脱醇

The coupling process of dehydrogenation of 1,4-butanediol and hydrogenation of dimethyl maleate over CuO/SiO2 catalysts to produce one important fine chemical γ-butyrolactone was carried out in a continuous fixed bed reactor under atmospheric pressure.

和传统的反应过程相比，耦合反应提高了顺丁烯二酸二甲酯加氢和1，4-丁二醇脱氢活性。

In the present report we describe a young man with CTX who was on high dose steroids for a misdiagnosed chronic inflammatory demyelinating polyneuropathy and had normal level of serum cholestanol.

本文报道1例青年男性CTX患者，该患者因被误诊为慢性炎症性脱髓鞘性多神经病而接受大剂量的激素治疗，并且患者的血清胆固烷醇水平正常。

Firstly, 3-ethylthiobutanal was prepared from crotonaldehyde reacting with ethanehiol in triethylamine with high yield. Secondly, methyl acetoacetate was converted to 6-ethylthiohept-3-en-2-one by three steps via hydrolysis, condensation with 3-ethyltio-butanal and dehydration, then 6-ethylthiohept-3-en-2-one was cycloco ndensed with dimethyl malonate by Michael addition and Claisen condensation, followed by saponification and decarboxylation to give the intermediate of 5-(2-ethylthiopropyl)-cyclohexane-1,3-dione.

首先，以巴豆醛与乙硫醇为原料，在三乙胺的催化作用下高收率制得3-乙硫基丁醛；然后从乙酰乙酸甲酯出发，通过碱水解、与3-乙硫基丁醛缩合、脱水三步反应合成6-乙硫基-3-烯-2-庚酮，接着6-乙硫基-3-烯-2-庚酮与丙二酸二甲酯通过Michael加成和Claisen缩合成环，再通过皂化和脱羧反应生成中间体5-[2-丙基]-1，3-环己二酮；再与丙酸酐反应丙酰化，最后与0-3-氯-2-丙烯基羟胺肟化，得到目标化合物烯草酮。

Oil and cyanogenic glycosides were extracted simultaneously from flaxseed by two-liquid-phase system of ethanol-hexane-water.

采用正己烷-乙醇-水三元双液相体系进行同时提取亚麻籽中油脂和脱除氰苷的研究，通过单因素试验和响应面分析进行优化，确定的优化提取条件为：料醇比为1∶3.4；料烷比为1∶5.4；提取时间为78.5 m in；N aOH浓度为0.12%；温度为55℃；乙醇浓度为85%。

The best clarifying treatment was attempted by means of modeling and optimization with GA coupled NN. The 85% decolour rate and 80% xylitol recovery percentage was achieved.

籍助于耦联神经网络的遗传算法的模型化和优化获得了最佳的发酵液澄清方案，达到了85％脱色率和80％木糖醇回收率。

We study the active sites for dehydrogenation of 2-butanol and the reason for producing the by-product.

我们还对仲丁醇脱氢的催化活性中心和副反应产生的原因进行了深入的研究。

The reaction technics for dehydrogenation of CHL was studied. Reduction temperature was confirmed at 220℃.

对环己醇脱氢催化剂进行了反应工艺条件的试验，确定了以220℃为催化剂的还原温度。

A Product main business categories: chemical solvents white oil, toluene, xylene, durene, valitin water, acetate, D resin, acetone, butanone, cyclohexanone , anti-white water, dichloromethane, trichloroethane, trichlorethylene, loose water-saving washing network water, open water, wash water, and days that water, rust agent, to water-logging, washing machine water, decontamination water, n-butyl alcohol, isopropyl alcohol, ethanol, industrial alcohol, car-washing water, washing machine water, clean lines of water, cleaning machine water, fire water, paint remover, fungicides, antifreeze water, chloroform, grinding fluid , diluent, release agent, dehydration agent substantial industrial solvents.

主要经营产品 A类：化工溶剂白电油、甲苯、二甲苯、四甲苯、凡立水、乙脂、丁脂、丙酮、丁酮、环己酮、防白水、二氯甲烷、三氯乙烷、三氯乙烯、松节水、洗网水、开油水、洗面水、天那水、除锈剂、去渍水、洗枪水、去污水、正丁醇、异丙醇、乙醇、工业酒精、洗车水、洗机水、抹线水、抹机水、火水、脱漆剂、杀菌剂、防冻水、哥罗仿、研磨液、稀释剂、脱模剂、脱水剂等大量工业溶剂。

Its mechanism is the use of anthraquinone in alkali conditions off proton surface forming 10 more stable carbon anion face, but because carbon anion and oxygen ion exist between testosterone and enolate type each other changes, cause reaction product complex, at least five, reaction selectivity, product yield, separation difficulties, and product purity is not high, therefore, using the type and quantity of alkali, phase transfer catalyst type, solvent, to optimize the selection process conditions so as to improve the yield target product.

其机理是利用蒽酮在碱存在的条件下脱去氢质子面形成10位较稳定的碳负离子面进行，但是因为碳负离子和氧负离子之间存在酮式和烯醇式的互变，导致反应复杂，产物至少有五种，反应选择性差，产物分离困难，产率低，且产品纯度不高，因此，利用对碱的种类和量的多少，相转移催化剂的种类，反应溶剂的选择，来优化反应工艺条件从而提高目标产物的产率。

The second synthetic strategy commenced from butane-1,4-diol 50, which underwent monobenzylation, Swern oxidation, enolization followed by acetylation and debenzylation to yield an intermediate 46 in an overall yield of 54% in a 4-step procedure.

第二条路线从1，4-丁二醇50开始，这个化合物经过单苄基化、Swern氧化、烯醇化随后乙酰化和脱苄基化共4步反应得到中间体46，总产率54％。

With Death guitarist Schuldiner adopting vocal duties, the band made a major impact on the scene.

随着死亡的吉他手Schuldiner接受主唱的职务，乐队在现实中树立了重要的影响。

But he could still end up breakfasting on Swiss-government issue muesli because all six are accused of nicking around 45 million pounds they should have paid to FIFA.

不过他最后仍有可能沦为瑞士政府&议事餐桌&上的一道早餐，因为这所有六个人都被指控把本应支付给国际足联的大约4500万英镑骗了个精光。