胺化

The method of urea for three times and oxidized starch was used to synthesize dust depressor of sulfonated melamine-urea-formaldehyde resin s.

采用氧化淀粉和3次投加尿素进行改性的工艺合成了改性磺化三聚氰胺脲醛树脂抑尘剂。

The tea polyphenols have been determined by spectrophotometric analysis using the principle of colored compounds produced by the diazonium coupled reaction.

利用芳香族伯胺重氮化偶合生成有色化合物的原理，建立了分光光度法测定茶多酚含量的方法。

Diazonium salt which was formed by reaction of diazotization of eldest aromatic amine then coupling with N-(1-naphthyl)-ethylenediamine dihydrochloride,in NH_3·H_2O-NH_4Cl solution showed a sensitive polarographic wave at peak potential of 0.58vs,SCE.

本文报道了芳香族伯胺的重氮－偶氮化反应所生成的偶氮化合物在NH＿3·N＿2O－NH＿4Cl底液中，在单扫描极谱上，峰电位－0.58V

This method is based on the diazotization of sulfadiazine with sodium nitrite in acidic medium and the coupling reaction with α-naphthylamine.

在盐酸介质中，利用磺胺嘧啶－亚硝酸钠－α-萘胺的重氮化－偶合反应，建立了流动注射光度法测定磺胺嘧啶的新方法。

Chapter two: Using 5-(4-aminophenyl)-10,15,20-triphenylporphyrin as thestarting compound, the classical diazotization of aniline and the resulting reaction ofdiazo salts were applied to porphyrin for the first time, and a series of asymmetriclysubstituted meso-tetraarylporphyrins including 5-(4-chlorophenyl)-10,15,20-triphenylporphyrin, 5-(4-iodinphenyl)-10,15,20-triphenylporphyrin, 5-(4-cyanophenyl)-10,15,20-triphenylporphyrin, 5-(4-bisphenyl)-10,15,20-triphenylporphyrin and 5-(4-hydroxylphenyl)-10,15,20-triphenylporphyrin were synthesized.

第二章：在已合成的5-(4-氨基苯基)-10，15，20-三苯基卟啉基础上，首次将芳胺的重氮化及重氮盐反应应用于卟啉，合成了5-(4-氯苯基)-10，15，20-三苯基卟啉、5-(4-碘基苯基)-10，15，20-三苯基卟啉、5-(4-氰基苯基)-10，15，20-三苯基卟啉、5-(4-联苯基)-10，15，20-三苯基卟啉和5-(4-羟基苯基)-10，15，20-三苯基卟啉等一系列不对称取代的meso-四芳基卟啉。

Use nitrite and the Sulfanilic acid diazotization in acidic conditions,with dinitroaniline coupling formation color reaction,established the method of using the color reaction Determination Chinese cabbage s Nitrite content.

在酸性条件下亚硝酸盐与对氨基苯磺酸重氮化后，再与盐酸萘乙二胺偶合形成颜色反应，建立了用比色法测定大白菜中亚硝酸盐的方法。

The dual-site phase-transfer catalyst, 1,4-bisbenzene dibromide, was synthesized in toluene solution at 70℃ from p-xylylene dibromide and tributylamine.

双活性基相间转移触媒是由二溴对二甲苯与三丁胺以甲苯为溶剂在70℃下反应生成溴化1，4-二苯。

The article includes three parts. The first, a steroselective and regioselective synthesis of digitoxin with glycosyl ortho-alkynylbenzoates as doners. The second, synthesis of different length chain of L-fucose with a SO3Na group in the position of C-2 hydroxy.

本文工作主要包括三部分内容，分别为采用全新发展的一种邻炔基苯甲酸酯的糖基供体进行地高辛的全合成并与常规的Schimidt供体及三氟亚胺酯供体进行结果比较；合成不同长度的2位硫酸化的岩藻糖糖链；对现有的合成伏格列波糖的一条合成路线进行工艺优化。

A liquid amine ashless antioxidant HAO without phosphorus and zinc was prepared by alkylation of diphenylamine and 12 carbon iso olefin mixture, which can be applied at high temperature.

以二苯胺和含C12 的混合异构烯烃为原料，通过烷基化工艺，研制出了适于高温条件下应用的不含磷、锌元素的液态胺型无灰抗氧剂双十二烷基二苯胺。

The influence of each condition on the reaction speed and yield was studied, and the optimal conditions were: the ratio of the amount of substance of aromatic amine and heptafluoro-isopropyl iodine was 1:1.1~1.5, the amount of substance of sodium dithionite, sodium bicarbonate, aniline compounds were respectively 1.1~1.3, the amount of substance of phase transfer catalyst TBAB and aniline compounds was 0.05~0.1, the concentration of aniline compound was 0.5~1.0 mol/L, reaction temperature was 10~20 ℃, and the solvent was aether.

最佳结果为：芳胺与七氟异丙基碘的物质的量比1：1.1~1.5，连二亚硫酸钠、碳酸氢钠与苯胺的物质的量分别为1.1~1.3，相转移催化剂四丁基溴化铵与苯胺的物质的量比在0.05~0.1，溶剂总用量使苯胺浓度在0.5~1.0 mol/L；反应温度10~20℃；溶剂采用乙醚。取代基供电子性越强，反应时间越短，产率越高；氨基的对位优先反应，氨基的邻位较难发生反应；且七氟异丙基总是优先取代在芳环电子云密度较高的位置上。

But we don't care about Battlegrounds.

但我们并不在乎沙场中的显露。

Ah! don't mention it, the butcher's shop is a horror.

啊！不用提了。提到肉，真是糟透了。