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胺化

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The synthesis of l-(4-acetylaminophenyl)-2-bromo-1-propanone was discussed, and the mechanism and possible factors were analyzed. Hence the routine was determined, in which l-(4-acetylaminophenyl)- 1-propanone was reacted with Bromine dissolved in ethanol, so that the a -bromination can be carried on, resulted in the yield of up to 70.4%.

探讨了1-(4-乙酰胺基苯基)-2-溴代-1-丙酮的合成方法,分析了反应机理和影响因素,确定将1-(4-乙酰氨基苯基)-1-丙酮溶解在乙醇中以溴的乙醇溶液进行α-溴化的合成路线,产率可达70.4%。

Tar-acenaphthene was used as starting material which was converted to 4,5-dibromo-1,8-naphthalimide through bromination, oxidation, condensation, and other steps.

以焦油苊为原料经溴化,氧化,缩合,等步骤合成了4,5-二溴取代-1,8-萘酰亚胺。

Objective: To compare the effect of ipratropium bromide with sulbutamol, on bronchodilatation in patients with asthma and COPD.

目的:比较溴化异丙托品气雾剂与沙丁胺醇气雾剂分别使用及联合应用对哮喘和COPD患者的支扩作用。

Taguchi method was used to design experiments to evaluate effects of concentration of butylamine, pH, ionic strength and temperature on immobilization behavior.

利用正交实验设计的方法系统地考察了预撑剂正丁胺的量、pH值、离子强度以及温度等各因素对固定化血红蛋白酶活性的影响。

Titanium silicalite 1(TS 1)with different crystal size s were synthesized in the system of TPABr n butylamine by adjusting the formation of gel and the method of crystallization.

在四丙基溴化铵正丁胺体系中合成不同晶粒大小的TS 1沸石,采用IR、XRD UV Vis、SEM、2 7AlMASNMR对其进行表征,并以丙烯环氧化反应为探针考察其催化性能。

The main objectives of this thesis are to study the effects of the chemical modification by caprylic aldehyde on the structure and properties of wheat protein.

本文旨在用单醛对小麦蛋白质塑料进行胺基酰化改性,研究醛的含量、模压温度等条件对蛋白质的结构、力学性能、吸湿性、流变性能等的影响。

The carboxyl groups of QDES were used to couple the free amino groups of EAH Sepharose 4B with the carbodiimide coupling method, and immobilized density was 5μmol/ml.

通过碳二亚胺反应将四肽配基QDES固定在商品介质EAH Sepharose 4B上制备出了配基固定化密度为5μmol/ml的亲和吸附介质,并利用亲和色谱柱考察了其吸附蛋白质特性。

The conjugation of MMS and Ab (ready for Reagent 1, R1): Chose the 3μm diameter Carboxyl MMS and use the carbodiimide cross-link technique activate the MMS with EDC and NHS in different concentration, then linked mice anti-HBsAg-IgG and mice anti-HCcAg-IgG on them.

磁微粒的活化及其与抗体的连接:选择粒径3μm的羧基化磁微粒,采用碳二亚胺共价交联法,在活化剂EDC与NHS的不同浓度组合条件下活化磁微粒,选择最适的活化剂浓度组合。

It was found that the condensation could be completed within 24 hours at 60°C in a solution containing 10mg CAWs, 20mg 2-aminoethyl mercaptan, 10mL CH2Cl2, 1 mL triethyl amine and 0.2g DCC (N, N'-dicyclohexyl carbodiimide).

实验结果表明:10mg经浓硝酸氧化处理过的碳原子线在含有20mg巯基乙胺、10mL CH2Cl2、1mLN3、0.2g DCC的液相反应体系中,60℃温度下作用24h可完成缩合反应,生成巯基化碳原子线。

Penicillin V acylase from the crude culture filtrate of Fusarium oxysporum FP 941 was purified with a single band on non-denaturing electrophoresis by means of (NH4)2SO4 fractional precipitation, adsorption on, and elution from, celite, ion-exchange column chromatography with DEAE-cellulose, and Sephadex G-200 gel filtration chromatography.

通过硫酸铵沉淀、硅藻土吸附、DEAD-纤维素离子交换层析和Sephadex G-200凝胶过滤,由尖镰孢FP941培养滤液中得到了聚丙烯酰胺凝胶电泳均一的青霉素V酰化酶。

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