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New compounds of the type of N--N'-(2,4-dichlorophenyloxyacetyl)-semicarbazides were synthesized by a series of reactions of preparing organic isocyanates by Curtius rearrangement with 2,4- dichloro aryloxyacetic acid hydrazide using one-pot procedures.

以芳香取代酸为原料,用Curtius重排的方法合成异氰酸酯,直接与2,4-二氯苯氧乙酰肼作用,一锅法合成了4种N-取代芳基-N'-(2,4-二氯苯氧乙酰基)氨基脲类化合物。

Based on the tissue culture, the effect of N-phenyl-N'-1,2,3-thiadiazol-5-ylurea, 6- benzyla minoprine(6-BA) and 1-Naphthylacetic acid on spore germination, protonema develop- ment and bud differentiation in Entodon challenged was investigated in this paper. The whole process was observed and taken pictures. The results show that TDZ, 6-BA and NAA have no significant effect on the spore germination. During the process of protonema development, 1.0 mg/L NAA can promote the primary development of protonema significantly, and 0.4 mg/L TDZ promotes branches formation in inter- mediate stage of the protonema development.

:研究了3种植物生长调节剂苯基噻二唑基脲、6-苄基腺嘌呤(6-BA)、萘乙酸对密叶绢藓孢子萌发、原丝体发育及芽体发生的影响,并对整个发育过程进行了显微观察和照相,结果表明:(1)3种植物生长调节剂对密叶绢藓孢子萌发影响不显著;(2)在原丝体发育阶段,1.0mg/LNAA对原丝体初期的发育促进效果显著,0.4mg/LTDZ对原丝体发育中期分枝的形成促进效果显著,6。

Compositions: deionized water, roseleaf, rose essential oil, rose extract, coco-glucoside, CAB-35, lauryl alcohol polyether ammonium sulfate, DMDM glycolylurea

成份: 去离子水、玫瑰花瓣、玫瑰精油、玫瑰花提取物,椰油基葡糖苷,椰油酰胺丙基甜菜碱,月桂醇聚醚硫酸铵, DMDM 乙内酰脲。

A series of 5-bromopyrimidinyl-containing new sulfonylureas have been synthesized through bromination of 2-amino-4-methyl pyrimidine, followed by further modification and then coupled with sulfonyl isocyanate.

通过2-氨基-4-甲基嘧啶溴代反应以及进一步的衍生、磺酰基异氰酸酯的胺解,合成了一系列含有5-溴嘧啶基的新磺酰脲。

In addition a series compounds of thiazole glycosides (17a~17f) were synthesized through 1-benzoyl-3-aryl-thioureas by phase-transfer catalysis method under mild condition.

另外,本文以1-苯甲酰基-3-芳基硫脲为原料通过相转移合成法合成了一系列噻唑类糖苷的衍生物(17a~17f)。

A novel compound——N-naphthalene acylN′-substituted p-chlorobenzamido thiocarbamide was synthesized by reaction of p-chlorobenzamido hydrazine and α-naphthalene acyl mustard oil,which was obtained by potassium thiocyanate combined with α-naphthalene acyl chloride formed from α-naphthylacetic acid and SOCl2 in anhydrous benzene.

通过α-萘乙酸和SOCl2在无水苯中反应制得α-萘乙酰氯,然后与硫氰酸钾反应生成α-萘乙酰基异硫氰酸酯,再与对氯苯甲酰肼进行加成反应,合成了新型化合物N-萘乙酰基-N′-对氯苯甲酰氨基硫脲,用薄层色谱法跟踪最后一步反应,确定了反应时间。

Naphthalene acetyl chloride was prepared firstly by the reaction between α-naphthylacetic acid and SOCl2 in anhydrous benzene,then reacted with potassium thiocyanate to obtain α-naphthalene acetyl isosulfocyanate,as taking an addition reaction with p-chloro benzoyl hydrazine the novel compound N-naphthalene acetyl-N'-p-chloro benzoylamino thiocarbamide was finally synthesized.

通过α-萘乙酸和SOC l2在无水苯中反应制得α-萘乙酰氯,然后与硫氰酸钾反应生成α-萘乙酰基异硫氰酸酯,再与对氯苯甲酰肼进行加成反应,生成新型化合物N-萘乙酰基-N'-对氯苯甲酰氨基硫脲。

Naphthalene acetyl chloride was prepared firstly by the reaction betweenα-naphthylacetic acid and SOCl2 in anhydrous benzene, then reacted with potassium thiocyanate to obtainα-naphthalene acetyl isosulfocyanate, as taking an addition reaction with p-chloro benzoyl hydrazine the novel compound N-naphthalene acetyl-N'-p-chloro benzoylamino thiocarbamide was finally synthesized.

通过α-萘乙酸和SOCl2在无水苯中反应制得α-萘乙酰氯,然后与硫氰酸钾反应生成α-萘乙酸基异硫氰酸酯,再与对氯苯甲酰肼进行加成反应,生成新型化合物N-萘乙酰基-N'-对氯苯甲酰氨基硫脲。

CH3OH could attack the phosphor atom in 1,3,2-dioxaphopholane of compiound (1) to give O-methyl O-hydroxyethyl-O-phthalimidoethyl thiophosphate in 85% yield; in the presence of potassium hydroxide aryl selenol could attack the carbon atom in 1,3,2-diox-aphopholane of the cyclic phospholipid conjugate of N^1-(2-furanidyl)-N^3--5-fluorouracil to give the corresponding product of ring-opening in high yields.

在室温下,以异丙醇作溶剂,苯硒酚与化合物2不反应。在氢氧化钾存在下,以异丙醇/水作溶剂(体积比20:1,在室温下,硒酚可以有效地进攻中化合物2中1,3,2-二氧磷杂环戊烷中的碳原子生成相应的开环产物。按照这一反应条件,顺利实现了硒酚对N^1-(2-呋喃基)-N^3-羟烷基-5-氟脲嘧啶硫代环甘油磷脂缀合物的亲核开环,生成甘油骨架的端碳原子上带有芳硒基新颖的磷脂核苷缀合物。

Ingredients: Water,Lauric Acid,Myristic Acid,Stearic Acid,Propylene Glocol,Potassium Hydroxide,Cocamidopropyl Betaine,Starch Hydroxypropyltrimnium Chloride,Sodium Laureth Sulfate,Glycol Distearate,Lavandula Angustifolia Oil,Creatine,Tetrasodium Edta,Perfume,Dmdm Hydantoin.

成分: 去离子水,月桂酸,肉豆蔻酸,硬脂酸,丙二醇,氢氧化钾,椰油酰胺丙基甜菜碱,淀粉羟丙基三甲基氯化铵,月桂醇聚醚硫酸钠,乙二醇双硬脂酸酯,薰衣草精油,肌酸,乙二胺四乙酸四钠,香精,DMDM 乙内酰脲。

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