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胺化

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Perfluoroguanidine can be prepared by the direct fluorination of dry ammeline with 5% fluorine at about -16℃.

全氟胍可以由于的三聚氰酰胺,用5%的氟在约-16℃直接进行氟化制得。

Perfluoroguanidine can be prepared by the direct fluorination of dry ammeline with 5% fluorine at about-16℃.

全氟胍可以由干的三聚氰酰胺,用5%的氟,在约-16℃直接进行氟化而制得。

So it has made the great progress. The method studied in this research from o-Dichlorobenzene is a ideal route to synthesize 2,4- dichlorofluorobenzene, which has temperate condition easy to control,safe process,low cost and good quality of products; The method of Phase transfer catalysis fluorination without solvent is better than present technology in presence of DMSO as solvent in many aspects; In a word,it is worth being promoted by the domestic correlative factories.

本课题所研究的以邻二氯苯为原料的2,4-二氯氟苯合成路线反应条件温和,工艺容易控制,生产安全,而且产品质量好,是比较理想的合成路线;以季胺盐为催化剂的无溶剂相转移催化氟化法与溶剂法相比具有明显的优势;通过实验确定的工艺条件对工业化生产有重要的指导意义,可提高以邻二氯苯为原料的工艺路线的市场竞争力。

METHODS: With formamide as dispersing agent, agarose was sulfated with the method of chlorosulfonic acid-pyridine.

以琼脂糖为原料,甲酰胺为分散剂,通过氯磺酸吡啶法制备了硫酸酯化琼脂糖。

The composing of CPA is: 25% DMSO,17% formamide, 10% propane-1, 2-diol and 6% PEG.

联合玻璃化保护剂的组成为:25%DMSO、17%甲酰胺、10%1,2-丙二醇和6%聚乙二醇。

The fuberidazole was prepared by reaction of O-phenylendiamine with furfural at the presence of CTMAB as catalyst.

以邻苯二胺和糠醛为原料,以十六甲基三烷基溴化铵为催化剂合成了麦穗宁。

Methods Activate GAMP with cyanogens bromide and prepare GAMP-protein conjugates using ADH as a linker and EDAC as a coupling agent.

方法采用溴化氰活化多糖,以无水己二酸二肼为连接剂,1-乙基-1-3-(3-二甲基氨基-丙基)-碳化二亚胺为偶联剂,制备结合物并免疫小鼠,检测小鼠血清中抗GAMP与抗载体蛋白抗体及抗GAMP抗体的杀菌活性。

Methods GAMP was activated with cyanogen bromide and combined with 1, 6-adipic acid dihydrazide. The prepared polysaccharide derivative GAMP-ADH was coupled to recombinant protein Pep10 with N-(3-dimethylaminopropyl)-N'-ethylcarbodiimide hydrochloride.

GAMP经溴化氰活化后,共价接合己二酰肼手臂,在碳二亚胺催化下与重组蛋白Pep10偶联,制备结合物GAMP-ADH-Pep10。

Methods Activate GAMP with cyanogens bromide and prepare GAMP-protein conjugates using ADH as a linker and EDAC as a coupling agent. Immunize mice with the conjugates and determine the antibodies against GAMP and carrier proteins in their sera as well as the bactericidal activity of antibody against GAMP.

采用溴化氰活化多糖,以无水己二酸二肼为连接剂,1-乙基-1-3-(3-二甲基氨基-丙基)-碳化二亚胺为偶联剂,制备结合物并免疫小鼠,检测小鼠血清中抗GAMP与抗载体蛋白抗体及抗GAMP抗体的杀菌活性。

Localization of Vps74p at the Golgi is not dependent on the N-terminal phosphorylation, but on its C-terminal domain.

Vps74p坐落在高基氏体是不需倚赖氮端被磷酸化,但是需要碳端的胺基酸序列。

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