,检测波长270 nm,按外标法定量。

Methods An SE-30 capillary column (30 m × 0.25 mm × 0.25 μm) and a flame ionization detector were used when n dodecane was used as the internal standard.

采用 SE 30 (30 m×0.25 mm×0.25 μm)石英毛细管色谱柱,以正十二烷为内标,进样口温度210 ℃,检测器温度300 ℃的气相色谱测定百秋李醇含量。

More than 400 company employees, have high-quality professional and technical, and management talent more than 60 people, covering over 8,000 square meters, the introduction of Japan and Germany 2-6 labeler color (20), Roland four-color machine, ECRM laser machines as licensing, Agfa-machine, a plastic machines, automatic Shaiban Ji, UV dryer, and other advanced production equipment.

公司现有员工400多人,拥有高素质的专业技术、管理人才60多人,占地面积8000多平方米,引进日本和德国二至六色贴标机(20台)、罗兰四色机、ECRM激光照牌机、爱克发冲片机、过胶机、全自动晒版机、UV干燥机等先进生产设备。

GC Analysis of Alachlor·Acetochlor·Atrazine 42% SE CAO Ying, SHI Xin-jin (Sanonda Zhengzhou Pesticide Co. Ltd., Zhengzhou 450009, China) Abstract: A method was introduced for the determination of alachlor, acetochlor and atrazine by GC With CP-7906 capillary column and FID detector, the internal standard was nonadecane. The three compositions were analyzed easily in the same condition and column.

42%甲草·乙·莠悬乳剂的气相色谱分析曹颖,师新进(沙隆达郑州农药有限公司,郑州 450009)摘要:采用气相色谱法,在CP-7906毛细管柱上以正十九烷作内标,用FID检测器测定甲草胺、乙草胺和莠去津的含量。

As to the high polarity, high boiling point resultant—trimesic acid, the analysis methods of infrared spetrum, gas chromatography-mass spectroscopy, vapour-phase chromatography, acid number titration and so on are seperately used to characterize its property. Infrared spetrum and gas chromatography-mass spectroscopy are used to have a qualitative analysis on the resultant and are compared with the stand diagram. Sulfuric acid-methanol esterification and rapid esterification are used to prepare the trimesic acid trimethyl-ester and have a FID quantitative analysis. So that we make sure the purity of trimesic acid in the resultant and also we have an acid alkali titration on the resultant to get its acid number, in order to verify the purity of trimesic acid in the resultant.

对于高极性、高沸点的固体产物均苯三甲酸,分别采用红外光谱、气质联用、气相色谱、酸值滴定等分析手段进行了表征:利用红外光谱、气质联用的方法进行产物的定性分析,并与在同一仪器、同一条件下做出的标准谱图进行比对;采用硫酸-甲醇酯化法和快速酯化法制备出均苯三甲酸三甲酯,对其进行气相色谱FID定量分析,进而确定固体产物中均苯三甲酸的纯度;用酸碱滴定法确定固体产物的酸值,以对固体产物中均苯三甲酸的纯度进行验证。

The machine is available in 4 colours (aluminium, sandblasted-brown, red and white), and is pre-set to be customized by changing the push-button console and deep-drawing logos and writings.

该机器有4种顏色(铸铝色,喷砂褐色,红色和白色)并且可以使用客制化的控制台图样,标誌和文字等来进行个性化的设计。

A method for Pendimethalin quantitation was established by using diamyl phthalate as internal standard with GC. The chromatographic column was HP-5, and temperature program was used: 200℃ for 0.5 min, programmed to rise at 10℃ to 240℃, then isothermal for 2.5 min.

采用HP-5石英毛细管色谱柱和FID检测器,以邻苯二甲酸二戊酯为内标物,在适宜的色谱条件下对二甲戊灵原药进行定量分析。

A simple,rapid,sensitive and accurate RP HPLC for simultaneous determination of ketamine, phenobarbitone and atropine in plasma was established.

本文采用ZorbaxC8色谱柱,甲醇-磷酸盐缓冲液(69∶31)为流动相,220nm为检测波长,非那西丁为内标,建立了同时测定人血浆中氯胺酮、苯巴比妥和阿托品浓度的反相高效液相色谱法。

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However, as the name(read-only memory)implies, CD disks cannot be written onorchanged in any way.

然而,正如其名字所指出的那样,CD盘不能写,也不能用任何方式改变其内容。

Galvanizes steel pallet is mainly export which suits standard packing of European Union, the North America. galvanizes steel pallet is suitable to heavy rack. Pallet surface can design plate type, corrugated and the gap form, satisfies the different requirements.

镀锌钢托盘多用于出口,替代木托盘,免薰蒸,符合欧盟、北美各国对出口货物包装材料的法令要求;喷涂钢托盘适用于重载上货架之用,托盘表面根据需要制作成平板状、波纹状及间隔形式,满足不同的使用要求。

A single payment file can be uploaded from an ERP system to effect all pan-China RMB payments and overseas payments in all currencies.

付款指令文件可从您的 ERP 系统上传到我们的电子银行系统来只是国内及对海外各种币种付款。