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胺化

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For it is rubor after damaging to the closing soft tissue, getting swollen, getting hot aching and model of functiolaesa these bed solicit and there is no fracture,no skin damaged, we designed the corresponding experiment, namely the law of hot board causes little mouse\'s painful experiment of threshold of pain; Freun\'s complete adjuvant caused the swollen experiment of big mouse\'s foot;The xylene caused the swollen experiment of little mouse\'s ear; Invigorating blood circulation silt experiment that changes the sex that the rheology appearance examines the blood and flows with the blood; Useing the high performance liquid chromatography-electrochemistry Detected monoamine neurotransmitters transmitter in the brain and serum; the experiment of immunohistochemistry measured the proto-oncogene C-FOS expresses.

针对闭合性软组织损伤后的红、肿、热、痛及功能障碍的典型临床体征,加上无骨折、无皮肤破损的特点,我们设计了相应的实验,即热板法致小鼠疼痛的痛阈实验;福氏完全佐剂(Freun\'s complete adjuvant,FCA)致大鼠足肿实验;二甲苯致小鼠耳肿实验;用血流变仪测血液流变性的活血化瘀实验;运用高效液相色谱—电化学(high performance liquid chromatography-electrochemistry Detection HPLC-ECD)法测量大脑及血清中单胺类神经递质的实验以及免疫组织化学法检测原癌基因C-FOS蛋白产物表达的实验。

The organic saponifier often is composed of alkaline amines. Some common limitations are the potential attack of the solder joint, chemical oxidation that reduces bath life, limited effectiveness on some of the new flux compositions, and a contributor to the VOC content.

有机皂化剂一般由碱性胺组成,其主要的局限性在于可能对焊点造成腐蚀,并发生氧化反应降低焊剂清洗寿命,另外,它对某些新型焊剂清洗效果欠佳,VOC排放量较高。

This invention is directed to the-tartaric acid salt of 2-amino-N-{1-(2,4-difluoro-benzyloxymethyl)-2-oxo-2-3-oxo-3a-pyridin-2-ylmethyl-2-(2,2,2-trifluoroethyl-2,3,3a, 4,6,7-hexahydro-pyrazolo(4,3-c) pyridin-5-yl-ethyl}-2-methyl-propionamide which is a growth hormone secretagogue and as such is useful for increasing the level of endogenous growth hormone.

本发明涉及2-氨基-N-{1--(2,4-二氟-卞氧甲基)-2-氧代-2-3-氧代-3a-(R-吡啶-2-基甲基-2-(2,2,2-三氟-乙基)-2,3,3a,4,6,7-六氢化-吡唑子基(4,3-c)吡啶-5-基-乙基}-2-甲基-丙酰胺的--酒石酸盐,它是一种生长激素促分泌素,并且可用于提高内源性生长激素水平。

Zinc Selenide hexagonal flakes and hexagonal prism have been synthesized by solvothermal method using ethylenediamine as solvent.

以乙二胺-乙醇为溶剂采用溶剂热法成功合成了具有六方结构的六边形硒化锌薄片和六边形棱柱。

The synthesis of the pentacyclic skeleton of Et-743 and the construction of the five chiral centers thereof.1. The core pentacyclic skeleton of phthalascidin was constructed with L-dopa as the starting material via thirteen steps. First, two basic synthons, the C-1 functionalized tetrahydroisoquinoline compounds 8 and N-protected Z-dopa derivative 9, were prepared from L-dopa. They were coupled via amide bond to form the dipeptide compounds 10, which were the first key intermediates. Then the primary hydroxyl groups were transformed into the corresponding amino aldehydes 11 via Swern oxidation. Followed by the intramolecular Pictet-Spengler cyclization, the pentacyclic compounds 12 were synthesized.

五环骨架的构建及五个正确手性中心的确立:1.1我们以L-多巴为起始原料,经过多步官能团保护和转化合成了基本结构单元8然后和苯丙氨酸衍生物9,通过缩合反应生成酰胺中间体10,经Swern氧化得到醛化合物11,然后再次利用分子内改良的Pictet-Spengler反应一步构建c,d两环,得到五环骨架化合物12,最后,实现了21-位羰基向氰基的转化,得到了C-1位官能化的化合物14,化合物14不但具有和Et-743一致的五环骨架,而且分子中五个手性中心立体构型也与其完全相同:其中,3,位和13,位的手性中心由原料L-多巴带入,而1,位,11,位和21,位手性中心则通过不对称诱导而确立。

This research uses dicyandiamide as firming agent in epoxy powder coating and sodium fluoride as additive in epoxy.

采用磷酸双氰胺盐作环氧粉末涂料的固化剂、氟化钠作添加剂。

The same is carried out in the microwave, ethanol, dichloroethane, sodium carbonate, tetrabutylammonium iodide ammonium dissolved in dimethylformamide, then access to carbon dioxide.

同样是在微波炉中进行,把乙醇,氯乙烷,碳酸钠,四丁基碘化铵溶解在二甲基甲酰胺中,再通入二氧化碳。

The N-alkylation of N-monosubstituted sulfonamide s with alkyl halides promoted by KF using ionic liquids as reaction media was reported in this paper.

报道了KF作用下离子液体介质中N-单取代磺酰胺和卤代烃的N-烷基化反应,考察了4种不同结构的离子液体BF4、BF4和PF6对反应的影响。

Two artificial antigens Bz_HS_protein and Bz_SO 2_protein have been synthesized by the succinic anhydride_carbodiimide method and the sulfonyl chloride method separately.

用琥珀酸酐-碳二亚胺法和氯磺化法合成了毕兹的两种人工抗原Bz_HS_protein和Bz_SO2_protein。

Monochloroethylene carbonate is prepared by chlorination of ethylene carbonate with sulfuryl chioride ,a solution of monochloroethylene carbonate in ethylene carbonate is reacted with triethylamine to give vinylene carbonate.A parameter design method was applied to select the optimum synthesis conditions.63.3% and 78% yields superior to the conventional for monochloroethylene carbonate and vinylene carbonate were obtained respectively,and the process was also simplified .

以碳酸乙烯酯为原料,用磺酰氯作为氯化剂生成一氯代碳酸乙烯酯,三乙胺为脱卤化剂在碳酸乙烯酯溶剂中合成碳酸亚乙烯酯,对一氯代碳酸乙烯酯和碳酸亚乙烯酯制备的工艺参数进行优化,收率分别达到63.3%和78%,均超过了传统方法,且简化了工艺,缩短了反应时间,易于工业化生产。

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但我们并不在乎沙场中的显露。

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啊!不用提了。提到肉,真是糟透了。

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