胶糖
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We investigated constituent of triterpenoid saponins ofAlbizzia, two new compounds together with two known compounds were isolated from Albizzia julibrissin Durazz. by using column chromatography (macroreticular resin, silica gel, Sephadex gel, reverse phase silica gel),preparative HPLC methods et al.On the basis of spectroscopic analysis, including IR,ESI-MS,~1H-NMR,~(13)C-NMR,HMBC,HMQC,~1H-~1HCOSY and chemical methods, the structure of two new compounds were identified as 3 - O -[β-D-xylopyranosyl(1→2)-β-D-fucopyranosyl (1→6)-β- D -2- deoxy - 2 - acetoamidoglucopyranosyl] -21-O-[(6S)-2- trans- 2,6-dimethyl - 6 - O-β- D - quinovopyranosyl -2,7- octadienoyl] - acacic acid- 28 - O-β-D-glucopyranosyl(1→3)[α-L-arabinofuranosyl(1→4)]-α-L-rhamnopyranosyl(1→2)-β-D-glucopyranoside acacic acid 3- O -β- D- glucopyranosy(1→3)-β- D- fucopyranosl(1→6) [β-D- xylopyranosyl (1→2)]-β-D-glucopyranoside ;two known compounds were acacic acid lactone 3- O -β-D- xylopyranosyl-(1→2)-β-D-fucopyranosl (1→6)- 2-deoxy -2 -acetoamido -β-D- glucopyranoside ; acacic acid lactone 3- O-β-D-xylopyranosyl(1→2)-α-L- arabinopyranosl (1→6)- 2- deoxy - 2- acetoamido -β-D-glucopyranoside . The study lays chemical foundation and chemical reference substance for enhancing quality standard of Albizzia julibrissin Durazz.
本研究论文在综述国内外对合欢属Albizzia三萜皂苷化学成分和药理作用研究进展的基础上,利用传统植化分离手段和现代分离技术,包括大孔树脂、硅胶、葡聚糖凝胶、反相硅胶等柱色谱,制备高效液相色谱法等技术从中药合欢皮中分离得到了4个化合物,其中,2个新化合物和2个己知化合物,并进一步通过现代分析技术IR,ESI-MS,~1H-NMR,~(13C-NMR,HMBC,HMQC,~1H-~1HCOSY等和化学方法鉴定了2个新化合物的结构分别是:3-O-[β-D-吡喃木糖基(1→2)-β-D-吡喃夫糖基(1→6)-β-D-2-去氧-2-乙酰氨基吡喃葡萄糖基]-21-O-[(6S)-2-反式-2,6-二甲基-6-O-β-D-吡喃鸡纳糖基-2,7-辛二烯酸基]-金合欢酸-28-O-α-L-呋喃阿拉伯糖基(1→4)[β-D-吡喃葡萄糖基(1→3)]-α-L-吡喃鼠李糖基(1→2)-β-D-吡喃葡萄糖苷,金合欢酸3-O-β-D-吡喃葡萄糖基(1→3)-β-D-吡喃夫糖基(1→6)[β-D-吡喃木糖基(1→2)]-β-D-吡喃葡萄糖苷;2个已知化合物结构分别是:金和欢酸内酯3-O-β-D-吡喃木糖基(1→2)-β-D-吡喃夫糖基(1→6)-β-D-2-去氧-2-乙酰氨基吡喃葡萄糖苷,金和欢酸内酯3-O-β-D-吡喃木糖基(1→2)-α-L-吡喃阿拉伯糖基(1→6)-β-D-2-去氧-2-乙酰氨基吡喃葡萄糖苷。
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Low molecular weight mannuronic acid, guluronic acid and κ-carrageenan were prepared from algin and carrageenan by the acid hydrolysis method, and their weight average molecular weights and the distribution widths of molecular weight were determined by high performance gel permeation chromatography respectively.
本文以褐藻胶和κ-卡拉胶为原料通过酸水解分别获得了低聚的甘露糖醛酸,古罗糖醛酸和低聚κ-卡拉胶,并采用HPGPC法测定了这3种低聚糖的重均分子量。
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Low molecular weight mannuronic acid, guluronic acid and κ carrageenan were prepared from algin and carrageenan by the acid hydrolysis method, and their weight average molecular weights and the distribution widths of molecular weight were determined by high performance gel permeation chromatography respectively.
本文以褐藻胶和κ-卡拉胶为原料通过酸水解分别获得了低聚的甘露糖醛酸、古罗糖醛酸和低聚κ-卡拉胶,并采用 HPGPC法测定了这 3种低聚糖的重均分子量。在此基础上再经硫酸酯化和成盐修饰制备了各自的硫酸酯碱式铝盐。
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Algin ; carrageenan ; mannuronic acid ; guluronic acid ; polysaccharide ; sulfate ; aluminium ; peptic ulcer
褐藻胶;卡拉胶;甘露糖醛酸;古罗糖醛酸;多糖;硫酸酯;铝;消化性溃疡
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Then test of film cell growth by high sugar, LPS, high sugar plus LPS was done with the result showing that FANG KIDNEY capsule can restrain the growth of film cell and composition of external base, it can be concluded that it has obvious effect in preventing the hardening of kidney small cell.
为进一步探讨糖肾胶囊的作用机制,还采用国内外经典细胞培养方法,成功地培养出肾小球系膜细胞,在此基础上进行高糖、LPS、及高糖加LPS诱导细胞膜增生,结果发现糖肾胶囊能抑制系膜细胞增生及细胞外基质胶原合成,证明其对防止肾小球硬化有明显作用。
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The effect of initial pH, temperature and N263 concentratio n on extraction of fucoidan was investigated. It has shown that temperature and initial pH of the solutions have no great influences on the extraction of fucoid an, and when N263 concentration is low, an increase in the concentration incre ases the extraction of fucoidan.
对影响萃取褐藻糖胶的水溶液初始pH、温度及N263浓度等因素研究结果表明,N263浓度是影响褐藻糖胶萃取的主要因素,而初始pH、温度等的影响不大。
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The methodology and its mechanism for the biomimetic synthesis of HAp/Col bone-like composite by in vitro imitating bone biomineralization and self-assemble process of materials is reviewed here. hydroxyapatite/collagen ; bonelike composite ; biomineralization ; self-assembly
从成分上来讲,天然骨除了含有羟基磷灰石无机成分外,还含有胶原(collagen,Col)、糖蛋白、糖胺聚糖等少量的有机成分无机物与有机物含量之比约为7∶3,其中胶原占有机质重量的90%犤2
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The molar ratio of sulfate ions to carboxylate ions is determined by conductometric titration method and the molecular weight is tested by high performance gel permeation chromatography. The precision of these two methods is also studied. To improve the detection sensitivity, guanidine hydrochloride is used as the best derivation reagent of 911. A systematic research is done on the optimum derivatization condition of 911 and Guanidine hydrochloride. The M /G ratio of 911 has direct relation to its biological activity.
论文首先对911的基本理化性质进行了系统的分析,以电导滴定法和高效凝胶渗透色谱法分别测定了分子中硫酸根羧酸根的比值和911的分子量,并探讨了两种分析方法的精密度。911分子没有紫外吸收,为提高检测灵敏度,本文采用荧光标记法,通过对三种荧光试剂与几种寡糖和多糖衍生效果的综合比较,最终确定了盐酸胍为最佳衍生试剂,并以911为代表详细探讨了衍生化反应的最优条件。911糖链结构与褐藻胶主链结构类似,以甘露糖醛酸和古罗糖醛酸的嵌段形式存在,分子中M/G比值与911的物理化学性质和生物活性有直接关系。
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The research displayed that yeasts Genus level can be discerned by agarose gel electrophoresis and polyacarylamide gel electrophoresis, but the latter is more advanced. The Saccharomyces cerevisiae strains ITS-1 sequences are most disalike, few of them are equal completely. The bigger differences are part of base pairs about Poly-T, others are exchanged by single base pair.
研究表明,以酵母菌株的rDNA ITS-1序列进行琼脂糖凝胶电泳,能把菌株分类鉴定到属的水平;采用非变性聚丙烯酰胺凝胶电泳能把部分酿酒酵母菌株分类鉴定到种的水平,区别效果较琼脂糖凝胶电泳有所提高;对rDNA ITS-1序列进行克隆、测序,经序列比对后发现,酿酒酵母属中酿酒酵母菌株的ITS-1序列大多数有差异,差异主要表现在ITS-1序列上游的一段Poly-T碱基上,其它处的差异仅是个别碱基的转换或颠换,ITS-1序列长度分布在360-370bp之间,G+C%含量均在35.3%左右。
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INGREDIENTS: skim milk, sugar, cream, chocolaty chips (sugar, coconut oil, cocoa processed with alkali, partially hydrogenated coconut oil, cocoa, salt, soy lecithin, natural flavor), corn syrup, cocoa processed with alkali, whey protein, egg yolks, tapioca maltodextrin, soy protein, natural flavor, Propylene Glycol Monostearate, guar gum, carrageenan, cellulose gum, mono and diglycerides, salt, malt extract, xanthan gum, molasses, vitamin A palmitate, dextrose, caramel color
成分:脱脂牛奶,糖,奶油, chocolaty芯片(糖,椰子油,可可碱处理,部分氢化的椰子油,可可粉,盐,酱油,卵磷脂,天然香料),玉米糖浆,可可碱处理,乳清蛋白,蛋蛋黄,木薯麦芽糊精,大豆蛋白,天然香料,丙二醇酯,瓜尔豆胶,卡拉胶,纤维素胶,单声道和diglycerides ,盐,麦芽提取物,黄原胶,糖蜜,维生素A棕榈酸酯,葡萄糖,焦糖色
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On the other hand, the more important thing is because the urban housing is a kind of heterogeneity products.
另一方面,更重要的是由于城市住房是一种异质性产品。
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Climate histogram is the fall that collects place measure calm value, cent serves as cross axle for a few equal interval, the area that the frequency that the value appears according to place is accumulated and becomes will be determined inside each interval, discharge the graph that rise with post, also be called histogram.
气候直方图是将所收集的降水量测定值,分为几个相等的区间作为横轴,并将各区间内所测定值依所出现的次数累积而成的面积,用柱子排起来的图形,也叫做柱状图。
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You rap, you know we are not so good at rapping, huh?
你唱吧,你也知道我们并不那么擅长说唱,对吧?