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Polyvinyl alcohol amidoxime chelate fiber was synthesised by pre irradiation graft copolymerization and amidoximation.

利用60Co-γ射线预辐照接枝和胺肟化反应合成了含羧基的聚乙烯醇胺肟螯合纤维。

2-Substituted-3,4-dihydro-1(2H)-isoquinolinones were synthesized from methyl 3-hydroxy-ben- zoates via allyl etherification, Claisen rearrangement, oxidation, reductive amination and aminolysis for the first time.

以3-羟基-4-甲氧基苯甲酸甲酯等为原料,通过烯丙基醚化、Claisen重排、氧化、与伯胺反应、还原、分子内酯的胺解六步反应合成了一系列2-取代-3,4-二氢-1-异喹啉酮类化合物。

The effect of polyamines on callus browning and synthesis of endogenous polyamines and enthene during the development of callus,which initiated from mature embryo of Buchloe dactyloides texoka,was studied.

以野牛草成熟胚诱导的愈伤组织为材料,研究了外源多胺对愈伤组织褐化的影响及愈伤组织不同生长时期内源多胺和乙烯合成代谢规律。

In this chapter, the folate-EDA was covalently connected with heparin- campotothecin by carbodiimide activation to get a folate-heparin-campotothecin conjugate.

以乙二胺作为连接臂,通过酰胺键将氨基化的叶酸与肝素-喜树碱复合物连接起来,制备了一种叶酸偶联的肝素-喜树碱复合物。

The synthesis of the intermediate amidetriazinone was a crucial step in the synthesis of triazinone. Ethyl acetate was used as the initial material then was carried out for five steps hydrazine hydrate, triphosgene, chloroacetone, hydrazine hydrate respectively with the yield of 59.8%.

三嗪酮类化合物的合成关键是中间体氨基三嗪酮,本文以乙酸乙酯为起始原料,经过酯的肼解、成环反应、胺的烷基化、酮和肼的缩合、酰胺的水解五步反应合成中间体氨基三嗪酮,其收率达59.8%。

Copolymerize methacrylic acid 3(4′-N,N-dimethylamino) ketone xanthate and acrylamide were copolymerized with N,N-methylene bisacrylamide,and then combined with silane ethylene group in the form of covalent bond on the quartz glass shee t to be made into a sensor,to determine ethanol.

将甲基丙烯酸3-(4′-N,N-二甲氨基)黄酮酯和丙烯酰胺、N,N′-亚甲基双丙烯酰胺共聚并共价键合在硅烷化的含乙烯基团的石英玻片上,制成了可测定乙醇的传感器。

In this Ph. D. dissertation, reverse microemulsion method was fully used infabricating and modifying polyacrylamide with functional and high-relative moleculeweight. The copolymerization of 2-acrylamide-2-methylpxopanesulfonic acid, fluorescent monomer 4-methoxy-N-(2-N\', N\'-dimethylamino ethyl)naphthalimide alkyl chloride quaternary ammonium salt, fluorescentmonomer 4-(N\'-methyl-1-piperazinylallyl)-N-butyl-naphthalimide chloride quaternaryammonium salt, Cationic monomer dimethylethylammonium bromide and hydrophobical monomer octadecylacrylate with acrylamide and properties of the copolymers werestudied. The interaction between five polymers and Al_2O_3(012) crystal surface have beensimulated by Materials Studio 3.0 program package, binding energies and non-bondinteraction energies and deformation energies have also been acquired.

本文以制备具有较高相对分子质量和功能型PAM为研究目的,将反相微乳液法运用到其制备及改性的有关环节,通过反相微乳液聚合工艺,将几种改性功能单体2-丙烯酰胺基-2-甲基-丙磺酸、荧光单体2-(4-甲氧基-1,8-萘二甲酰亚胺基)-乙基二甲基烯丙基氯化铵、荧光单体4-(N'-甲基-1-哌嗪基)-N-丁基-1,8-萘烯丙氯季铵盐、阳离子单体丙烯酰氧乙基-二甲基-乙基溴化铵和疏水单体丙烯酸十八酯与AM共聚,制备AMPS改性PAM、荧光示踪型PAM、阳离子单体DMB改性PAM和OA改性PAM等四类不同功能单体改性PAM,并研究其应用性能。

Water, Sodium Laureth Sulfate, Cocamidopropyl Betaine, Cocamide MEA, Disodium Cocamphodiacetate, Sodium Lauryl Sulfate, PEG 40 Hydrogenated Castor Oil, Perfume, Sodium Chloride, Propylene Glycol, Quaternium 80, Methylparaben, Polyquaternium 10, Hydroxypropyl Guar Hydroxpropyltrimonium Chloride, Citric Acid, Diazolidinyl Urea, Tetrasodium EDTA, Polyquaternium 7, Propylparaben, Sodium Hydroxide, Panthenol, Persea Gratissima Oil, Penta Sodium Pentetate, Hedera Helix Extract, Bambusa Vulgaris Extract

水,月桂醇聚醚硫酸酯钠,椰油酰胺丙基甜菜碱,椰油酰胺MEA,椰油酰两性基二乙酸二钠,月桂醇硫酸酯钠,PEG 40 氢化篦麻油,香料,氯化钠,丙二醇,季铵盐-80,苯甲酸甲脂,聚季铵盐-10,羟丙基瓜尔胶羟丙基三甲基氯化铵,柠檬酸,重氮烷基咪唑脲,乙二氨四醋酸四钠,聚季铵盐-7,对羟基苯甲酸丙酯,氢氧化钠,泛酰醇,酪梨油,喷替酸五钠,常春藤萃取物,银竹萃取物。

Pharmacological results also indicated that the carbonyl and imino of Z-47 are important to its marked antiinflammatory and analgesic activity. The activity will be reduced or abolished with Z-47 converted to oximes or/and acetamides.

药理结果还表明,Z-47结构中的羰基和仲胺基对Z-47的显著抗炎镇痛作用具有重要的贡献,将Z-47羰基变成肟或/和将Z-47仲胺基酰化都会造成抗炎镇痛作用的降低甚至是丧失。

To our surprise, when the amount of iodide was added to 1:1 ratio with samarium, another different reaction occurred to give the iodination product (2Z)-2-alk-2-enoates in high yields.

同样地,结构类似的三氯乙醇酰胺的酯在二碘化钐的促进下也发生了类似的还原消除反应,以高产率得到N-(2,2-二氯乙烯)酰胺,该方法特色是条件温和,反应迅速。

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