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Ni-S-Co coated electrode was prepared on foam nickel matrix by means of gradient electrodepostion method by increasing sulphourea concentration in electrolyte.

以泡沫镍为基体,通过提高镀液中硫脲浓度的方法梯度电沉积制备了非晶态Ni-S-Co合金镀层电极。

The mechanism of thiocarbonyl compounds with thiourea function group has been proposed according to the photoreaction products.5. Total of one heterocyclothione intermidate and four heterocyclothione compounds have been synthesized and structurally characterized.

根据所得到的产物对具有硫脲基团的硫羰基化合物的光反应机理进行合理的推测。5、合成与表征了1个环硫酮中间体和4个杂环硫酮类化合物,摸索出合成杂环硫酮中间体较佳反应条件。

A series of urea,thiourea and thiodiazole derivatives bearing mercaptotetrazole were synthesized using NaN_3 as a nitrogen source.

以叠氮化钠为氮源,合成了一系列含四唑环的芳基脲及噻二唑类化合物,其结构经1H NMR,IR和元素分析表征。

Reactive oxygen species causing DNA oxidative damage comes from two kinds of ways:one is from cellular normal physiological metabolism;the other is from outer environment.Redox-sensitive green fluorescent protein was expressed in Saccharomyces cerevisiae.Recombinant cells were evaluated in monitoring the changes in the redox state of living cells when challenged with toxicologically relevant metal ions NaAsO_2 or Pb(NO_3)_2 by measuring emission intensity at 510 nm with a Hitachi F6500 fluorescence spectrophotometer,roGFP expressed in yeast responded not only to typical membrane-permeant oxidants H_2O_2 and reductants DTT,but also to toxicological metal ion-induced intracellular redox changes in a dose-dependent manner.Moreover,exposure of yeast cells to NaAsO_2 or Pb(NO_3)_2 at concentrations that induced redox changes reported by roGFP caused up to 2~3 fold increases in DNA mutation frequency.This mutagenic effect was largely caused by oxidative stress since blocking the production of hydryl radicals with thiourea significantly reduced the mutation rate as well as delayed the cell death.

本文将对氧化还原状态变化敏感的绿色荧光蛋白roGFP1-R12,在酵母细胞中实现了多拷贝强表达;荧光扫描经强氧化剂H_2O_2和还原剂DTT以及环境中重金属NaAsO_2或Pb(NO_3)_2处理后的酵母细胞悬液,测定510 nm处的荧光发射强度结果显示,表达的绿色荧光蛋白对氧化还原水平敏感,且在510 nm处的荧光强度与一定的重金属浓度呈正相关,即roGFP1-R12在510nm处的荧光发射值随重金属浓度的增高而增强,从而说明重金属对细胞的毒性在一定程度上很可能是通过破坏细胞内的氧化还原平衡发生作用;同时通过该绿色荧光蛋白对胞内氧化还原状态变化的响应情况可以来实时检测环境中的重金属;遗传学的点突变频率及致死率实验数据表明,重金属能导致菌体的点突变频率和致死率升高,且活性氧的清除剂巯基脲能明显降低这种点突变和致死率,说明由重金属引发的这种点突变和致死效应在很大程度上是依赖于重金属对细胞诱导产生的氧化胁迫。

The invention relates to a pipeline polyurea outer anticorrosive coating and the making method thereof, making heated prepolymerization reaction on dibenzo-methane diisocyanate, carbodiimide diisocyanate, polyether binary alcohol and polyether trihydric alcohol to prepare prepolymer solution A, and making end amino polyethylene oxide ether, dimethyl sulfur-based toluene diamine, diethyl diamine, iso-propyl titanate solution, polyacrylate, carbon black, titanium dioxide and lightweight calcium carbonate into solution B, and as using, respectively heating the solutions A and B to 65 deg.C and then mixing them, then quickly spraying and curing to form a coat.

本发明涉及一种管道用聚脲外防腐涂料及制造方法,由二苯基甲烷二异氰酸酯、碳化二亚胺化二异氰酸酯、聚醚二元醇和聚醚三元醇通过加热预聚反应制成预聚物的A液、由端氨基聚氧化乙烯醚、二甲硫基甲苯二胺、二乙基甲苯二胺、钛酸异丙酯溶液、聚丙烯酸酯溶液、碳黑、钛白粉和轻质碳酸钙配制而成的B液组成,使用时将A液和B液分别加热至65℃后混合,然后快速喷涂固化形成涂层。

New compounds of the type of unsymmetrically substituted ureas are synthesized by a series of reactions of preparing organic isocyanates by Curtius rearrangement with aromatic amine.

以3 苯基 2 丙烯酸为原料,用Curtius重排的方法合成异氰酸酯,直接与芳香胺作用,合成了5 种N 取代苯基 N′苯丙烯基脲类化合物。

Aminobenzothiazoleswere diazotized and then coupled with active methylenecompounds to form a kinds of new hydrazones.

苯基硫脲在浓硫酸中,先在溴作用下氧化合环,再直接硝化,得到产率95%,纯度98%的2-氨基-6-硝基苯并噻唑。

In pacemaker cells of SA node superfused with the oxygenated K—H solution, MDP, APA, V〓, VDD, RPF and APD〓 were—45±5mv, 48±4mv, 2. 4±0.9v/s, 89±8 mv/s, 200±11bpm and 206±15ms, respectively. Anoxia (perfused for 20min with a modified K—H solution gassed with 100% N〓 and deprived of glucose) increased MDP, APA and V〓, and decreased VDD and RPF in a timedependent manner. At anoxia for 20min, the above parameters were—58±5mv, 64±5mv, 11. 7±2. 7v/s, 24±7mv/s, 92±11bpm and 179± 14ms, respectively. ADase (10U/L).

环戊腺苷和苯基异丙基腺苷不仅能增加豚鼠窦房结起搏细胞APA、MDP和〓,且能减小VDD、RPF和〓在环戊腺苷20nmol/L浓度时,MDA、APA和〓分别增值5.4±0.7mv、7.6±0.9mv和2.4±0.5v/s,VDD、RPF和〓分别降低32±4mv/s、68±9bpm和31±12ms(p.05或0.01)。0.1μmol/L 8—苯茶碱和10μmol/L格列苯脲能明显地抑制环戊腺苷的电生理效应。

Segmented polyester polyurethaneurea based n 4, 4'-disphenylmethane diisocyanate, ethylene diamine and polybutylene adipate elastomers and their deuterated polymers were studied by means of IR spectroscopy.

用红外光谱法对基於4,4'-二苯基甲烷二异氰酸酯、乙二胺和聚己二酸丁二醇酯的嵌段聚酯型聚脲氨酯弹性体及其氘化產物进行了研究。

For the isolated Uracil, the shift of the appropriate hydrogen atoms can generate many different tautomers. Moreover, theoretical studies demonstrate that some tautomers of Uracil possibly result in the mispair of nucleic acid base pairs.

通过氢原子的转移,脲嘧啶可以产生许多互变异构体,而且研究表明它的一些互变异构形式可能会导致碱基的错配。

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Since this year, in a lot of villages of Beijing, TV of elevator liquid crystal was removed.

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