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胶溶

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The influences of N,N'-methene biacrylamide cross-linker,monomer concentration,polymerization time and temperature on swelling ratio were investigated,and reversibility of the hydrogels under various pH conditions at given temperature.

目的通过合成聚丙烯酸-co-α-甲基丙烯酸水凝胶,研究N,N'-亚甲基双丙烯酰胺交联剂、丙烯酸和α-甲基丙烯酸单体浓度、聚合时间对其水凝胶溶胀率的影响,以及温度和不同pH值时水凝胶的pH可逆性。

The conditions of synthesis, such as mass ratio of monomer, and different dry method, were investigated.

考察了原料配比和干燥方法对凝胶溶胀性能的影响,研究了其pH敏感性及pH溶胀-退胀特性。

The effect of the amount of silica powder and sulfuric acid employed as well as polyacrylamide added on the properties of the gel electrolyte was studied and the mechanism of the peptization of silica powder to form thixotropic silica gel electrolyte was discussed.

研究了SiO2粉末和H2SO4用量及聚丙烯酰胺添加量对凝胶电解液性能的影响,并分析讨论了SiO2粉末胶溶形成触变性硅凝胶电解液的机理和特点。

The A13 sol and Al(0H)3—Zr4 sol is prepared by peptization method with A1(NO3)3 , ZrOCl2 and NH3H2O as starting materials, using A1(NO3)3 solution and Zr4 sol as peptizing agents, and the preparation process, preparation conditions and colloid structure are analyzed.

本文以Al(NO_3)_3,ZrOCl_2和氨水为原料,分别以Al(NO_3)_3溶液和Zr_4溶胶作为胶溶剂,通过胶溶法制备Al_3溶胶和Al_3—Zr_4溶胶,并对两种溶胶的制备过程,制备条件和胶团结构进行了分析。

During the process of peptization and hydrothermal crystallization, the aggregation behavior and the resulting morphology of nanocrystalline titania (TiO2) were studied by X-ray diffraction, scanning electron microscope, and dynamic light scattering techniques.

通过XRD、SEM和动态光散射粒度测定仪研究了胶溶及水热晶化过程中纳米TiO2晶粒聚集行为及形貌。实验结果表明,在胶溶无定形沉淀过程中所形成的大小为10-15nm的锐钛矿型胶粒或金红石型胶粒易定向聚集成更大的、具有(30-50)nm×(80-100)nm的次级晶粒。含有次级晶粒的溶胶前驱液在水热晶化过程中,次级晶粒发生崩裂并生长成结晶度更高的大小约为10-30nm球形和大小约为20-60nm棒状纳米TiO2

Under the vacuum,the composite is heated up by this machine to be in the peptization,so that two pieces of glass cement can be agglutinated together. This special kind of machine is used to produce doubling nipped silk, textile insertion, nipped net and arts and crafts glass with various designs.

CH-玻璃夹胶机:本机器利用真空条件下将物体加热,使其中复合材料达到胶溶液态,从而使两件玻璃胶合在一起的专用夹胶机设备,主要适用于安全玻璃生产,通过新的纳米线生产玻璃线结构,该设备可生产夹胶、夹丝、夹布、夹网及各种图案的工艺玻璃。

Aluminum Ispropoxide was hydrolyzed to prepare Al〓O〓 sol. The hydrolyzed 〓CHOH affected the sol peptization. The colloidal particle was the smallest when the peptization time was 12 hours.γ-Al〓O〓 membrane without cracks, thickness about 2μm, was prepared from 1M sol with a suitable amount of PVA solution. The mean pore size of the membrane was about 3nm. And, the H〓/N〓 separation factor was 3. 53, exhibiting good separation performance.

异丙醇铝为前驱体,水解制备Al〓O〓溶胶,水解产生的异丙醇影响溶胶的胶溶效果,并且胶溶12小时得到的胶粒最小。1M溶胶加PVA制备厚度2μm左右,无开裂γ-Al〓O〓膜,经600℃煅烧,平均孔径为3nm,H〓/N〓分离系数可达到3.53,表现了很好的分离性能。

Secondly, according to the construction and characteristic of the N-isopropylacrylamide and the temperature-sensitivity of PNIPA hydrogel, Pdualistic hydrogel was synthesized by microwave low temperature plasma. The effects of the factors on the swelling characteristic of P dualistic hydrogel, such as treatment time and power of plasma, concentrations of crosslinking agent and total monomers, proportion of AMPS, polymerizing temperature etc, was discussed in detail. The three dimensions structure , thermostability , reversional volume , swelling/deswelling kinetics, temperature-sensitivity and pH-sensitivity of the hydrogel were also investigated. The optimal synthesizing technics of P dualistic hydrogel initiated by microwave low temperature plasma was confirmed.

在此基础上,结合NIPA的结构特征和PNIPA的温敏性,用微波低温等离子体引发聚合了P二元智能凝胶,详细探讨了微波低温等离子体处理功率、处理时间、总单体浓度、AMPS单体浓度、交联剂浓度及聚合反应溫度等因素对P二元凝胶溶胀性能的影响;并对其三维交联结构、热稳定性、失水-吸水动力学、温度敏感性、pH敏感性、体积复原性等进行了研究;确定了适合微波低温等离子体引发聚合P二元智能凝胶的最佳工艺。

The peptizing temperature, the concentration of acids and the peptizing time have effect on the process of crystalizing and the growing up of the crystalline.

胶溶时的温度、酸浓度及胶溶时间对晶化过程和晶粒长大均有显著影

The peptizing mechanism of pseudo-boehmite powder was analyzed, and the multi- nucleus model of colloidal nucleus and electrical double layers model of micelle were proposed, based on the measurement of conductivity, the analysis of IR infrared spectra and the equilibrium profiles of dissolution-precipitation for Al3+ at different pH values.

通过胶溶过程中电导率的测定、胶团表面基团的FTIR分析和Al~(3+)的沉淀溶解平衡的热力学分析,提出了拟薄水铝石的胶溶过程机理、胶核的多核结构模型和胶团的双电层结构模型。

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