膜的

Then the relations of structures and properties of microporous membranes used in lithium-ion batteries were discussed.

介绍了锂离子电池隔膜用微孔膜的制备原理与结构，重点叙述了熔融拉伸法和热致相分离法制备微孔膜的基本原理和膜结构影响因素，并在此基础上讨论了锂离子电池隔膜用微孔膜结构与性能之间的关系。

Results:(1) FSN can inhibit secondary joints swelling and multi-arthritis evidently, improve the whole condition of rats; at the same time, it can also lighten the synovial inflammation and hyperplasia of lesion joints distinctly, and prevent the joint cartilage and bone from destruction; the collective efficiency of FSN is better than TWP.(2) FSN can raise AA rats low LTT of spleen to normal nearly, remedy the disorder of Th / Ts and Thl / Th2 cells balance in peripheral blood, restrain exorbitant TNF- a ? IL-1 produced by PM O , thereof exert anti-inflammatory and immunoregulation effect.(3) Inside the lesion joints, FSN can depress abnormal hyper-expression of TNF- a mRNA and NF-kB in synovial tissues, as well as advance the expression of Caspase-3 (a proteolytic enzyme of apoptosis), reduce synovial immflamination and proliferation.(4) FSN can lower the expression of VEGF in synovial tissue,reduce neogenetic veins, so inhibit the growth of pannus tissue and the damage of cartilage and bone by that.(5) The above effect of FSN are in proportion to its dosage.Conclusions: FSN has inhibitory effects on symptom and condition of experimental RA, which is better than TWP as a whole.

结果：(1)FSN有明显的抗炎作用，可显著抑制AA大鼠足跖肿胀与多关节炎，改善大鼠的全身情况，同时明显减轻病变关节滑膜炎症与增生，防止关节软骨及骨质的破坏，其综合作用优于TWP；(2)FSN还能使AA大鼠低下的脾LTT恢复至接近正常，纠正外周血中T细胞亚群Th／Ts及Th1／Th2平衡紊乱，抑制大鼠PHφ过高的TNF-α、IL-1分泌，而发挥抗炎和免疫调节作用；(3)在病变关节局部，FSN能显著抑制AA大鼠滑膜细胞异常增高的TNF-αmRNA的表达，降低滑膜组织中NF-kB表达，并增加凋亡蛋白酶Caspase-3表达，从而抑制滑膜的炎症与增殖；(4)FSN还可下调滑膜组织中VEGF表达，减少血管新生，由此抑制血管翳的形成及其对软骨和软骨下骨的侵蚀；(5)FSN的上述作用皆呈现一定的量效依赖关系，高剂量组作用优于低剂量组。

FSN can raise AA rats low LTT of spleen to normal nearly, remedy the disorder of Th/Ts and Th1/Th2 cells balance in peripheral blood, restrain exorbitant TNF-α、IL-1 produced by PMφ, thereof exert anti-inflammatory and immunoregulation effect.(3) Inside the lesion joints, FSN can depress abnormal hyper-expression of TNF-αmRNA and NF-kB in synovial tissues, as well as advance the expression of Caspase-3 (a proteolytic enzyme of apoptosis), reduce synovial immflammation and proliferation.(4) FSN can lower the expression of VEGF in synovial tissue, reduce neogenetic veins, so inhibit the growth of pannus tissue and the damage of cartilage and bone by that.(5) The above effect of FSN are in proportion to its dosage. Conclusions: FSN has inhibitory effects on symptom and condition of experimental RA, which is better than TWP as a whole.

结果：(1)FSN有明显的抗炎作用，可显著抑制AA大鼠足跖肿胀与多关节炎，改善大鼠的全身情况，同时明显减轻病变关节滑膜炎症与增生，防止关节软骨及骨质的破坏，其综合作用优于TWP；(2)FSN还能使AA大鼠低下的脾LTT恢复至接近正常，纠正外周血中T细胞亚群Th/Ts及Th1/Th2平衡紊乱，抑制大鼠PMφ过高的TNF-α、IL-1分泌，而发挥抗炎和免疫调节作用；(3)在病变关节局部，FSN能显著抑制AA大鼠滑膜细胞异常增高的TNF-αmRNA的表达，降低滑膜组织中NF-kB表达，并增加凋亡蛋白酶Caspase-3表达，从而抑制滑膜的炎症与增殖；(4)FSN还可下调滑膜组织中VEGF表达，减少血管新生，由此抑制血管翳的形成及其对软骨和软骨下骨的侵蚀；(5)FSN的上述作用皆呈现一定的量效依赖关系，高剂量组作用优于低剂量组。

The studies of hydrogen behaviour in HR-1 stainless steel and its composite sample with CVD coated chromium oxidic film have been presented.

本文介绍氢在HR－1不锈钢基体及镀有氧化铬膜的复合材料中的行为研究，包括基体的准备；膜的制备；用不同手段从不同角度对膜进行的分析测试；膜与基体之间的平均结合力测定；用不锈钢材料构成的高温低压渗透回路的建造、调试、密封性能校准；纯HR－1基体材料中的氢渗透规律研究；有膜复合材料中氢的稳态迁移过程的表现规律实验结果。

The results show that the surface quality of phosphating film is obviously improved by ZY, and a uniform and compact coating can be obtained when phosphated at 20℃ for about 20 minutes, which is 1.09 g/m^2 in weight, can withstand CuSO4 solution dropping for above 200 s, and resist mass fraction of 3% NaCl solution soaking for more than 5 hours.

结果表明，成膜助剂ZY明显地改善了磷化膜的表面质量，在20℃、磷化20min时可以获得均匀致密的磷化膜，膜重为1.09g/平方公尺，耐CuSO4点滴时间超过200s，质量分数为3%的NaCl溶液浸泡时间超过5h。

It indicated that the multiple-layered films were mainly composed by C-F, C=C and Si-O bonging, a little Si-C and Si-F bonding were also existed because of history effect. The bondgap were calculated as 2.7eV. The dielectric constant of the multiple-layered films was close relative to the thickness of the covering layer-SiOx, so the thickness had better be reduce. The bonding configurations of multiple-layered films had no evident changes after 400癈 annealing, the thickness raise very little and the dielectric constant increase 8%. Compared with one-layered a-C:F films prepared in the same conditions, the SiOx/a-C:F/SiOx multiple-layered films had a better thermal stability.

结果表明，多层膜主要由C-F，C=C，Si-O键构成，由于器壁的历史效应，薄膜中还存在少量Si-C和Si-F键；多层膜的光学带隙经计算约为2.7eV；多层膜的介电常数与包层SiO_x厚度有很大关系，应尽可能减小SiO_x厚度；在经历200-400℃的N_2氛围中退火后，多层膜的红外结构没有发生太大的变化：膜厚度稍微增大，介电常数只增加了8％，与同样制备条件下沉积的单层a-C：F薄膜相比具有较好的热稳定性。

Sensing ability of PSS/PANI self-assembled film with different doping/dedoping structure to DMMP and CEES was investigated. Results demonstrate that the gas sensitivity of PSS/PANI self-assembled film is affected by the size of dopant counterions. Gas sensitivity of self-assembled film increases with increasing size of dopant counterions. It is found that sensing ability of PSS/PANI self-assembled film to DMMP increases significantly by redoping/dedoping EB-PSS/PANI film with sarin acid that has similar structure with DMMP.

首次考察了不同掺杂/脱掺杂结构的PSS/PANI自组装膜对化学战剂模拟剂DMMP和CEES的敏感性能，研究表明，掺杂酸对离子的尺寸大小对PSS/PANI自组装膜的气敏性有很大影响，较大的对离子尺寸有利于提高自组装膜的气敏性；并且发现采用与DMMP结构类似的沙林酸对EB-PSS/PANI自组装膜进行再掺杂-脱掺杂，能显著提高PSS/PANI自组装膜对DMMP的敏感性能。

POMs and deys are still maintained integrallty.AFM exhibits the films is even.The thickness of each layer is about 1.25nm. The AFM images reflect that there are some protuberances on the outer surface layer of the film, which due to the aggregates of spherical structure PMo12. Cyclic Voltammograms reflects the redox potentials of dye in multilayer shifts towards more positive values than pure dye multiplayer which may be explained by charge transfer from dye to POM. Fluorescence spectra show that polyoxometalates caused the fluorescence decay of dyes, which maybe used as fluorescence sensors.

UV-VIS说明复合膜均匀生长； IR 光谱、XPS能谱研究结果表明，紫外光照前后，膜中多酸/染料分子间没有发生显著的光化学反应，各组分的结构仍然保持；原子力显微镜显示，膜的外表面是均匀的，每一个双层厚度大约是1.25nm，膜表面的隆起，可能是多酸阴离子簇堆积所引起；循环伏安测定结果表明，由于多酸阴离子的影响，有机染料的氧化还电位发生了正的偏移，反映出复合膜中染料分子与多酸阴离子间发生了荷移相互作用，导致染料分子失去部分电子而使氧化性略强；荧光光谱研究结果表明，多酸阴离子可以有效地引发荧光染料的荧光淬灭，这为多酸在荧光传感器方面的应用提供了有价值的信息。

The copolymer derived from the copolymerization in high capacity kettle were testified that copolymerization between AN and MMA occurred. The microcapsules in the films are distributed in the copolymer film matrix. The heat-absorbing temperatures and heat-evolving temperatures of the films are almost the same as that of the MOCT, respectively. In addition, the enthalpy efficiency of MOCT, the melting enthalpy and the crystallizing enthalpy rises with the contents of MOCT increasing.The decomposition temperature of copolymers in the films containing various contents of MOCT decreases with the contents of MOCT increasing.

采用30升聚合釜合成了丙烯腈—甲基丙烯酸甲酯共聚物，证实了丙烯腈和甲基丙烯酸甲酯发生了共聚反应；正十八烷微胶囊分散和镶嵌到了共聚物膜基体中；正十八烷微胶囊含量不同的共聚物膜的吸热温度放热温度与纯正十八烷微胶囊的吸放热温度基本相同；随着正十八烷微胶囊含量的增加，共聚物膜的热焓和热效率逐渐增加；共聚物膜中的共聚物的热稳定性温度随着正十八烷微胶囊含量的增加逐渐减小，共聚物膜的结晶度则有所增大。

The humidity resistance and the sensitivity to chemical warfare agents simulants of the tuned films were also investigated.Self-assembled LBL polyaniline films were prepared from aniline monomers by in situ polymerization and the mechanism of film formation was discussed. It was proposed that the self-assembly of polyaniline occurred through the quick absorption of aniline monomer cations or aniline monomer cation radicals on the glass surfaces by electrostatic attractions to form homogeneous polymerization centers, then increased gradually by the way of upright to the glass supports for extensity, leading to the polyaniline chain growth. The polyaniline was doped under acidic condition to absorb anionic polyelectrolyte, such as sodium polystyrene sulfonate based on the electrostatic force, or to adsorb polymer based on hydrogen-bonding interactions, for example Polyvinyl Alcohol, and then recycled to fabricate_n or_n self-assembled multilayer films.

跟踪了原位聚合的具有纳米结构的聚苯胺多层自组装膜的成膜过程，提出了该自组装膜的成膜机理：聚合反应初始阶段的苯胺阳离子或苯胺阳离子自由基通过静电作用快速吸附到带负电荷的基片表面，形成均匀的聚合中心，然后以垂直于基片的方式进行链增长生成PANI；PANI在酸性条件下经现场掺杂后带正电荷，再通过静电作用吸附带负电荷的聚电解质如聚苯乙烯磺酸钠，或通过氢键作用吸附聚合物如聚乙烯醇，这样循环LBL-SA即得到_n或_n等原位聚合聚苯胺自组装膜。

Do you know, i need you to come back

你知道吗，我需要你回来

Yang yinshu、Wang xiangsheng、Li decang,The first discovery of haemaphysalis conicinna.

1〕 杨银书，王祥生，李德昌。安徽省首次发现嗜群血蜱。