至高

The conclusions were as follows: theνO-H andνC=O IR absorption maxima shifted towards higher wave numbers after imprinting 17β-estradiol on TFMAA-co-TRIM copolymer with the red shift of theνO-H groups being apparent after precipitation polymerization for 16h while that forνC=O groups being observed after polymerization for 24h. A strong interaction between TFMAA and 17β-estradiol was confirmed by the high selectivity for 17β-estradiol, as indicted by the values of the separation factor of isomers of 17β-estradiol/17α-estradiol (2.28) and the imprinted factor (3.01). Particle diameter of TFMAA-co-TRIM polymer was between 300 nm and 1.5μm, which suited well for solid phase sorbent throughout at low column pressure. The recognition of imprinting TFMAA-co-TRIM polymer for sterol molecules was driven by enthalpy eluted with acetronitile, and low temperature was in favor of the separation of sterol structure analogues on imprinting column. TFMAA-co-TRIM polymer possessed of determinate anti-heat stability, with melting point beginning at 255.84℃, Tp=257.40℃, control TFMAA-co-TRIM polymer and imprinting TFMAA-co-TRIM polymer were respectively decompounded at 267.79℃and 343.11℃, and solid micro-extraction noddle prepared by the special polymerization also showed definite recognition for 17β-estradiol by GC/MS detecting at 270℃. By selection of various washing and elution solvents, elution reagents of close polymerization system were of more advantage in template molecules retention and recognition on molecularly imprinted solid phase extraction column. At a certain extent, progesterone, 17α-estradiol, 17β-estradiol and 4-androstene-3, 17-dione could be intercepted on the MISPE column. Especially, MISPE had high selectivity for progesterone, and imprinting TFMAA-co-TRIM polymer could achieve adsorption balance within 50 min by absorption kinetics test for 17β-estradiol. However, MISPE column showed better selectivity and enrichment property for 17β-estradiol than C18 and CSPE columns according to the data from HPLC and GC/MS analyses. Recovery of 17β-estradiol on MISPE column was up to 85.5% while when prime extracting solution of milk powder was sampled, the recovery of CSPE and C18 columns were 43.7% and 30.7%, respectively.

通过研究阐明：紫外聚合产物TFMAA-co-TRIM中的νO-H振动吸收峰在聚合16h后红移，νC=O振动吸收峰在聚合24h后红移；TFMAA-co-TRIM对雌二醇异构体的印迹因子达到了3.01，α为2.28，优于其它功能单体参与得到的聚合物识别特性；TFMAA-co-TRIM聚合物粒径介于300 nm至1.5μm之间，作为色谱固定相具有良好的通量和低的柱压；在乙腈流动相中，TFMAA-co-TRIM分子印迹固定相的分离过程主要被焓驱动，低温有利于分子印迹固定相分离甾醇结构类似物；TFMAA-co-TRIM分子印迹聚合物在255.84℃时开始熔融，Tp=257.40℃，聚合物CP的降解温度在267.79℃，MIP降解温度在343.11℃，制备的固相微萃取头初步经GC/MS 270℃的耐热性测定；不同的洗提溶剂筛选证明了选择接近聚合溶剂的洗脱体系更有利于MISPE发挥识别效应；分子印迹固相萃取柱对孕酮、17α-雌二醇、17β-雌二醇和雄烯二酮都具有不同程度的保留特性，可作为此类化合物的吸附材料，特别对孕酮强保留的富集特性，可作为孕酮的选择性识别吸附剂，其分子印迹聚合物对17β-雌二醇的吸附动力学测定显示在50 min内基本达到吸附平衡，具有作为传感器核心敏感材料的潜力；对比萃取奶粉中17β-雌二醇性能，MISPE柱比非分子印迹固相萃取柱和C18柱具有更高的保留，回收率依次为85.5%，43.7%和30.7%。

Credible estimates suggest that the losses on nonperforming loans exceeded 40%-50% of China's GDP.

可信度较高的估计认为，不良贷款的损失占到了中国国内生产总值的40%至50%以上。

However, with the improvement of people's living standard as well as changes in diet, our country the incidence of childhood obesity has risen to 7%, body weight and blood pressure is directly related to hypertension in obese than normal incidence of high-3 times more weight.

然而，随着人们生活水平的提高以及饮食结构的改变，我国儿童肥胖的发生率上升至7%左右，体重与血压有直接关系，肥胖者高血压病发病率比正常者体重高3倍以上。

Center, the largest ore body in Handan County, Huang Liang Meng Gao Village area of North West by yongnian Kong to great saphenoushan shan qu leopard, more than ten kilometers long from north to south, about four billion tons reserves, there are 10 kinds of chemical constituents.

最大矿体中心在邯郸县黄粱梦高北村一带，由永年的北西岗至邯山区大隐豹，南北长10多公里，储量约为40亿吨，化学成分有10种。

Nouveau riche upstarts have caused prices of properties on the Rublyovka to rocket sky-high.

新近产生的爆发户已经令到在卢比窝卡的房地产的价格标升至火箭般高。

The company bases itselfupon high-end,insists the six words development guideline ,"Euramerican,classical,hight-grade",and the three development roads,"brand,series,and Occidentalize",and implements the development strategy of "existence based on quality, developed based on design innovation, and surpassing based on excellent service "to improve marketcompetitiveness and in fluence of the brand of Zhongzhixin Furniture!

公司立足高端，坚持以"欧美古典高档"六字发展方针坚持走"品牌化系列化欧美化"三大发展路线执行以质量求生存以设计创新求发展以优质服务求超越的发展策略持续提升中至信家具品牌市场竞争和影响力！

The water rose until it was on a level with the river banks.

水涨至与河岸一般高。

Gregorian chant and plainsong which are monodic (i.e. written as one musical line) gradually developed during the 11th to 13th centuries into organum (i.e. two or three lines moving simultaneously but independently, therefore almost inadvertently representing the beginnings of harmony).

格里高利高唱和plainsong是monodic ，逐步发展，在11日至十三世纪到organum （即两个或三个动线，同时但独立的，所以几乎在不经意代表的开端和谐）。

Jointly develop ,produce with the key scientific research universities and colleges "baixing" and "Tendly" brand Hi-Tech new-type Origanum oil ( draw from the origanum vulgarel grass) betaine、garlicin、 organic copper、organic chromium、sodium dia-cetate、methionine copper、methionine iron、methionine zinc、methionine manganese etc. Series of products. Obtain the scientific and technological result first prize of Henan , The third-class scientific and technological progresses is rewarded ,advanced enterprise of Xiangcheng city scientific and technological , undertake the two scientific and technological brainstorm project of "the eighth five-Year Plan period provinces in dependently. Awarded to "outstanding private scientific and technological enterprise of Henna province" by the scientific and technological drawing room of henna province in 2001.With bear two of national" the Ninth five-Year Plan jointly by fodder by Chinese Academy of Agricultural Sciences, one shiwu scientific and technological brainstorm project.

与重点科研院校联合研制、生产"百兴""添德利"牌高科技最新型饲料添加剂：牛至油，甜菜碱、大蒜素、有机铜、有机铬、双乙酸钠、蛋氨酸铜、铁、锌、锰络合物等系列产品，分别获得河南省科技成果一等奖，科技进步三等奖，项城市科技先进企业，独立承担两项省"八五"科技攻关项目，2001年被河南省科技厅授予"河南省优秀民营科技企业"，同中国农科院饲料所联合承担两项国家"九五"，一项"十五"科技攻关项目。

They typically run about 2 to 6 points higher in loan origination fees as well.

通常来说约2至6点收费较高，贷款也是起源。

The labia have now been sutured together almost completely.The drains and the Foley catheter come out at the top.

此刻阴唇已经几乎完全的缝在一起了，排除多余淤血体液的管子和Foley导管从顶端冒出来。

To get the business done, I suggest we split the difference in price.

为了做成这笔生意，我建议我们在价格上大家各让一半。