脱氮的

Over the AlPO〓, the deamination and dealkylation of diethylmine and triethylmine produced ethylene selectivily. Over AlPONs of acid-base bifunctional catalysts the ethylnitrol formed selectivily.

二乙胺、三乙胺在酸性的磷酸铝上选择性的脱烷基/脱氨生成乙烯，在酸碱两性的氮化磷酸铝上选择性脱烷基/脱氢生成乙腈。

Both the protection and deprotective group methods for the amino-group on side chain of a new N-pivot lariat crown ether were studied comparatively.

研究了一种新的氮支套素冠醚侧链上氨基的保护和脱保护基方法，结果表明，由过量乙二胺与对甲苯磺酰氯反应得到的单保护乙二胺（N－对甲苯磺酰基乙二胺4a），经N－烷基化环化反应，然后在氢化铝锂存在下脱除保护基，即可制得最佳产率的N－（2－氨基已基）单氮杂－12－冠－4（1）。

The prepared powders were characterized by XRD, UV-Vis, FTIR, N_2 adsorption, Fluorescence spectroscopy, etc. N-doped TiO_2 evidently shows its absorbance shoulder shift into visible light region. Moreover, N-doping retards the transition of TiO_2 from anatase to rutile type as well as restrains the growth of the crystal size which leads to less decrease of surface area. These characteristics are considered to benefit the photoactivity of TiO_2; When all the samples were applied to the photodecomposition of Methylene Blue under visible light(λ＞400 nm), the N-doped TiO_2 show an obvious superiority when compared to the undoped TiO_2, the active hydroxyl groups are found to play a important role in this high photoactivity; When the same experiment was performed under UV light, all the samples show the consistent sequence of photoactivity as in the visible light.

通过UV-Vis、XRD、BET、IR、FL等表征手段测试表明：掺氮不仅使TiO_2的光吸收区域拓展到可见光区，而且有利于延缓TiO_2晶相的转换，从而抑止了高温煅烧下所引起的晶粒增大以及比表面积的降低，且氮源浓度越高，此现象越明显，这些特征都有利于催化剂光催化活性的提高；在主波长大于400nm的可见光催化亚甲基蓝实验当中，掺氮TiO_2的光催化活性明显优越于未掺氮样品，亚甲基蓝在90min内达到88％的脱色率。

Compared to the other carbon and nitrogen sources studied, sucrose and malt extract were found to be the suitable carbon/nitrogen sources. The decolorization efficiency of Cerrena unicolor Y5002 to orange G was similar at different orange G concentration below 500mg/L; however, alizarin red inhibited the decolorization reaction at the concentration of 400mg/L or above 400mg/L.

对一色齿毛菌Cerrena unicolor Y5002的液体培养脱色条件进行了研究，其最适碳源和氮源分别为蔗糖和麦芽浸粉；在不同橙黄G浓度下均获得较高的脱色率，因此浓度为500mg/L的橙黄G未对该菌的脱色能力产生抑制作用，而浓度为400mg/L茜素红则对其脱色作用产生明显抑制。

The results indicate that there is the significant linear correlation between the decoloration value and half-time and molecular descriptors, especially MW/S and number of azonic groups of azo dyes. Moreover, a QSPR model of azo dyes was achieved and used for calculation of predicted decoloration value and half-time of the dyes.

结果表明，染料分子结构描述符MW/S值、芳香环数目偶氮基数目和与I/O值与脱色率和半衰期之间存在着较好的线性相关性，其中MW/S值和偶氮基数目对脱色率和半衰期的贡献最为显著；所获得的QSPR定量关系模型可用于计算和估计水溶性阴离子偶氮染料的理论脱色率和半衰期。

CuRF coupounds are based on the combination of deprotonation and ICT mechanisms. The secondary amines conjugated to 1,8-naphthalimide could be deprotonated by Cu2+, and as a result, large red shifts in both absorption and fluorescence spectra were obtained, from which one could sense Cu2+ colorimetrically and ratiometrically.

CuRF 系列则是基于脱氢和ICT原理的结合，铜离子与受体的作用能够诱使共轭氮原子上的氢脱去，共轭氮原子显负电增强了对荧光团的供电能力，从而引起荧光波长的红移，同时也造成了吸收光谱的红移。

According to the above study result, the diversity of microorganisms population in the SUFR system is complex and the bio-community formed in the SUFR system is stable. The close relations between abundance of bacteria and nutrients were found. The correlation between heterotrophic bacteria and COD was 0.949. The correlation between organic phosphate bacteria and TP was 0.815. The correlation between nitrosobacteria and NH3-N was 0.909. The correlation between disnitrifier bacteria and TN was 0.653. These inneglectable great factors effecting on phosphorus-uptake and phosphorus-release of phosphorus accumulating organisms are the influent COD、the concentration of DO、the sludge retention time、the temperature. The diversity of organic phosphate bacteria population in the SUFR reactor was complex and there is no phosphate bacteria taking the absolute superiority in quantity. The near-native pure culture method powerfully complement the traditional pure culture technique and enrich culture technique. The sludgy bioactivity is very good in whole SUFR reactor. By the quality of being biochemistry, the anaerobic phase is higher than anoxic phase and the anoxic phase is higher than aerobic phase of SUFR.

通过以上试验内容研究发现，SUFR 系统中的微型动物种群较多，微生物生态系统稳定；系统中微生物的数量与营养盐的含量密切相关，其中总异养菌与COD的相关系数r 为0.949，有机磷细菌与TP 的相关系数r 为0.815，亚硝化菌与NH4+-N的相关系数r 为0.909，反硝化菌的数量和TN 的相关系数r 为0.653；污水生物除磷工艺中进水COD 的浓度、DO 浓度、泥龄的长短、温度都是影响聚磷菌释磷及吸磷效果的不可忽视的因素；SUFR 系统中的磷细菌呈现种群多样化的趋势，没有占绝对优势数量的磷细菌；微孔滤膜近自然培养法是对传统纯培养技术和富集培养技术的有力补充；整个SUFR 反应器系统中污泥的生物活性很好，就可生化性来讲，厌氧反应器大于缺氧反应器大于好氧反应器；按照动力学方程式求出的细胞生长动力学特征值和SUFR 脱氮除磷系统工艺的实测值结果基本吻合。

The preparation of the membrane is that the phthalazine polyether-sulfone-ketone polymer is mixed with chloroform, Ethanol or butanol according to certain quality proportion; after the magnetic stirring, the evenly mixed casting solution is obtained, filtered and carried out with vacuum deaeration; The casting solution is scraped into membrane of certain thickness on the non-woven fabric by adopting the scraper; the membrane is standed for 24 hours in the air of certain humidity and temperature to obtain the plate ultrafiltration membrane of phthalazine polyether-sulfone-ketone.

本发明公开了属于高分子膜分离技术领域的一种二氮杂萘聚醚砜酮类聚合物平板超滤膜的制备方法，所述膜的制备方法为：用二氮杂萘聚醚砜酮类聚合物与氯仿、无水乙醇或正丁醇按照一定的质量比混合，磁力搅拌后得到混合均匀的铸膜液，过滤并真空脱泡；将铸膜液采用刮刀在无纺布上刮制成一定厚度的膜，该膜在一定湿度和温度的空气中静置24h后即得到二氮杂萘聚醚砜酮类平板超滤膜。

Through taken the measurements of pH, TOC, UV-Vis spectra and high-performance liquid chromatograph in the degrading process of solution ,it was found that the COD of dye solution increased, pH continuing declined and TOC reduced gradually. The UV-Vis spectra and high-performance shown that though dye molecules had been destroyed, Strong Chromophore Azo Double Bond of dye was certainly under attack, the big conjugated system was vandalized and dye molecules were decolorized degradation, but they were not completely changed into carbon dioxide and other inorganic matter by mineralization, it appeared accumulation of aromatic ring and double benzene nucleus, so it is thus evident that complete destruction of aromatic ring is more difficult than the double benzene.

通过测定直接大红染料脱色过程中的溶液pH、TOC、紫外可见光谱图和高效液相色谱图可知，在脱色处理时间(6h)范围内，染料溶液的COD值增大， pH值持续下降，TOC值逐渐降低，结合紫外可见光谱图和高效液相色谱图，说明染料分子虽然已经遭到破坏，染料分子内强生色基团偶氮双键确实遭到攻击，大的共轭体系被破坏，染料分子被脱色，却没有完全被彻底矿化成二氧化碳等无机物，出现了芳环和萘环结构的累积现象，可见完全破坏芳环比破坏偶氮双键发色团更困难。

X-ray diffraction. The microstructure and cross section microhardness of nitrided layers were observed and analyzed by optical microscope and microhardness tester.

在一定的工件表面温度下，粒子表面物理吸附的氮原子发生脱附，脱附下来的活性氮原子渗入基体的内部，形成渗氮层。

I can not make it blossom and suits me

我不能让树为我开花

When temperatures are above approximately 80 °C discolouration of the raceways or rolling elements is a frequent feature.

当温度高于 80 °C 左右时，滚道或滚动元件褪色是很常见的特征。